KR100996479B1 - 무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계 - Google Patents

무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계 Download PDF

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Publication number
KR100996479B1
KR100996479B1 KR1020057022008A KR20057022008A KR100996479B1 KR 100996479 B1 KR100996479 B1 KR 100996479B1 KR 1020057022008 A KR1020057022008 A KR 1020057022008A KR 20057022008 A KR20057022008 A KR 20057022008A KR 100996479 B1 KR100996479 B1 KR 100996479B1
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weight
catalyst
surface area
bet surface
titanium dioxide
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KR20060015268A (ko
Inventor
제바스티안 슈토르크
위르겐 췰케
자무엘 네토
프랑크 로조브스키
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바스프 에스이
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20—Vanadium, niobium or tantalum
    • B01J23/22—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/612—Surface area less than 10 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)
  • Furan Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020057022008A 2003-05-23 2004-05-15 무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계 Expired - Fee Related KR100996479B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10323818.2 2003-05-23
DE10323818A DE10323818A1 (de) 2003-05-23 2003-05-23 Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid

Publications (2)

Publication Number Publication Date
KR20060015268A KR20060015268A (ko) 2006-02-16
KR100996479B1 true KR100996479B1 (ko) 2010-11-24

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KR1020057022008A Expired - Fee Related KR100996479B1 (ko) 2003-05-23 2004-05-15 무수 프탈산 제조를 위한 3 층 또는 4 층 촉매계

Country Status (15)

Country Link
US (2) US7687425B2 (https=)
EP (1) EP1628763B1 (https=)
JP (1) JP4829113B2 (https=)
KR (1) KR100996479B1 (https=)
CN (1) CN1795049B (https=)
AT (1) ATE372827T1 (https=)
BR (1) BRPI0410472B1 (https=)
DE (2) DE10323818A1 (https=)
ES (1) ES2290712T3 (https=)
MX (1) MXPA05012454A (https=)
PL (1) PL1628763T3 (https=)
RU (1) RU2005140086A (https=)
TW (1) TWI343834B (https=)
WO (1) WO2004103561A1 (https=)
ZA (1) ZA200510369B (https=)

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DE10334132A1 (de) 2003-07-25 2005-04-07 Basf Ag Silber, Vanadium und ein Promotormetall enthaltendes Multimetalloxid und dessen Verwendung
DE102004026472A1 (de) * 2004-05-29 2005-12-22 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
US8097558B2 (en) * 2004-05-29 2012-01-17 Sud-Chemie Ag Catalyst and method for producing phthalic anhydride
JP5174462B2 (ja) * 2004-11-18 2013-04-03 ビーエーエスエフ ソシエタス・ヨーロピア 触媒を製造するための二酸化チタン混合物の使用
CN101090769B (zh) * 2005-03-02 2011-09-28 苏德-化学股份公司 用于制备邻苯二甲酸酐的多层催化剂的生产方法
DE102005009473A1 (de) * 2005-03-02 2006-09-07 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
US7968491B2 (en) * 2005-05-22 2011-06-28 Sud-Chemie Ag Multi-layer catalyst for producing phthalic anhydride
DE102005026360A1 (de) * 2005-06-07 2006-12-28 Basf Ag Verfahren zur Präformierung von Oxidationskatalysatoren
US20090163726A1 (en) * 2006-05-19 2009-06-25 Basf Se Catalyst system for preparing carboxylic acids and/or carboxylic anhydrides
EP1860091A1 (de) * 2006-05-23 2007-11-28 Süd-Chemie Ag Katalysator enthaltend Titandioxid, insbesondere zur Herstellung von Phthalsäurenanhydrid
JP2009541245A (ja) * 2006-06-20 2009-11-26 ビーエーエスエフ ソシエタス・ヨーロピア 触媒系及びカルボン酸及び／又は無水カルボン酸の製造法
BRPI0720411A2 (pt) 2006-12-21 2013-12-31 Basf Se Processo para oxidação em fase gasosa, e, sistema catalisador para a realização de processos de oxidação em fase gasosa
US8311837B1 (en) * 2008-06-13 2012-11-13 West Corporation Mobile voice self service system
DE102009041960A1 (de) 2009-09-17 2011-04-07 Süd-Chemie AG Verfahren zur Herstellung einer Katalysatoranordnung für die Herstellung von Phthalsäureanhydrid
DE102009049173A1 (de) 2009-10-13 2011-04-21 Süd-Chemie AG Reaktoranordnung zur katalytischen Gasphasenoxidation
EP2501472A1 (de) * 2009-11-20 2012-09-26 Basf Se Mehrlagenkatalysator zur herstellung von carbonsäuren und/oder carbonsäureanhydriden mit vanadiumantimonat in wenigstens einer katalysatorlage und verfahren zur herstellung von phthalsäureanhydrid mit niedriger hotspottemperatur
DE102010006854A1 (de) 2010-02-04 2011-08-04 Süd-Chemie AG, 80333 Verfahren zur Gasphasenoxidation von Kohlenwasserstoffen
DE102010012090A1 (de) 2010-03-19 2011-11-17 Süd-Chemie AG Verfahren zur katalytischen Gasphasenoxidation von Kohlenwasserstoffen und Katalysereaktionsvorrichtung
US20110230668A1 (en) * 2010-03-19 2011-09-22 Basf Se Catalyst for gas phase oxidations based on low-sulfur and low-calcium titanium dioxide
US8901320B2 (en) 2010-04-13 2014-12-02 Basf Se Process for controlling a gas phase oxidation reactor for preparation of phthalic anhydride
US8859459B2 (en) 2010-06-30 2014-10-14 Basf Se Multilayer catalyst for preparing phthalic anhydride and process for preparing phthalic anhydride
DE112011102205A5 (de) * 2010-06-30 2013-06-27 Basf Se Mehrlagenkatalysator zur Herstellung von Phthalsäureanhydrid und Verfahren zur Herstellung von Phthalsäureanhydrid
US9212157B2 (en) 2010-07-30 2015-12-15 Basf Se Catalyst for the oxidation of o-xylene and/or naphthalene to phthalic anhydride
BR112013001388A2 (pt) * 2010-07-30 2016-05-24 Basf Se catalisador para a oxidação de o-xileno e/ou naftaleno para anidrido ftálico, e, processo para a oxidação em fase gasosa
US9029289B2 (en) 2012-07-16 2015-05-12 Basf Se Catalyst for preparing carboxylic acids and/or carboxylic anhydrides
DE102013000654B4 (de) * 2013-01-16 2020-10-15 Clariant International Ltd. Verfahren zur Optimierung der Aktivität eines Phthalsäureanhydrid-Katalysators
BR112015032335A2 (pt) 2013-06-26 2017-07-25 Basf Se processo para preparar anidrido ftálico
US9656983B2 (en) 2013-06-26 2017-05-23 Basf Se Process for starting up a gas phase oxidation reactor
BR112015031535B1 (pt) 2014-04-24 2021-09-21 Clariant International Ltd. Arranjo de catalisadores com fração de vazios otimizada, seu uso e processo de preparação de anidrido de ácido ftálico
EP3047904A1 (en) * 2015-01-22 2016-07-27 Basf Se Catalyst system for oxidation of o-xylene and/or naphthalene to phthalic anhydride
IT202100021746A1 (it) * 2021-08-11 2023-02-11 Polynt S P A Letto catalitico multistrato per la produzione di anidride ftalica.

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Also Published As

Publication number Publication date
WO2004103561A1 (de) 2004-12-02
RU2005140086A (ru) 2006-08-10
MXPA05012454A (es) 2006-02-22
CN1795049B (zh) 2012-02-01
ATE372827T1 (de) 2007-09-15
DE502004004958D1 (de) 2007-10-25
KR20060015268A (ko) 2006-02-16
BRPI0410472A (pt) 2006-05-30
US7687425B2 (en) 2010-03-30
JP2007533426A (ja) 2007-11-22
EP1628763B1 (de) 2007-09-12
DE10323818A1 (de) 2004-12-09
TW200505566A (en) 2005-02-16
TWI343834B (en) 2011-06-21
US20060276661A1 (en) 2006-12-07
PL1628763T3 (pl) 2008-02-29
BRPI0410472B1 (pt) 2014-01-28
JP4829113B2 (ja) 2011-12-07
EP1628763A1 (de) 2006-03-01
ZA200510369B (en) 2007-04-25
CN1795049A (zh) 2006-06-28
US20100210857A1 (en) 2010-08-19
ES2290712T3 (es) 2008-02-16
US7985705B2 (en) 2011-07-26

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St.27 status event code: A-4-4-P10-P22-nap-X000

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000