RU2005140086A - Трех- или четырехслойные катализаторные системы для получения ангидрида фталевой кислоты - Google Patents

Трех- или четырехслойные катализаторные системы для получения ангидрида фталевой кислоты Download PDF

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Publication number
RU2005140086A
RU2005140086A RU2005140086/04A RU2005140086A RU2005140086A RU 2005140086 A RU2005140086 A RU 2005140086A RU 2005140086/04 A RU2005140086/04 A RU 2005140086/04A RU 2005140086 A RU2005140086 A RU 2005140086A RU 2005140086 A RU2005140086 A RU 2005140086A
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RU
Russia
Prior art keywords
catalyst
layer
bet surface
calculated
titanium dioxide
Prior art date
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RU2005140086/04A
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English (en)
Russian (ru)
Inventor
Себастиан ШТОРК (DE)
Себастиан ШТОРК
Юрген ЦЮЛЬКЕ (DE)
Юрген Цюльке
Самюэль НЕТО (DE)
Самюэль НЕТО
Франк РОЗОВСКИ (DE)
Франк РОЗОВСКИ
Original Assignee
БАСФ Акциенгезельшафт (DE)
Басф Акциенгезельшафт
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Publication of RU2005140086A publication Critical patent/RU2005140086A/ru

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002Mixed oxides other than spinels, e.g. perovskite
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20Vanadium, niobium or tantalum
    • B01J23/22Vanadium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14Phosphorus; Compounds thereof
    • B01J27/186Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198Vanadium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/19Catalysts containing parts with different compositions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/60Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/60Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61Surface area
    • B01J35/612Surface area less than 10 m2/g
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/60Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61Surface area
    • B01J35/61310-100 m2/g
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00Constitutive chemical elements of heterogeneous catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)
  • Furan Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
RU2005140086/04A 2003-05-23 2004-05-15 Трех- или четырехслойные катализаторные системы для получения ангидрида фталевой кислоты RU2005140086A (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10323818.2 2003-05-23
DE10323818A DE10323818A1 (de) 2003-05-23 2003-05-23 Katalysatorsysteme zur Herstellung von Phthalsäureanhydrid

Publications (1)

Publication Number Publication Date
RU2005140086A true RU2005140086A (ru) 2006-08-10

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
RU2005140086/04A RU2005140086A (ru) 2003-05-23 2004-05-15 Трех- или четырехслойные катализаторные системы для получения ангидрида фталевой кислоты

Country Status (15)

Country Link
US (2) US7687425B2 (https=)
EP (1) EP1628763B1 (https=)
JP (1) JP4829113B2 (https=)
KR (1) KR100996479B1 (https=)
CN (1) CN1795049B (https=)
AT (1) ATE372827T1 (https=)
BR (1) BRPI0410472B1 (https=)
DE (2) DE10323818A1 (https=)
ES (1) ES2290712T3 (https=)
MX (1) MXPA05012454A (https=)
PL (1) PL1628763T3 (https=)
RU (1) RU2005140086A (https=)
TW (1) TWI343834B (https=)
WO (1) WO2004103561A1 (https=)
ZA (1) ZA200510369B (https=)

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DE10334132A1 (de) 2003-07-25 2005-04-07 Basf Ag Silber, Vanadium und ein Promotormetall enthaltendes Multimetalloxid und dessen Verwendung
DE102004026472A1 (de) * 2004-05-29 2005-12-22 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
US8097558B2 (en) * 2004-05-29 2012-01-17 Sud-Chemie Ag Catalyst and method for producing phthalic anhydride
JP5174462B2 (ja) * 2004-11-18 2013-04-03 ビーエーエスエフ ソシエタス・ヨーロピア 触媒を製造するための二酸化チタン混合物の使用
CN101090769B (zh) * 2005-03-02 2011-09-28 苏德-化学股份公司 用于制备邻苯二甲酸酐的多层催化剂的生产方法
DE102005009473A1 (de) * 2005-03-02 2006-09-07 Süd-Chemie AG Mehrlagen-Katalysator zur Herstellung von Phthalsäureanhydrid
US7968491B2 (en) * 2005-05-22 2011-06-28 Sud-Chemie Ag Multi-layer catalyst for producing phthalic anhydride
DE102005026360A1 (de) * 2005-06-07 2006-12-28 Basf Ag Verfahren zur Präformierung von Oxidationskatalysatoren
US20090163726A1 (en) * 2006-05-19 2009-06-25 Basf Se Catalyst system for preparing carboxylic acids and/or carboxylic anhydrides
EP1860091A1 (de) * 2006-05-23 2007-11-28 Süd-Chemie Ag Katalysator enthaltend Titandioxid, insbesondere zur Herstellung von Phthalsäurenanhydrid
JP2009541245A (ja) * 2006-06-20 2009-11-26 ビーエーエスエフ ソシエタス・ヨーロピア 触媒系及びカルボン酸及び/又は無水カルボン酸の製造法
BRPI0720411A2 (pt) 2006-12-21 2013-12-31 Basf Se Processo para oxidação em fase gasosa, e, sistema catalisador para a realização de processos de oxidação em fase gasosa
US8311837B1 (en) * 2008-06-13 2012-11-13 West Corporation Mobile voice self service system
DE102009041960A1 (de) 2009-09-17 2011-04-07 Süd-Chemie AG Verfahren zur Herstellung einer Katalysatoranordnung für die Herstellung von Phthalsäureanhydrid
DE102009049173A1 (de) 2009-10-13 2011-04-21 Süd-Chemie AG Reaktoranordnung zur katalytischen Gasphasenoxidation
EP2501472A1 (de) * 2009-11-20 2012-09-26 Basf Se Mehrlagenkatalysator zur herstellung von carbonsäuren und/oder carbonsäureanhydriden mit vanadiumantimonat in wenigstens einer katalysatorlage und verfahren zur herstellung von phthalsäureanhydrid mit niedriger hotspottemperatur
DE102010006854A1 (de) 2010-02-04 2011-08-04 Süd-Chemie AG, 80333 Verfahren zur Gasphasenoxidation von Kohlenwasserstoffen
DE102010012090A1 (de) 2010-03-19 2011-11-17 Süd-Chemie AG Verfahren zur katalytischen Gasphasenoxidation von Kohlenwasserstoffen und Katalysereaktionsvorrichtung
US20110230668A1 (en) * 2010-03-19 2011-09-22 Basf Se Catalyst for gas phase oxidations based on low-sulfur and low-calcium titanium dioxide
US8901320B2 (en) 2010-04-13 2014-12-02 Basf Se Process for controlling a gas phase oxidation reactor for preparation of phthalic anhydride
US8859459B2 (en) 2010-06-30 2014-10-14 Basf Se Multilayer catalyst for preparing phthalic anhydride and process for preparing phthalic anhydride
DE112011102205A5 (de) * 2010-06-30 2013-06-27 Basf Se Mehrlagenkatalysator zur Herstellung von Phthalsäureanhydrid und Verfahren zur Herstellung von Phthalsäureanhydrid
US9212157B2 (en) 2010-07-30 2015-12-15 Basf Se Catalyst for the oxidation of o-xylene and/or naphthalene to phthalic anhydride
BR112013001388A2 (pt) * 2010-07-30 2016-05-24 Basf Se catalisador para a oxidação de o-xileno e/ou naftaleno para anidrido ftálico, e, processo para a oxidação em fase gasosa
US9029289B2 (en) 2012-07-16 2015-05-12 Basf Se Catalyst for preparing carboxylic acids and/or carboxylic anhydrides
DE102013000654B4 (de) * 2013-01-16 2020-10-15 Clariant International Ltd. Verfahren zur Optimierung der Aktivität eines Phthalsäureanhydrid-Katalysators
BR112015032335A2 (pt) 2013-06-26 2017-07-25 Basf Se processo para preparar anidrido ftálico
US9656983B2 (en) 2013-06-26 2017-05-23 Basf Se Process for starting up a gas phase oxidation reactor
BR112015031535B1 (pt) 2014-04-24 2021-09-21 Clariant International Ltd. Arranjo de catalisadores com fração de vazios otimizada, seu uso e processo de preparação de anidrido de ácido ftálico
EP3047904A1 (en) * 2015-01-22 2016-07-27 Basf Se Catalyst system for oxidation of o-xylene and/or naphthalene to phthalic anhydride
IT202100021746A1 (it) * 2021-08-11 2023-02-11 Polynt S P A Letto catalitico multistrato per la produzione di anidride ftalica.

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Also Published As

Publication number Publication date
WO2004103561A1 (de) 2004-12-02
MXPA05012454A (es) 2006-02-22
CN1795049B (zh) 2012-02-01
ATE372827T1 (de) 2007-09-15
DE502004004958D1 (de) 2007-10-25
KR20060015268A (ko) 2006-02-16
BRPI0410472A (pt) 2006-05-30
US7687425B2 (en) 2010-03-30
JP2007533426A (ja) 2007-11-22
EP1628763B1 (de) 2007-09-12
DE10323818A1 (de) 2004-12-09
TW200505566A (en) 2005-02-16
TWI343834B (en) 2011-06-21
US20060276661A1 (en) 2006-12-07
PL1628763T3 (pl) 2008-02-29
BRPI0410472B1 (pt) 2014-01-28
JP4829113B2 (ja) 2011-12-07
EP1628763A1 (de) 2006-03-01
ZA200510369B (en) 2007-04-25
CN1795049A (zh) 2006-06-28
US20100210857A1 (en) 2010-08-19
ES2290712T3 (es) 2008-02-16
KR100996479B1 (ko) 2010-11-24
US7985705B2 (en) 2011-07-26

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Effective date: 20081217