DE112007001382T5 - Alkalimetalltitanate und Verfahren zu deren Synthese - Google Patents

Alkalimetalltitanate und Verfahren zu deren Synthese Download PDF

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Publication number
DE112007001382T5
DE112007001382T5 DE112007001382T DE112007001382T DE112007001382T5 DE 112007001382 T5 DE112007001382 T5 DE 112007001382T5 DE 112007001382 T DE112007001382 T DE 112007001382T DE 112007001382 T DE112007001382 T DE 112007001382T DE 112007001382 T5 DE112007001382 T5 DE 112007001382T5
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DE
Germany
Prior art keywords
mixture
alkali metal
lithium titanate
doped
dopant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE112007001382T
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German (de)
English (en)
Inventor
Pu Ann Arbor Zhang
Suresh Ann Arbor Mani
Michael R. Ann Arbor Wixom
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
A123 Systems LLC
Original Assignee
T/J Technologies Inc Ann Arbor
TJ Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by T/J Technologies Inc Ann Arbor, TJ Technologies Inc filed Critical T/J Technologies Inc Ann Arbor
Publication of DE112007001382T5 publication Critical patent/DE112007001382T5/de
Granted legal-status Critical Current

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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • C01G23/003Titanates
    • C01G23/005Alkali titanates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00Compounds of zirconium
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/50Solid solutions
    • C01P2002/52Solid solutions containing elements as dopants
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
DE112007001382T 2006-06-05 2007-06-05 Alkalimetalltitanate und Verfahren zu deren Synthese Granted DE112007001382T5 (de)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US81094206P 2006-06-05 2006-06-05
US60/810,942 2006-06-05
US82267506P 2006-08-17 2006-08-17
US60/822,675 2006-08-17
US11/757,658 2007-06-04
US11/757,658 US7879493B2 (en) 2006-06-05 2007-06-04 Alkali metal titanates and methods for their synthesis
PCT/US2007/070387 WO2007143640A2 (en) 2006-06-05 2007-06-05 Alkali metal titanates and methods for their synthesis

Publications (1)

Publication Number Publication Date
DE112007001382T5 true DE112007001382T5 (de) 2009-05-07

Family

ID=38790638

Family Applications (1)

Application Number Title Priority Date Filing Date
DE112007001382T Granted DE112007001382T5 (de) 2006-06-05 2007-06-05 Alkalimetalltitanate und Verfahren zu deren Synthese

Country Status (6)

Country Link
US (1) US7879493B2 (enExample)
JP (1) JP5362555B2 (enExample)
KR (1) KR101410844B1 (enExample)
CA (1) CA2654605A1 (enExample)
DE (1) DE112007001382T5 (enExample)
WO (1) WO2007143640A2 (enExample)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102008026580A1 (de) * 2008-06-03 2009-12-10 Süd-Chemie AG Verfahren zur Herstellung von Lithiumtitan-Spinell und dessen Verwendung
DE102009049470A1 (de) * 2009-10-15 2011-04-28 Süd-Chemie AG Verfahren zur Herstellung von feinteiligen Lithiumtitan-Spinellen und deren Verwendung
DE102009049693A1 (de) 2009-10-16 2011-04-21 Süd-Chemie AG Phasenreines Lithiumaluminiumtitanphosphat und Verfahren zur Herstellung und dessen Verwendung
WO2011145443A1 (ja) * 2010-05-18 2011-11-24 株式会社 村田製作所 電極活物質およびその製造方法、ならびにそれを備えた非水電解質二次電池
JP5672859B2 (ja) 2010-08-26 2015-02-18 宇部興産株式会社 微細な炭素繊維と複合化されたリチウムチタン複合酸化物電極材料
WO2012111294A1 (ja) * 2011-02-15 2012-08-23 パナソニック株式会社 リチウムイオン二次電池用負極活物質材料およびその製造方法
EP2677575B1 (en) * 2011-02-15 2017-06-28 Panasonic Intellectual Property Management Co., Ltd. Negative electrode active material for lithium ion secondary battery, and manufacturing method for same
KR101262054B1 (ko) 2011-02-17 2013-05-09 이화여자대학교 산학협력단 2차원 나노구조 리튬 티타늄 산화물, 그 제조방법 및 상기 2차원 나노구조 리튬 티타늄 산화물을 포함한 전극 물질
CN103503218B (zh) * 2011-04-20 2016-02-03 松下知识产权经营株式会社 非水电解质二次电池
CN102842706B (zh) * 2011-06-22 2015-05-13 比亚迪股份有限公司 一种钛酸锂材料的制备方法及钛酸锂材料、锂离子电池
JP5897444B2 (ja) * 2011-10-28 2016-03-30 富士フイルム株式会社 非水二次電池用電解液及び二次電池
WO2013081231A1 (ko) * 2011-11-30 2013-06-06 주식회사 휘닉스소재 이종 금속이 도핑된 리튬 티탄 복합 산화물의 제조 방법, 및 이에 의하여 제조된 이종 금속이 도핑된 리튬 티탄 복합 산화물
DE102012208608A1 (de) * 2012-05-23 2013-11-28 Robert Bosch Gmbh Verfahren zum Herstellen einer Elektrode für einen elektrochemischen Energiespeicher und Elektrode
CN102780005B (zh) * 2012-08-20 2015-11-11 山东大学 一种钇改性的钛酸锂负极材料及其制备方法
CN103771500B (zh) * 2012-10-18 2015-06-24 上海纳米技术及应用国家工程研究中心有限公司 锂离子二次电池a、b位同时掺杂纳米钛酸锂的制备方法
GB201306814D0 (en) * 2013-04-15 2013-05-29 Johnson Matthey Plc Improvements in lithium-containing materials
KR101796233B1 (ko) * 2013-05-23 2017-12-01 주식회사 포스코 이종 금속이 도핑된 리튬 티탄 복합 산화물의 제조 방법, 및 이에 의하여 제조된 이종 금속이 도핑된 리튬 티탄 복합 산화물
RU2558140C1 (ru) * 2014-02-18 2015-07-27 Общество с ограниченной ответственностью "Научный центр "Автономные источники тока" (ООО "Научный центр "АИТ") АНОДНЫЙ МАТЕРИАЛ ЛИТИЙ-ИОННОГО АККУМУЛЯТОРА НА ОСНОВЕ LiCrTiO4 СО СТРУКТУРОЙ ШПИНЕЛИ И СПОСОБ ЕГО ПОЛУЧЕНИЯ
WO2015138019A1 (en) * 2014-03-12 2015-09-17 Imra America,Inc. Negative electrode active material for energy storage devices and method for making the same
EP3327833B1 (en) * 2015-12-24 2021-06-02 LG Chem, Ltd. Negative electrode active material having improved output characteristics and electrode for electrochemical device including the negative electrode active material
CN108417823B (zh) * 2018-02-28 2021-03-30 华南理工大学 一种利用重复球磨法制备的Li2FeTi1-yMoyO4材料及其制备方法与应用
JP7771597B2 (ja) * 2020-09-28 2025-11-18 Ube株式会社 チタン酸リチウム粉末、それを用いた電極、及び蓄電デバイス

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3502118B2 (ja) 1993-03-17 2004-03-02 松下電器産業株式会社 リチウム二次電池およびその負極の製造法
DE69727285T2 (de) 1996-06-14 2004-11-25 Hitachi Maxell, Ltd., Ibaraki Sekundäre lithiumbatterie
JPH10251020A (ja) * 1997-03-11 1998-09-22 Ishihara Sangyo Kaisha Ltd 金属置換チタン酸リチウムおよびその製造方法ならびにそれを用いてなるリチウム電池
US6221531B1 (en) 1998-07-09 2001-04-24 The University Of Chicago Lithium-titanium-oxide anodes for lithium batteries
JP4540167B2 (ja) 1999-02-16 2010-09-08 東邦チタニウム株式会社 チタン酸リチウムの製造方法
US6645673B2 (en) 1999-02-16 2003-11-11 Toho Titanium Co., Ltd. Process for producing lithium titanate and lithium ion battery and negative electrode therein
JP3625680B2 (ja) * 1999-03-25 2005-03-02 三洋電機株式会社 リチウム二次電池
JP2001354421A (ja) * 2000-06-08 2001-12-25 Toyota Central Res & Dev Lab Inc リチウム二次電池電極活物質用リチウムチタン複合酸化物およびその製造方法
US7211350B2 (en) * 2001-01-29 2007-05-01 Rutgers University Foundation Nanostructure lithium titanate electrode for high cycle rate rechargeable electrochemical cell
US6827921B1 (en) 2001-02-01 2004-12-07 Nanopowder Enterprises Inc. Nanostructured Li4Ti5O12 powders and method of making the same
WO2003008334A1 (en) 2001-07-20 2003-01-30 Altair Nanomaterials Inc. Process for making lithium titanate
US6706445B2 (en) * 2001-10-02 2004-03-16 Valence Technology, Inc. Synthesis of lithiated transition metal titanates for lithium cells
ATE485241T1 (de) 2002-03-08 2010-11-15 Altair Nanomaterials Inc Verfahren zur herstellung nanoskaliger und submikronskaliger lithium-übergangsmetalloxide
DE10319464A1 (de) 2003-04-29 2004-11-18 Basf Ag Verfahren zur Herstellung von nanokristallinen Lithiumtitanat-Spinellen

Also Published As

Publication number Publication date
WO2007143640A2 (en) 2007-12-13
US20070281211A1 (en) 2007-12-06
US7879493B2 (en) 2011-02-01
JP5362555B2 (ja) 2013-12-11
JP2009542562A (ja) 2009-12-03
KR20090015131A (ko) 2009-02-11
WO2007143640A3 (en) 2008-10-09
KR101410844B1 (ko) 2014-06-23
CA2654605A1 (en) 2007-12-13

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Owner name: A123 SYSTEMS INC. ( N.D. GES. D. STAATES DELAW, US

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