KR101080442B1 - 친수화 블로킹된 폴리이소시아네이트 - Google Patents

친수화 블로킹된 폴리이소시아네이트 Download PDF

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Publication number
KR101080442B1
KR101080442B1 KR1020057011419A KR20057011419A KR101080442B1 KR 101080442 B1 KR101080442 B1 KR 101080442B1 KR 1020057011419 A KR1020057011419 A KR 1020057011419A KR 20057011419 A KR20057011419 A KR 20057011419A KR 101080442 B1 KR101080442 B1 KR 101080442B1
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South Korea
Prior art keywords
polyisocyanate
weight
ionic
polyisocyanate according
coating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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KR1020057011419A
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English (en)
Korean (ko)
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KR20050085792A (ko
Inventor
토르스텐 리쉐
크리스토프 귀르틀러
카린 나우요크스
토마스 펠러
Original Assignee
바이엘 머티리얼사이언스 아게
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Publication of KR101080442B1 publication Critical patent/KR101080442B1/ko
Anticipated expiration legal-status Critical
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/80—Masked polyisocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/80—Masked polyisocyanates
    • C08G18/8061—Masked polyisocyanates masked with compounds having only one group containing active hydrogen
    • C08G18/8093—Compounds containing active methylene groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
    • C08G18/0819—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups
    • C08G18/0823—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups containing carboxylate salt groups or groups forming them
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
    • C08G18/0819—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups
    • C08G18/0828—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups containing sulfonate groups or groups forming them
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2815—Monohydroxy compounds
    • C08G18/283—Compounds containing ether groups, e.g. oxyalkylated monohydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3819—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen
    • C08G18/3821—Carboxylic acids; Esters thereof with monohydroxyl compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3819—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen
    • C08G18/3823—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen containing -N-C=O groups
    • C08G18/3831—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen containing -N-C=O groups containing urethane groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/703—Isocyanates or isothiocyanates transformed in a latent form by physical means
    • C08G18/705—Dispersions of isocyanates or isothiocyanates in a liquid medium
    • C08G18/706—Dispersions of isocyanates or isothiocyanates in a liquid medium the liquid medium being water
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04—Polyurethanes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Paints Or Removers (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020057011419A 2002-12-20 2003-12-06 친수화 블로킹된 폴리이소시아네이트 Expired - Fee Related KR101080442B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10260298.0 2002-12-20
DE10260298A DE10260298A1 (de) 2002-12-20 2002-12-20 Hydrophilierte blockierte Polysocyanate

Publications (2)

Publication Number Publication Date
KR20050085792A KR20050085792A (ko) 2005-08-29
KR101080442B1 true KR101080442B1 (ko) 2011-11-04

Family

ID=32404131

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020057011419A Expired - Fee Related KR101080442B1 (ko) 2002-12-20 2003-12-06 친수화 블로킹된 폴리이소시아네이트

Country Status (14)

Country Link
US (1) US7220814B2 (enExample)
EP (1) EP1581576B1 (enExample)
JP (1) JP4538327B2 (enExample)
KR (1) KR101080442B1 (enExample)
CN (1) CN1326903C (enExample)
AT (1) ATE471347T1 (enExample)
AU (1) AU2003292202A1 (enExample)
BR (1) BR0317429A (enExample)
CA (1) CA2510554C (enExample)
DE (2) DE10260298A1 (enExample)
ES (1) ES2345883T3 (enExample)
MX (1) MXPA05006531A (enExample)
RU (1) RU2345097C2 (enExample)
WO (1) WO2004058847A1 (enExample)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10260269A1 (de) * 2002-12-20 2004-07-01 Bayer Ag Neue Dual Cure-Systeme
DE102005048823A1 (de) * 2005-10-10 2007-04-12 Bayer Materialscience Ag Reaktivsysteme, deren Herstellung und Verwendung
JP5399625B2 (ja) * 2007-11-13 2014-01-29 日東電工株式会社 複合フィルム
SI2218740T1 (sl) * 2009-02-13 2014-03-31 Bayer Materialscience Llc ÄŚistilni poliuretanski premazi na vodni osnovi
US8940853B2 (en) * 2011-03-16 2015-01-27 Asahi Kasei Chemicals Corporation Cationic blocked polyisocyanate and aqueous composition comprising the same
EP2971416A2 (en) 2013-03-15 2016-01-20 Spectrum Brands, Inc. Wireless lockset with integrated antenna, touch activation, and light communication method
CN105452320B (zh) * 2013-08-23 2019-02-26 三井化学株式会社 封端异氰酸酯、涂料组合物、粘接剂组合物和物品
CN104448232B (zh) * 2013-09-13 2017-12-15 万华化学集团股份有限公司 一种氨基磺酸改性的多异氰酸酯及其制备方法和用途
JP2015102636A (ja) * 2013-11-22 2015-06-04 富士フイルム株式会社 偏光子保護フィルム、偏光板及び画像表示装置
JP6226762B2 (ja) * 2014-01-31 2017-11-08 富士フイルム株式会社 光学用ポリエステルフィルム、偏光板、画像表示装置、光学用ポリエステルフィルムの製造方法、および易接着層用組成物
RU2713424C1 (ru) 2016-06-03 2020-02-05 ХАНТСМЭН ИНТЕРНЭШНЛ ЭлЭлСи Композиция блокированного изоцианата
CN108264622B (zh) * 2016-12-30 2020-06-19 比亚迪股份有限公司 水性聚氨酯及其制备中间体和制备方法
US10858474B2 (en) 2017-01-31 2020-12-08 Hewlett-Packard Development Company, L.P. Reactive polyurethane dispersions
WO2018143922A1 (en) 2017-01-31 2018-08-09 Hewlett-Packard Development Company, L.P. Reactive polyurethane dispersions
US10640599B2 (en) 2017-01-31 2020-05-05 Hewlett-Packard Development Company, L.P. Reactive polyurethane dispersions
EP3507318B1 (en) 2017-01-31 2022-11-09 Hewlett-Packard Development Company, L.P. Reactive polyurethane dispersions
CN106565928A (zh) * 2017-02-23 2017-04-19 北京理工大学 一种混合亲水聚异氰酸酯固化剂
CN107236114B (zh) * 2017-06-15 2021-01-29 盐城工学院 一种含纳米二氧化硅结构的水性封闭型聚异氰酸酯交联剂及其制备方法
EP3560975B2 (de) 2018-04-25 2023-12-06 Covestro Intellectual Property GmbH & Co. KG Ionisch hydrophilierte polyisocyanate und antioxidantien
ES2884214T3 (es) 2018-04-25 2021-12-10 Covestro Deutschland Ag Poliisocianatos hidrofilizados iónicamente y secuestradores de radicales y/o descomponedores de peróxidos
EP3560974A1 (de) * 2018-04-25 2019-10-30 Covestro Deutschland AG Ionisch hydrophilierte polyisocyanate, wassergehalt

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5350825A (en) 1992-12-02 1994-09-27 Bayer Aktiengesellschaft At least partially blocked organic polyisocyanates, a process for their preparation and their use in coating compositions
US6025433A (en) 1995-12-20 2000-02-15 Basf Coatings Ag Thermosetting paint composition

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4108814A (en) 1974-09-28 1978-08-22 Bayer Aktiengesellschaft Aqueous polyurethane dispersions from solvent-free prepolymers using sulfonate diols
DE2456469C2 (de) 1974-11-29 1983-01-13 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von in Wasser löslichen bzw. dispergierbaren blockierten Polyisocyanaten und ihre Verwendung als Beschichtungsmittel
DE2853937A1 (de) 1978-12-14 1980-07-03 Bayer Ag Verfahren zur herstellung von wasserdispergierbaren oder -loeslichen blockierten polyisocyanaten, die nach dem verfahren erhaeltlichen blockierten polyisocyanate, sowie diese blockierte polyisocyanate als isocyanatkomponente enthaltende lackbindemittel
GB2290793B (en) * 1994-06-20 1998-05-06 Cray Valley Ltd Powder coating compositions
JP3431285B2 (ja) * 1994-07-13 2003-07-28 旭化成株式会社 水性ブロックポリイソシアナート組成物及びそれを含む水性塗料組成物
JP3947260B2 (ja) * 1997-02-19 2007-07-18 旭化成ケミカルズ株式会社 水性ブロックポリイソシアネート組成物
DE19750186A1 (de) 1997-11-13 1999-05-20 Bayer Ag Hydrophilierungsmittel, ein Verfahren zu dessen Herstellung sowie dessen Verwendung als Dispergator für wäßrige Polyurethan-Dispersionen
DE19813352A1 (de) 1998-03-26 1999-09-30 Bayer Ag Malonesterblockierte Polyisocyanate mit Formaldehyd gegen Thermovergilbung
RU2148061C1 (ru) * 1998-04-09 2000-04-27 Институт проблем химической физики РАН Блокированные полиизоцианаты, способ их получения, применение их в качестве компонента защитных и декоративных покрытий и магнитная регистрирующая среда на основе блокированных полиизоцианатов
DE10024624A1 (de) 2000-05-18 2001-11-22 Bayer Ag Modifizierte Polyisocyanate
JP3884277B2 (ja) * 2001-02-21 2007-02-21 関西ペイント株式会社 ブロックイソシアネート基含有樹脂組成物及びこれを含む熱硬化性組成物
DE10132016A1 (de) * 2001-07-03 2003-01-16 Bayer Ag Cyclische Ketone als Blockierungsmittel
NZ530396A (en) * 2001-07-03 2005-07-29 Bayer Ag Cyclic ketones as blocking agents
DE10226926A1 (de) * 2002-06-17 2004-02-05 Bayer Ag Blockierte Polyisocyanate
DE10260270A1 (de) * 2002-12-20 2004-07-01 Bayer Ag Hydrophile Polyurethan-Polyharnstoff-Dispersion
DE10260299A1 (de) * 2002-12-20 2004-07-01 Bayer Ag Reaktivsysteme, deren Herstellung und deren Verwendung

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5350825A (en) 1992-12-02 1994-09-27 Bayer Aktiengesellschaft At least partially blocked organic polyisocyanates, a process for their preparation and their use in coating compositions
US6025433A (en) 1995-12-20 2000-02-15 Basf Coatings Ag Thermosetting paint composition

Also Published As

Publication number Publication date
RU2005122823A (ru) 2006-01-20
BR0317429A (pt) 2005-11-16
US7220814B2 (en) 2007-05-22
CN1326903C (zh) 2007-07-18
US20040138403A1 (en) 2004-07-15
CA2510554A1 (en) 2004-07-15
ATE471347T1 (de) 2010-07-15
EP1581576A1 (de) 2005-10-05
MXPA05006531A (es) 2005-08-26
EP1581576B1 (de) 2010-06-16
KR20050085792A (ko) 2005-08-29
JP2006510784A (ja) 2006-03-30
CN1729223A (zh) 2006-02-01
ES2345883T3 (es) 2010-10-05
CA2510554C (en) 2011-09-20
RU2345097C2 (ru) 2009-01-27
AU2003292202A1 (en) 2004-07-22
JP4538327B2 (ja) 2010-09-08
WO2004058847A1 (de) 2004-07-15
DE50312819D1 (en) 2010-07-29
DE10260298A1 (de) 2004-07-01
HK1088024A1 (en) 2006-10-27

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St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20141101

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20141101

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000