JP5362555B2 - アルカリ金属チタン酸塩及びそれらの合成方法 - Google Patents

アルカリ金属チタン酸塩及びそれらの合成方法 Download PDF

Info

Publication number
JP5362555B2
JP5362555B2 JP2009514491A JP2009514491A JP5362555B2 JP 5362555 B2 JP5362555 B2 JP 5362555B2 JP 2009514491 A JP2009514491 A JP 2009514491A JP 2009514491 A JP2009514491 A JP 2009514491A JP 5362555 B2 JP5362555 B2 JP 5362555B2
Authority
JP
Japan
Prior art keywords
lithium
alkali metal
mixture
dopant
lithium titanate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2009514491A
Other languages
English (en)
Japanese (ja)
Other versions
JP2009542562A (ja
JP2009542562A5 (enExample
Inventor
プ ザン
スレッシュ マニ
マイケル アール ウィクソム
Original Assignee
エイ123 システムズ インコーポレイテッド
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by エイ123 システムズ インコーポレイテッド filed Critical エイ123 システムズ インコーポレイテッド
Publication of JP2009542562A publication Critical patent/JP2009542562A/ja
Publication of JP2009542562A5 publication Critical patent/JP2009542562A5/ja
Application granted granted Critical
Publication of JP5362555B2 publication Critical patent/JP5362555B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • C01G23/003Titanates
    • C01G23/005Alkali titanates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00Compounds of zirconium
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/50Solid solutions
    • C01P2002/52Solid solutions containing elements as dopants
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
JP2009514491A 2006-06-05 2007-06-05 アルカリ金属チタン酸塩及びそれらの合成方法 Active JP5362555B2 (ja)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US81094206P 2006-06-05 2006-06-05
US60/810,942 2006-06-05
US82267506P 2006-08-17 2006-08-17
US60/822,675 2006-08-17
US11/757,658 2007-06-04
US11/757,658 US7879493B2 (en) 2006-06-05 2007-06-04 Alkali metal titanates and methods for their synthesis
PCT/US2007/070387 WO2007143640A2 (en) 2006-06-05 2007-06-05 Alkali metal titanates and methods for their synthesis

Publications (3)

Publication Number Publication Date
JP2009542562A JP2009542562A (ja) 2009-12-03
JP2009542562A5 JP2009542562A5 (enExample) 2010-07-22
JP5362555B2 true JP5362555B2 (ja) 2013-12-11

Family

ID=38790638

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2009514491A Active JP5362555B2 (ja) 2006-06-05 2007-06-05 アルカリ金属チタン酸塩及びそれらの合成方法

Country Status (6)

Country Link
US (1) US7879493B2 (enExample)
JP (1) JP5362555B2 (enExample)
KR (1) KR101410844B1 (enExample)
CA (1) CA2654605A1 (enExample)
DE (1) DE112007001382T5 (enExample)
WO (1) WO2007143640A2 (enExample)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102008026580A1 (de) * 2008-06-03 2009-12-10 Süd-Chemie AG Verfahren zur Herstellung von Lithiumtitan-Spinell und dessen Verwendung
DE102009049470A1 (de) * 2009-10-15 2011-04-28 Süd-Chemie AG Verfahren zur Herstellung von feinteiligen Lithiumtitan-Spinellen und deren Verwendung
DE102009049693A1 (de) 2009-10-16 2011-04-21 Süd-Chemie AG Phasenreines Lithiumaluminiumtitanphosphat und Verfahren zur Herstellung und dessen Verwendung
JP5553110B2 (ja) * 2010-05-18 2014-07-16 株式会社村田製作所 電極活物質およびその製造方法、ならびにそれを備えた非水電解質二次電池
JP5672859B2 (ja) 2010-08-26 2015-02-18 宇部興産株式会社 微細な炭素繊維と複合化されたリチウムチタン複合酸化物電極材料
WO2012111294A1 (ja) * 2011-02-15 2012-08-23 パナソニック株式会社 リチウムイオン二次電池用負極活物質材料およびその製造方法
EP2677575B1 (en) * 2011-02-15 2017-06-28 Panasonic Intellectual Property Management Co., Ltd. Negative electrode active material for lithium ion secondary battery, and manufacturing method for same
KR101262054B1 (ko) 2011-02-17 2013-05-09 이화여자대학교 산학협력단 2차원 나노구조 리튬 티타늄 산화물, 그 제조방법 및 상기 2차원 나노구조 리튬 티타늄 산화물을 포함한 전극 물질
EP2701231A4 (en) * 2011-04-20 2014-11-19 Panasonic Corp SECONDARY BATTERY WITH NON-WATER ELECTROLYTE
CN102842706B (zh) * 2011-06-22 2015-05-13 比亚迪股份有限公司 一种钛酸锂材料的制备方法及钛酸锂材料、锂离子电池
JP5897444B2 (ja) * 2011-10-28 2016-03-30 富士フイルム株式会社 非水二次電池用電解液及び二次電池
WO2013081231A1 (ko) * 2011-11-30 2013-06-06 주식회사 휘닉스소재 이종 금속이 도핑된 리튬 티탄 복합 산화물의 제조 방법, 및 이에 의하여 제조된 이종 금속이 도핑된 리튬 티탄 복합 산화물
DE102012208608A1 (de) * 2012-05-23 2013-11-28 Robert Bosch Gmbh Verfahren zum Herstellen einer Elektrode für einen elektrochemischen Energiespeicher und Elektrode
CN102780005B (zh) * 2012-08-20 2015-11-11 山东大学 一种钇改性的钛酸锂负极材料及其制备方法
CN103771500B (zh) * 2012-10-18 2015-06-24 上海纳米技术及应用国家工程研究中心有限公司 锂离子二次电池a、b位同时掺杂纳米钛酸锂的制备方法
GB201306814D0 (en) * 2013-04-15 2013-05-29 Johnson Matthey Plc Improvements in lithium-containing materials
KR101796233B1 (ko) * 2013-05-23 2017-12-01 주식회사 포스코 이종 금속이 도핑된 리튬 티탄 복합 산화물의 제조 방법, 및 이에 의하여 제조된 이종 금속이 도핑된 리튬 티탄 복합 산화물
RU2558140C1 (ru) * 2014-02-18 2015-07-27 Общество с ограниченной ответственностью "Научный центр "Автономные источники тока" (ООО "Научный центр "АИТ") АНОДНЫЙ МАТЕРИАЛ ЛИТИЙ-ИОННОГО АККУМУЛЯТОРА НА ОСНОВЕ LiCrTiO4 СО СТРУКТУРОЙ ШПИНЕЛИ И СПОСОБ ЕГО ПОЛУЧЕНИЯ
WO2015138019A1 (en) * 2014-03-12 2015-09-17 Imra America,Inc. Negative electrode active material for energy storage devices and method for making the same
WO2017111566A1 (ko) 2015-12-24 2017-06-29 주식회사 엘지화학 출력 특성이 향상된 음극 활물질 상기 음극 활물질을 포함하는 전기화학소자용 전극
CN108417823B (zh) * 2018-02-28 2021-03-30 华南理工大学 一种利用重复球磨法制备的Li2FeTi1-yMoyO4材料及其制备方法与应用
JP7771597B2 (ja) * 2020-09-28 2025-11-18 Ube株式会社 チタン酸リチウム粉末、それを用いた電極、及び蓄電デバイス

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3502118B2 (ja) * 1993-03-17 2004-03-02 松下電器産業株式会社 リチウム二次電池およびその負極の製造法
US6379843B1 (en) * 1996-06-14 2002-04-30 Hitachi Maxwell, Ltd. Nonaqueous secondary battery with lithium titanium cathode
JPH10251020A (ja) * 1997-03-11 1998-09-22 Ishihara Sangyo Kaisha Ltd 金属置換チタン酸リチウムおよびその製造方法ならびにそれを用いてなるリチウム電池
US6221531B1 (en) * 1998-07-09 2001-04-24 The University Of Chicago Lithium-titanium-oxide anodes for lithium batteries
US6645673B2 (en) * 1999-02-16 2003-11-11 Toho Titanium Co., Ltd. Process for producing lithium titanate and lithium ion battery and negative electrode therein
JP4540167B2 (ja) * 1999-02-16 2010-09-08 東邦チタニウム株式会社 チタン酸リチウムの製造方法
JP3625680B2 (ja) * 1999-03-25 2005-03-02 三洋電機株式会社 リチウム二次電池
JP2001354421A (ja) * 2000-06-08 2001-12-25 Toyota Central Res & Dev Lab Inc リチウム二次電池電極活物質用リチウムチタン複合酸化物およびその製造方法
US7211350B2 (en) * 2001-01-29 2007-05-01 Rutgers University Foundation Nanostructure lithium titanate electrode for high cycle rate rechargeable electrochemical cell
US6827921B1 (en) * 2001-02-01 2004-12-07 Nanopowder Enterprises Inc. Nanostructured Li4Ti5O12 powders and method of making the same
US6890510B2 (en) * 2001-07-20 2005-05-10 Altair Nanomaterials Inc. Process for making lithium titanate
US6706445B2 (en) * 2001-10-02 2004-03-16 Valence Technology, Inc. Synthesis of lithiated transition metal titanates for lithium cells
US6881393B2 (en) * 2002-03-08 2005-04-19 Altair Nanomaterials Inc. Process for making nano-sized and sub-micron-sized lithium-transition metal oxides
DE10319464A1 (de) * 2003-04-29 2004-11-18 Basf Ag Verfahren zur Herstellung von nanokristallinen Lithiumtitanat-Spinellen

Also Published As

Publication number Publication date
JP2009542562A (ja) 2009-12-03
KR101410844B1 (ko) 2014-06-23
CA2654605A1 (en) 2007-12-13
US7879493B2 (en) 2011-02-01
WO2007143640A2 (en) 2007-12-13
DE112007001382T5 (de) 2009-05-07
WO2007143640A3 (en) 2008-10-09
US20070281211A1 (en) 2007-12-06
KR20090015131A (ko) 2009-02-11

Similar Documents

Publication Publication Date Title
JP5362555B2 (ja) アルカリ金属チタン酸塩及びそれらの合成方法
EP3145870B1 (en) Doped nickelate materials
US6680143B2 (en) Lithium metal oxide electrodes for lithium cells and batteries
US20250015260A1 (en) Cathode with disordered rocksalt material and method of forming the cathode
EP2361888B1 (en) Titanium oxide-based compound for electrode and lithium secondary battery using the same
JP5879761B2 (ja) リチウム複合化合物粒子粉末及びその製造方法、並びに非水電解質二次電池
CN101485015A (zh) 碱金属钛酸盐及它们的合成方法
JP5177672B2 (ja) リチウム電池用活物質及びその製造方法、並びにそれを用いたリチウム電池
JP2008255000A (ja) 新規チタン酸化物及びその製造方法、並びにそれを活物質として用いたリチウム二次電池
TWI636960B (zh) 鈦酸化合物、鈦酸鹼金屬化合物及此等的製造方法,以及將此等作爲活性物質使用的蓄電裝置
TW201312841A (zh) 用於鋰離子電化學電池之高容量正電極及其製造方法
JP4997609B2 (ja) リチウムマンガン系複合酸化物の製造方法
US20110223098A1 (en) Titanium oxide and method of producing the same
US20060003229A1 (en) Rechargeable electrochemical cell
JP2016522137A (ja) チタン酸リチウムの調製方法
TWI572561B (zh) Lithium manganate particles for nonaqueous electrolyte storage batteries and methods for producing the same, and nonaqueous electrolyte batteries
WO2018169004A1 (ja) ニッケルマンガン系複合酸化物及びその製造方法
JP6826447B2 (ja) 正極活物質粒子中の残存リチウム量の低減方法
JP5810752B2 (ja) チタン酸リチウム粒子粉末、非水電解質二次電池用負極活物質粒子粉末並びに非水電解質二次電池
JP5196486B2 (ja) 複合チタン酸化物の製造方法
CN109643787A (zh) 电极材料、电极材料用于基于锂离子的电化学电池的用途、基于锂离子的电化学电池
JP2017188421A (ja) 非水電解質二次電池用の正極活物質粒子及びその製造方法、並びに非水電解質二次電池
US12062785B2 (en) Method of producing a rechargeable high-energy battery having an anionically redox-active composite cathode
EP0864539B1 (en) Process for producing lithium-cobalt oxide
JP2002075366A (ja) リチウム二次電池正極用リチウムマンガン酸化物及びその製造方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20100607

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20100607

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20120914

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20120924

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20121221

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20130104

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130325

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20130415

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130716

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20130805

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20130904

R150 Certificate of patent or registration of utility model

Ref document number: 5362555

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

Free format text: JAPANESE INTERMEDIATE CODE: R150

S531 Written request for registration of change of domicile

Free format text: JAPANESE INTERMEDIATE CODE: R313531

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313113

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250