KR100936420B1 - 포스겐을 제조하기 위한 반응기 및 방법 - Google Patents

포스겐을 제조하기 위한 반응기 및 방법 Download PDF

Info

Publication number
KR100936420B1
KR100936420B1 KR1020047013342A KR20047013342A KR100936420B1 KR 100936420 B1 KR100936420 B1 KR 100936420B1 KR 1020047013342 A KR1020047013342 A KR 1020047013342A KR 20047013342 A KR20047013342 A KR 20047013342A KR 100936420 B1 KR100936420 B1 KR 100936420B1
Authority
KR
South Korea
Prior art keywords
reactor
catalyst
tube
heat transfer
transfer medium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
KR1020047013342A
Other languages
English (en)
Korean (ko)
Other versions
KR20040087326A (ko
Inventor
올베르트게르하르트
마트케토르스텐
반데르바에렌루크
네베얀스필립
하메네커얀
Original Assignee
바스프 에스이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 바스프 에스이 filed Critical 바스프 에스이
Publication of KR20040087326A publication Critical patent/KR20040087326A/ko
Application granted granted Critical
Publication of KR100936420B1 publication Critical patent/KR100936420B1/ko
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/001—Controlling catalytic processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B01J31/28—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of the platinum group metals, iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B01J12/007—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B01J8/0085—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction promoting uninterrupted fluid flow, e.g. by filtering out particles in front of the catalyst layer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/80—Phosgene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/00044—Temperature measurement
    • B01J2208/00061—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00513—Controlling the temperature using inert heat absorbing solids in the bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/0061—Controlling the level
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00018—Construction aspects
    • B01J2219/0002—Plants assembled from modules joined together
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00777—Baffles attached to the reactor wall horizontal
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S585/00—Chemistry of hydrocarbon compounds
    • Y10S585/919—Apparatus considerations
    • Y10S585/921—Apparatus considerations using recited apparatus structure
    • Y10S585/922—Reactor fluid manipulating device
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S585/00—Chemistry of hydrocarbon compounds
    • Y10S585/919—Apparatus considerations
    • Y10S585/921—Apparatus considerations using recited apparatus structure
    • Y10S585/924—Reactor shape or disposition

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020047013342A 2002-02-27 2003-02-12 포스겐을 제조하기 위한 반응기 및 방법 Expired - Lifetime KR100936420B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10208398.3 2002-02-27
DE10208398 2002-02-27

Publications (2)

Publication Number Publication Date
KR20040087326A KR20040087326A (ko) 2004-10-13
KR100936420B1 true KR100936420B1 (ko) 2010-01-12

Family

ID=27762465

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020047013342A Expired - Lifetime KR100936420B1 (ko) 2002-02-27 2003-02-12 포스겐을 제조하기 위한 반응기 및 방법

Country Status (12)

Country Link
US (2) US8409539B2 (enExample)
EP (1) EP1485195B1 (enExample)
JP (1) JP4424991B2 (enExample)
KR (1) KR100936420B1 (enExample)
CN (1) CN1302842C (enExample)
AT (1) ATE309856T1 (enExample)
AU (1) AU2003208834A1 (enExample)
BR (1) BR0307973A (enExample)
DE (1) DE50301676D1 (enExample)
ES (1) ES2253661T3 (enExample)
IN (1) IN237581B (enExample)
WO (1) WO2003072237A1 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101361002B1 (ko) * 2012-05-21 2014-02-12 고등기술연구원연구조합 간접 가열식 ｖｏｃ 반응기
KR20240103832A (ko) * 2022-12-27 2024-07-04 이화여자대학교 산학협력단 포름산염 제조 반응기, 그의 운전방법 및 상기 반응기를 포함하는 포름산 제조장치

Families Citing this family (74)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100936420B1 (ko) * 2002-02-27 2010-01-12 바스프 에스이 포스겐을 제조하기 위한 반응기 및 방법
JP4145607B2 (ja) * 2002-08-23 2008-09-03 三菱化学株式会社 多管式反応器を用いた気相接触酸化方法
DE102004010383B4 (de) * 2004-03-03 2007-04-12 Man Dwe Gmbh Vorrichtung zur Simulierung des Reaktionsprozesses in und Verfahren zur Optimierung von Mantelrohrreaktoren
DE102004018267B4 (de) * 2004-04-15 2007-05-03 Man Dwe Gmbh Reaktoranordnung zur Durchführung katalytischer Gasphasenreaktionen
DE102004041777A1 (de) 2004-08-28 2006-03-02 Bayer Materialscience Ag Verfahren und Vorrichtung zur Herstellung von Phosgen
DE102005001952A1 (de) * 2005-01-14 2006-07-27 Man Dwe Gmbh Rohrbündelreaktor zur Durchführung exothermer oder endothermer Gasphasenreaktionen
DE102005032663A1 (de) 2005-07-13 2007-01-18 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102005061626A1 (de) * 2005-12-21 2007-06-28 Basf Ag Verfahren der kontinuierlichen heterogen katalysierten partiellen Dehydrierung wenigstens eines zu dehydrierenden Kohlenwasserstoffs
JP4692351B2 (ja) * 2006-03-29 2011-06-01 Ｊｆｅスチール株式会社 空気分離機に付属するアルゴン精製器
US7504533B2 (en) * 2006-04-24 2009-03-17 Bayer Materialscience Llc Process for the production of isocyanates
DE102006022761A1 (de) * 2006-05-16 2007-11-22 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102006023261A1 (de) * 2006-05-18 2007-11-22 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor aus Chlorwasserstoff und Sauerstoff
DE102006023581A1 (de) * 2006-05-19 2007-11-22 Bayer Materialscience Ag Verfahren zur Abtrennung von Chlor aus dem Produktgas eines HCI-Oxidationsprozesses
DE102006024518A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor aus Chlorwasserstoff und Sauerstoff
DE102006024515A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Chlorwasserstoff-Oxidation mit Sauerstoff
DE102006024506A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor aus Chlorwasserstoff und Sauerstoff
DE102006024516A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor aus Chlorwasserstoff und Sauerstoff
DE102006029790A1 (de) * 2006-06-27 2008-01-03 Basf Ag Verfahren der kontinuierlichen heterogen katalysierten partiellen Dehydrierung wenigstens eines zu dehydrierenden Kohlenwasserstoffs
CN101020891B (zh) * 2007-02-07 2011-04-06 秦皇岛领先科技发展有限公司 列管式固定床生物反应器
DE102007020444A1 (de) 2007-04-27 2008-11-06 Bayer Materialscience Ag Verfahren zur Oxidation eines Chlorwasserstoffenthaltenden Gasgemisches
US8343433B2 (en) * 2007-12-18 2013-01-01 Dow Technology Investments Llc Tube reactor
DE102007061477A1 (de) * 2007-12-20 2009-07-02 Man Dwe Gmbh Rohrbündelreaktor
DE102008009761A1 (de) 2008-02-19 2009-08-27 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102008012037A1 (de) 2008-03-01 2009-09-03 Bayer Materialscience Ag Verfahren zur Herstellung von Methylen-diphenyl-diisocyanaten
JP5586624B2 (ja) * 2008-11-26 2014-09-10 ハンツマン・インターナショナル・エルエルシー イソシアネートの製造方法
JP5336828B2 (ja) * 2008-12-02 2013-11-06 三井化学株式会社 塩化カルボニルの製造方法および製造装置、ならびに、ポリイソシアネートの製造方法および製造装置
US9023300B2 (en) 2008-12-16 2015-05-05 Basf Se Reactor and process for preparing phosgene
WO2010076209A1 (de) * 2008-12-16 2010-07-08 Basf Se Reaktor und verfahren zur herstellung von phosgen
KR101778312B1 (ko) 2009-03-11 2017-09-13 바스프 에스이 포스겐의 제조 방법
DE102009032020A1 (de) 2009-07-07 2011-01-13 Bayer Materialscience Ag Verfahren zur Herstellung von Polycarbonat
SG174714A1 (en) 2010-03-30 2011-10-28 Bayer Materialscience Ag Process for preparing diaryl carbonates and polycarbonates
SG174715A1 (en) 2010-03-30 2011-10-28 Bayer Materialscience Ag Process for preparing diaryl carbonates and polycarbonates
CN101893251B (zh) * 2010-07-26 2011-09-21 王兴军 一种锅炉的吸热器
FR2965490B1 (fr) 2010-09-30 2013-01-11 Aet Group Dispositif et procede pour la phosgenation en continu
EP2586767A1 (de) 2011-10-25 2013-05-01 Bayer MaterialScience AG Verfahren zur Herstellung von Diarylcarbonaten und Polycarbonaten
JP6156860B2 (ja) * 2012-04-04 2017-07-05 住友化学株式会社 多管式反応器および多管式反応器の設計方法
PT2872443T (pt) 2012-07-11 2022-08-30 Covestro Intellectual Property Gmbh & Co Kg Dispositivo e método para produzir fosgénio
CN105408249A (zh) 2013-07-26 2016-03-16 沙特基础全球技术有限公司 用于生产高纯光气的方法和装置
EP3024783A1 (en) 2013-07-26 2016-06-01 SABIC Global Technologies B.V. Method and apparatus for producing high purity phosgene
JP5667253B2 (ja) * 2013-08-01 2015-02-12 三井化学株式会社 塩化カルボニルの製造装置およびポリイソシアネートの製造装置
CN104415770B (zh) * 2013-08-26 2016-08-31 万华化学集团股份有限公司 一种制备光气的催化剂及制备光气的方法
WO2015069762A2 (en) * 2013-11-06 2015-05-14 Watt Fuel Cell Corp. Chemical reactor with manifold for management of a flow of gaseous reaction medium thereto
US9358526B2 (en) 2013-11-19 2016-06-07 Emerging Fuels Technology, Inc. Optimized fischer-tropsch catalyst
US9180436B1 (en) 2013-11-19 2015-11-10 Emerging Fuels Technology, Inc. Optimized fischer-tropsch catalyst
KR101859209B1 (ko) * 2014-02-04 2018-06-27 사빅 글로벌 테크놀러지스 비.브이. 카보네이트의 제조 방법
WO2015119981A2 (en) * 2014-02-04 2015-08-13 Sabic Global Technologies B.V. Method for producing carbonates
DE102014202593A1 (de) 2014-02-13 2015-08-13 Siemens Aktiengesellschaft Umwandlung von Metallcarbonat in Metallchlorid
DE102014202591A1 (de) * 2014-02-13 2015-08-13 Siemens Aktiengesellschaft Umwandlung von Metallcarbonat in Metallchlorid
ES2804677T3 (es) 2014-06-11 2021-02-09 Haldor Topsoe As Un proceso para la producción segura de fosgeno
CN104190328B (zh) * 2014-08-12 2017-02-01 中国天辰工程有限公司 一种可用于制取气相氰化氢的反应器
EP3194065B1 (de) 2014-08-20 2019-12-25 Bayer Aktiengesellschaft Verfahren zur phosgenierung von hydroxyl-, thiol-, amino- und/oder formamidgruppen enthaltenden verbindungen
WO2017019961A1 (en) * 2015-07-29 2017-02-02 Primus Green Energy Inc. Two-stage reactor for exothermal and reversible reactions and methods thereof
DE102015013516B4 (de) * 2015-10-20 2018-01-18 Frank Brucker Rohrbündelwärmeübertrager und Fertigungsverfahren für Rohrbündelwärmeübertrager
DE102016100908A1 (de) * 2015-11-06 2017-05-11 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Anlage und Verfahren zur Erzeugung von Fettalkohol
WO2017144584A1 (en) * 2016-02-26 2017-08-31 Shell Internationale Research Maatschappij B.V. Alkane oxidative dehydrogenation (odh)
CN109476563B (zh) * 2016-07-26 2021-09-03 国际壳牌研究有限公司 乙烷的氧化脱氢（odh）
MX2019000807A (es) * 2016-07-26 2019-10-07 Shell Int Research Deshidrogenacion oxidativa (odh) de etano.
EP3421426A1 (de) * 2017-06-29 2019-01-02 Covestro Deutschland AG Energieeffizientes verfahren zur bereitstellung von phosgen-dampf
CN107175056A (zh) * 2017-07-12 2017-09-19 陕西省石油化工研究设计院 高效的液芯光纤光催化反应器
EP3498752A1 (de) 2017-12-18 2019-06-19 Covestro Deutschland AG Verfahren zur herstellung eines polycarbonats unter verwendung eines organischen lösungsmittels auf der grundlage von chlorkohlenwasserstoffen
CN109941965B (zh) * 2019-04-21 2023-05-26 苏州市泰利登净化设备有限公司 一种甲醇制氢设备
KR20220005048A (ko) 2019-04-25 2022-01-12 바스프 에스이 포스겐의 제조 방법
WO2020233921A1 (de) 2019-05-20 2020-11-26 Basf Se Verfahren und reaktor zur herstellung von phosgen
KR20220045150A (ko) 2019-08-08 2022-04-12 코베스트로 인텔렉쳐 프로퍼티 게엠베하 운트 콤파니 카게 폴리카르보네이트를 제조하는 방법
CN112441585B (zh) * 2019-08-30 2022-07-12 万华化学集团股份有限公司 光气合成及盐水蒸发电解一体化处理工艺
EP3862317A1 (de) * 2020-02-06 2021-08-11 Basf Se Verfahren und reaktor zur herstellung von phosgen
WO2021233708A1 (en) 2020-05-20 2021-11-25 Basf Se Process, reaction mixture and catalyst for the production of phosgene
US12491484B2 (en) * 2021-01-15 2025-12-09 CRI, hf Reactor for synthesis of methanol or other products
EP4308281A1 (en) 2021-03-19 2024-01-24 Basf Se Apparatus and method for hotspot detection in a tube bundle reactor
WO2022223203A1 (en) 2021-04-21 2022-10-27 Basf Se Process for preparing phosgene
EP4347102B1 (de) 2021-05-27 2025-02-26 Basf Se Verfahren zur herstellung von phosgen
US20240317590A1 (en) 2021-07-23 2024-09-26 Basf Se Method for producing phosgene
WO2024003247A1 (en) 2022-06-30 2024-01-04 Basf Se Process for producing phosgene
CN115520868B (zh) * 2022-10-25 2023-11-21 摩珈(上海)生物科技有限公司 一种光气的循环制备方法及其装置系统

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3807963A (en) * 1972-03-09 1974-04-30 J Smith Reaction apparatus
US4231959A (en) * 1978-02-15 1980-11-04 Stauffer Chemical Company Phosgene manufacture

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2986454A (en) 1957-07-23 1961-05-30 American Cyanamid Co Tubular catalytic converter
US3518284A (en) * 1967-02-20 1970-06-30 Shell Oil Co Partial oxidation of organic compounds
DE2238851B2 (de) 1972-08-07 1979-08-30 Hoechst Ag, 6000 Frankfurt Verfahren zur Herstellung von Acrolein und/oder Acrylsäure unter Vermeidung von Nachreaktionen bei der katalytischen Oxidation von Propylen und/oder Acrolein
JP4024301B2 (ja) * 1996-02-21 2007-12-19 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ホスゲンの製造方法
US6084125A (en) * 1996-02-27 2000-07-04 Praxair Technology, Inc. Process for producing aliphatic acids using a reactor system having a shell and a tube reactor configuration to force circulation of reaction liquid
EP0998973A1 (de) * 1998-10-27 2000-05-10 Balcke-Dürr Energietechnik GmbH Gekühlter Rohrbündelreaktor
JP2004501759A (ja) * 2000-06-29 2004-01-22 エイチ２ジーイーエヌ・イノベーションズ・インコーポレイテッド 炭化水素の水蒸気改質による改良された水素発生のためのシステム及び炭化水素から水素を製造するための集積化されたケミカル・リアクタ
JP4092090B2 (ja) * 2001-06-26 2008-05-28 株式会社日本触媒 固体粒子充填反応器およびその反応器を用いた接触気相酸化方法
KR100936420B1 (ko) * 2002-02-27 2010-01-12 바스프 에스이 포스겐을 제조하기 위한 반응기 및 방법

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3807963A (en) * 1972-03-09 1974-04-30 J Smith Reaction apparatus
US4231959A (en) * 1978-02-15 1980-11-04 Stauffer Chemical Company Phosgene manufacture

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101361002B1 (ko) * 2012-05-21 2014-02-12 고등기술연구원연구조합 간접 가열식 ｖｏｃ 반응기
KR20240103832A (ko) * 2022-12-27 2024-07-04 이화여자대학교 산학협력단 포름산염 제조 반응기, 그의 운전방법 및 상기 반응기를 포함하는 포름산 제조장치
KR102840405B1 (ko) 2022-12-27 2025-07-29 이화여자대학교 산학협력단 포름산염 제조 반응기, 그의 운전방법 및 상기 반응기를 포함하는 포름산 제조장치

Also Published As

Publication number Publication date
US20130072717A1 (en) 2013-03-21
US8821829B2 (en) 2014-09-02
IN237581B (enExample) 2010-01-01
EP1485195B1 (de) 2005-11-16
JP4424991B2 (ja) 2010-03-03
US20050118088A1 (en) 2005-06-02
IN2004CH01858A (enExample) 2006-06-23
AU2003208834A1 (en) 2003-09-09
CN1302842C (zh) 2007-03-07
ES2253661T3 (es) 2006-06-01
BR0307973A (pt) 2004-12-21
KR20040087326A (ko) 2004-10-13
JP2005525986A (ja) 2005-09-02
ATE309856T1 (de) 2005-12-15
DE50301676D1 (de) 2005-12-22
CN1638856A (zh) 2005-07-13
EP1485195A1 (de) 2004-12-15
US8409539B2 (en) 2013-04-02
WO2003072237A1 (de) 2003-09-04

Similar Documents

Publication Publication Date Title
KR100936420B1 (ko) 포스겐을 제조하기 위한 반응기 및 방법
US6855272B2 (en) Low pressure drop reforming exchanger
CA2046304C (en) Process and apparatus for exothermic reactions
CN1321056C (zh) 通过气相氧化氯化氢制备氯
JP2005525986A5 (enExample)
US8034308B2 (en) Multi-stage multi-tube shell-and-tube reactor
US4714592A (en) Radial flow catalytic reactor including heat exchange apparatus within the bed
EP1839735B1 (en) A transverse tubular heat exchange reactor and a process for catalytic synthesis therein
KR840006444A (ko) 반응 방법 및 반응기
US20090143619A1 (en) Process for the production of phosgene with reduced co emission
KR101057049B1 (ko) 염화수소의 기체상 산화에 의한 염소의 제조 방법
JPH0376976B2 (enExample)
KR20060126736A (ko) 염화수소의 기체상 산화에 의한 염소의 제조 방법
AU603007B2 (en) Catalyst layer-fixed reactor
US3932139A (en) Reactor for the catalytic ammonia synthesis at high temperatures and pressures
JP4386719B2 (ja) 触媒系の試験のための反応器
CA2271367C (en) Horizontal ammonia converter adapted for high activity catalyst
CA1037229A (en) Catalytic reactor for the catalytic reaction of so2 to so3
US20220332587A1 (en) Process and reactor for producing phosgene
WO2006117572A1 (en) Apparatus and process for steam reforming of hydrocarbons
US20240317590A1 (en) Method for producing phosgene
US3567404A (en) Reactor vessel
RU2206384C1 (ru) Реактор для проведения экзотермических каталитических реакций и способ его использования
US20230074789A1 (en) Process and reactor for producing phosgene
US7776285B2 (en) Reactor and process for carrying out endothermic or exothermic catalytic reaction

Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20040826

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
A201 Request for examination
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20071126

Comment text: Request for Examination of Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20090429

Patent event code: PE09021S01D

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

Patent event code: PE07011S01D

Comment text: Decision to Grant Registration

Patent event date: 20091022

GRNT Written decision to grant
PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 20100105

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 20100106

End annual number: 3

Start annual number: 1

PG1601 Publication of registration
FPAY Annual fee payment

Payment date: 20130103

Year of fee payment: 4

PR1001 Payment of annual fee

Payment date: 20130103

Start annual number: 4

End annual number: 4

FPAY Annual fee payment

Payment date: 20140107

Year of fee payment: 5

PR1001 Payment of annual fee

Payment date: 20140107

Start annual number: 5

End annual number: 5

FPAY Annual fee payment

Payment date: 20150105

Year of fee payment: 6

PR1001 Payment of annual fee

Payment date: 20150105

Start annual number: 6

End annual number: 6

FPAY Annual fee payment

Payment date: 20151230

Year of fee payment: 7

PR1001 Payment of annual fee

Payment date: 20151230

Start annual number: 7

End annual number: 7

FPAY Annual fee payment

Payment date: 20170105

Year of fee payment: 8

PR1001 Payment of annual fee

Payment date: 20170105

Start annual number: 8

End annual number: 8

FPAY Annual fee payment

Payment date: 20171221

Year of fee payment: 9

PR1001 Payment of annual fee

Payment date: 20171221

Start annual number: 9

End annual number: 9

FPAY Annual fee payment

Payment date: 20181226

Year of fee payment: 10

PR1001 Payment of annual fee

Payment date: 20181226

Start annual number: 10

End annual number: 10

FPAY Annual fee payment

Payment date: 20191219

Year of fee payment: 11

PR1001 Payment of annual fee

Payment date: 20191219

Start annual number: 11

End annual number: 11

PR1001 Payment of annual fee

Payment date: 20201217

Start annual number: 12

End annual number: 12

PR1001 Payment of annual fee

Payment date: 20211220

Start annual number: 13

End annual number: 13

PR1001 Payment of annual fee

Payment date: 20221222

Start annual number: 14

End annual number: 14

PC1801 Expiration of term

Termination date: 20230812

Termination category: Expiration of duration