KR101191154B1 - 리튬이차전지용 금속산화물계 양극활물질의 재처리 및 합성 방법 - Google Patents

리튬이차전지용 금속산화물계 양극활물질의 재처리 및 합성 방법 Download PDF

Info

Publication number
KR101191154B1
KR101191154B1 KR20100092676A KR20100092676A KR101191154B1 KR 101191154 B1 KR101191154 B1 KR 101191154B1 KR 20100092676 A KR20100092676 A KR 20100092676A KR 20100092676 A KR20100092676 A KR 20100092676A KR 101191154 B1 KR101191154 B1 KR 101191154B1
Authority
KR
South Korea
Prior art keywords
active material
component
cathode active
secondary battery
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR20100092676A
Other languages
English (en)
Korean (ko)
Other versions
KR20120030865A (ko
Inventor
정경윤
이화영
조병원
Original Assignee
한국과학기술연구원
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 한국과학기술연구원 filed Critical 한국과학기술연구원
Priority to KR20100092676A priority Critical patent/KR101191154B1/ko
Priority to JP2011007943A priority patent/JP5112526B2/ja
Priority to US13/015,421 priority patent/US8835026B2/en
Publication of KR20120030865A publication Critical patent/KR20120030865A/ko
Application granted granted Critical
Publication of KR101191154B1 publication Critical patent/KR101191154B1/ko
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/54Reclaiming serviceable parts of waste accumulators
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/40Complex oxides containing nickel and at least one other metal element
    • C01G53/42Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • H01M4/0471Processes of manufacture in general involving thermal treatment, e.g. firing, sintering, backing particulate active material, thermal decomposition, pyrolysis
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • H01M4/049Manufacturing of an active layer by chemical means
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/84Recycling of batteries or fuel cells

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
KR20100092676A 2010-09-20 2010-09-20 리튬이차전지용 금속산화물계 양극활물질의 재처리 및 합성 방법 Expired - Fee Related KR101191154B1 (ko)

Priority Applications (3)

Application Number Priority Date Filing Date Title
KR20100092676A KR101191154B1 (ko) 2010-09-20 2010-09-20 리튬이차전지용 금속산화물계 양극활물질의 재처리 및 합성 방법
JP2011007943A JP5112526B2 (ja) 2010-09-20 2011-01-18 リチウム二次電池用金属酸化物系正極活物質の再処理及び合成方法
US13/015,421 US8835026B2 (en) 2010-09-20 2011-01-27 Recovery and synthesis method for metaloxidic cathodic active material for lithium ion secondary battery

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR20100092676A KR101191154B1 (ko) 2010-09-20 2010-09-20 리튬이차전지용 금속산화물계 양극활물질의 재처리 및 합성 방법

Publications (2)

Publication Number Publication Date
KR20120030865A KR20120030865A (ko) 2012-03-29
KR101191154B1 true KR101191154B1 (ko) 2012-10-15

Family

ID=45816901

Family Applications (1)

Application Number Title Priority Date Filing Date
KR20100092676A Expired - Fee Related KR101191154B1 (ko) 2010-09-20 2010-09-20 리튬이차전지용 금속산화물계 양극활물질의 재처리 및 합성 방법

Country Status (3)

Country Link
US (1) US8835026B2 (enExample)
JP (1) JP5112526B2 (enExample)
KR (1) KR101191154B1 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022065721A1 (ko) * 2020-09-28 2022-03-31 주식회사 엘지에너지솔루션 양극 스크랩을 이용한 활물질 재사용 방법
WO2022080657A1 (ko) * 2020-10-16 2022-04-21 주식회사 엘지에너지솔루션 양극 스크랩을 이용한 활물질 재사용 방법

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11955613B2 (en) 2012-04-04 2024-04-09 Worcester Polytechnic Institute Charge material for recycled lithium-ion batteries
KR101294335B1 (ko) 2012-05-25 2013-08-16 한국과학기술연구원 재활용을 통한 리튬 이차전지용 리튬인산철 양극활물질의 제조 방법, 이에 따라 제조된 리튬 이차전지용 리튬인산철 양극활물질, 리튬인산철 양극 및 리튬 이차전지
JP6159228B2 (ja) * 2012-11-07 2017-07-05 株式会社半導体エネルギー研究所 非水系二次電池用正極の製造方法
KR101439427B1 (ko) 2013-03-14 2014-09-11 한국과학기술연구원 리튬이차전지용 올리빈계 양극소재의 재활용 방법, 이에 의하여 제조된 양극소재, 이를 포함하는 리튬이차전지용 양극 및 리튬이차전지
WO2015041381A1 (ko) * 2013-09-17 2015-03-26 국립대학법인 울산과학기술대학교 산학협력단 리튬 이차 전지 및 리튬 이차 전지 시스템
CN103618093A (zh) * 2013-10-31 2014-03-05 中南大学 一种铝电池用铝合金阳极材料热处理方法
JP6312576B2 (ja) * 2014-10-29 2018-04-18 信越化学工業株式会社 リチウム複合酸化物の再生方法、電気化学デバイスの製造方法、並びに、リチウムイオン二次電池の製造方法
JP6294219B2 (ja) * 2014-12-25 2018-03-14 信越化学工業株式会社 リチウムコバルト系複合酸化物の製造方法
JP6374348B2 (ja) * 2015-05-18 2018-08-15 信越化学工業株式会社 リチウムリン系バナジウム複合酸化物炭素複合体、及びその製造方法、リチウムイオン二次電池、並びに、電気化学デバイス
CN107326181B (zh) * 2017-05-26 2018-11-09 金川集团股份有限公司 废旧锂离子电池剥离浸出一步完成的回收方法
CN109921120B (zh) * 2017-12-13 2020-12-22 中国科学院过程工程研究所 一种三元正极材料制备过程中废弃耐火材料回收处理的方法
CN109449434B (zh) * 2018-09-20 2021-08-20 广东佳纳能源科技有限公司 一种利用废旧锂离子电池制备三元锂电池正极材料前驱体的方法
KR102738931B1 (ko) * 2019-05-20 2024-12-04 에스케이이노베이션 주식회사 리튬 전구체 분리 방법 및 리튬 전구체 분리 시스템
KR102742136B1 (ko) 2020-05-29 2024-12-11 주식회사 엘지에너지솔루션 양극 스크랩을 이용한 활물질 재사용 방법
KR102887856B1 (ko) * 2020-08-24 2025-11-17 주식회사 엘지에너지솔루션 양극 스크랩을 이용한 활물질 재사용 방법
CN113151680B (zh) * 2021-02-08 2023-06-16 中国科学院宁波材料技术与工程研究所 一种废旧锂电池回收再利用的方法
CN113522868B (zh) * 2021-06-29 2022-12-13 格林美(湖北)新能源材料有限公司 一种去除正极材料表面残碱的洗涤方法
JP7694599B2 (ja) * 2023-03-29 2025-06-18 トヨタ自動車株式会社 再生材料の製造方法および製造システム
KR102875748B1 (ko) * 2024-11-20 2025-10-27 (주) 에스쓰리알 안전하게 폐리튬일차전지의 리튬을 회수하기 위한 폐리튬일차전지 전처리 방법과 이를 이용한 폐리튬일차전지의 리튬 회수 방법
KR102858723B1 (ko) * 2025-02-04 2025-09-12 주식회사 알디솔루션 암모니아 가스 기반 건식 열처리 방식을 활용한 리튬이온 배터리 재활용 장치 및 방법

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11293357A (ja) * 1998-04-14 1999-10-26 Hiroyuki Nakazawa コバルト化合物の選択的回収方法
JP2005194106A (ja) 2003-12-12 2005-07-21 Nippon Chem Ind Co Ltd リチウムマンガンニッケル複合酸化物の製造方法
JP2007012629A (ja) * 2000-07-27 2007-01-18 Matsushita Electric Ind Co Ltd 正極活物質およびこれを含む非水電解質二次電池
KR100975317B1 (ko) 2009-11-20 2010-08-12 한국지질자원연구원 망간 및 아연을 함유하는 폐전지로부터의 황산망간 및 황산아연 제조방법

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3935594B2 (ja) * 1997-03-14 2007-06-27 三菱重工業株式会社 非水溶媒系電池の処理方法
JP3625638B2 (ja) * 1998-03-17 2005-03-02 株式会社東芝 廃電池の処理装置
CA2319285A1 (en) * 2000-09-13 2002-03-13 Hydro-Quebec A method for neutralizing and recycling spent lithium metal polymer rechargeable batteries
JP4767798B2 (ja) * 2006-09-05 2011-09-07 住友大阪セメント株式会社 電極材料の製造方法、リチウムの回収方法、正極材料及び電極並びに電池
KR101069807B1 (ko) * 2010-04-14 2011-10-04 한국과학기술연구원 리튬전지 양극활물질로부터 코발트를 전해 환원 추출하는 방법

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11293357A (ja) * 1998-04-14 1999-10-26 Hiroyuki Nakazawa コバルト化合物の選択的回収方法
JP2007012629A (ja) * 2000-07-27 2007-01-18 Matsushita Electric Ind Co Ltd 正極活物質およびこれを含む非水電解質二次電池
JP2005194106A (ja) 2003-12-12 2005-07-21 Nippon Chem Ind Co Ltd リチウムマンガンニッケル複合酸化物の製造方法
KR100975317B1 (ko) 2009-11-20 2010-08-12 한국지질자원연구원 망간 및 아연을 함유하는 폐전지로부터의 황산망간 및 황산아연 제조방법

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022065721A1 (ko) * 2020-09-28 2022-03-31 주식회사 엘지에너지솔루션 양극 스크랩을 이용한 활물질 재사용 방법
WO2022080657A1 (ko) * 2020-10-16 2022-04-21 주식회사 엘지에너지솔루션 양극 스크랩을 이용한 활물질 재사용 방법

Also Published As

Publication number Publication date
KR20120030865A (ko) 2012-03-29
JP5112526B2 (ja) 2013-01-09
US8835026B2 (en) 2014-09-16
JP2012064557A (ja) 2012-03-29
US20120068107A1 (en) 2012-03-22

Similar Documents

Publication Publication Date Title
KR101191154B1 (ko) 리튬이차전지용 금속산화물계 양극활물질의 재처리 및 합성 방법
JP2012064557A5 (enExample)
CN107196007B (zh) 一种锂电池回收再利用方法
KR101392616B1 (ko) 리튬 이온 전지의 폐 양극재를 이용한 전구체 원료의 재생 방법, 그 방법에 의해 재생된 원료를 사용하여 제조한 전구체, 양극재 및 리튬 이온 전지
KR102064668B1 (ko) 리튬이온이차전지의 폐 양극재로부터 양극활물질 전구체용 원료를 재생하는 방법, 이에 의하여 재생된 양극활물질 전구체용 원료, 양극활물질 전구체, 양극활물질, 양극 및 리튬이온이차전지
JP2021504885A (ja) 様々な金属の水酸化物および酸化物ならびにそれらの誘導体の調製プロセス
ES3010710A2 (es) Metodo para recuperar material de bateria de litio de desecho
KR20200123659A (ko) 폐양극활물질분말로부터 전구체 제조를 위한 혼합금속화합물의 제조방법
CN111471856A (zh) 红土镍矿一步酸浸并联产磷酸铁锂正极活性材料的方法
KR101835038B1 (ko) 수산화리튬의 제조 방법
CN115472948B (zh) 一种利用废旧锰酸锂再生钠电正极材料的方法
KR20220145818A (ko) 배터리 레벨 Ni-Co-Mn 혼합액 및 배터리 레벨 Mn 용액의 제조방법
CN112375910A (zh) 废动力电池粉的回收处理方法
EP3951979B1 (en) Method for separating transition metal from waste cathode material
KR102710458B1 (ko) 리튬 함유 폐액으로부터 리튬 성분을 회수하는 방법
EP4527797A1 (en) Method for producing high-purity lithium phosphate from waste saggar
KR101316620B1 (ko) 고순도 나노입자 이산화망간 제조방법
CN113611857B (zh) 一种利用含锰钴镍废渣制备三元正极材料的方法
CN118771415A (zh) 一种带有镍钴锰三元正极材料的废旧锂电池回收工艺
KR20240078291A (ko) 폐배터리로부터 황산리튬을 생산하는 방법
CN112259820A (zh) 一种利用废旧锂电池制备核壳型三元正极材料的方法
EP4538402A1 (en) All-in-one nickel smelting method for recovering nickel metal from raw materials containing nickel
EP4538400A1 (en) All-in-one nickel smelting method for nickel oxide recovery from raw materials containing nickel
US20250070290A1 (en) Impurity control in lithium-ion battery recycling
KR102873789B1 (ko) 젖산을 이용한 폐이차전지 양극활물질의 친환경적 재생방법

Legal Events

Date Code Title Description
A201 Request for examination
PA0109 Patent application

St.27 status event code: A-0-1-A10-A12-nap-PA0109

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

D13-X000 Search requested

St.27 status event code: A-1-2-D10-D13-srh-X000

D14-X000 Search report completed

St.27 status event code: A-1-2-D10-D14-srh-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U11-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R13-asn-PN2301

St.27 status event code: A-5-5-R10-R11-asn-PN2301

FPAY Annual fee payment

Payment date: 20151002

Year of fee payment: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

FPAY Annual fee payment

Payment date: 20161004

Year of fee payment: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20171010

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20171010

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R13-asn-PN2301

St.27 status event code: A-5-5-R10-R11-asn-PN2301