JPWO2014010492A1 - 混合ペレット - Google Patents
混合ペレット Download PDFInfo
- Publication number
- JPWO2014010492A1 JPWO2014010492A1 JP2014524763A JP2014524763A JPWO2014010492A1 JP WO2014010492 A1 JPWO2014010492 A1 JP WO2014010492A1 JP 2014524763 A JP2014524763 A JP 2014524763A JP 2014524763 A JP2014524763 A JP 2014524763A JP WO2014010492 A1 JPWO2014010492 A1 JP WO2014010492A1
- Authority
- JP
- Japan
- Prior art keywords
- mass
- carbon atoms
- parts
- pellet
- butyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000008188 pellet Substances 0.000 title claims abstract description 77
- -1 amine compound Chemical class 0.000 claims abstract description 109
- 239000004594 Masterbatch (MB) Substances 0.000 claims abstract description 52
- 229920005672 polyolefin resin Polymers 0.000 claims abstract description 19
- 229920000098 polyolefin Polymers 0.000 claims abstract description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims description 33
- 125000000217 alkyl group Chemical group 0.000 claims description 29
- 229910052751 metal Inorganic materials 0.000 claims description 25
- 239000002184 metal Substances 0.000 claims description 25
- 238000002156 mixing Methods 0.000 claims description 22
- 150000003839 salts Chemical class 0.000 claims description 20
- 229910019142 PO4 Inorganic materials 0.000 claims description 12
- 229910052783 alkali metal Inorganic materials 0.000 claims description 12
- 229910052782 aluminium Inorganic materials 0.000 claims description 11
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 11
- 125000003118 aryl group Chemical group 0.000 claims description 11
- 150000001340 alkali metals Chemical class 0.000 claims description 10
- 239000010452 phosphate Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- 239000011342 resin composition Substances 0.000 claims description 9
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 8
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 7
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 7
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 7
- 125000003545 alkoxy group Chemical group 0.000 claims description 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 4
- 125000003342 alkenyl group Chemical group 0.000 claims description 3
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 3
- 125000005113 hydroxyalkoxy group Chemical group 0.000 claims description 3
- 125000002768 hydroxyalkyl group Chemical group 0.000 claims description 3
- 230000000903 blocking effect Effects 0.000 abstract description 13
- 230000007774 longterm Effects 0.000 abstract description 4
- 238000003860 storage Methods 0.000 abstract description 4
- 229920005989 resin Polymers 0.000 description 28
- 239000011347 resin Substances 0.000 description 28
- 150000001875 compounds Chemical class 0.000 description 23
- 238000000034 method Methods 0.000 description 17
- 239000003795 chemical substances by application Substances 0.000 description 11
- 229920001577 copolymer Polymers 0.000 description 11
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 11
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 10
- 235000021317 phosphate Nutrition 0.000 description 10
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 9
- 239000002216 antistatic agent Substances 0.000 description 9
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 9
- 238000013329 compounding Methods 0.000 description 9
- GDVKFRBCXAPAQJ-UHFFFAOYSA-A dialuminum;hexamagnesium;carbonate;hexadecahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Al+3].[Al+3].[O-]C([O-])=O GDVKFRBCXAPAQJ-UHFFFAOYSA-A 0.000 description 9
- 229920001971 elastomer Polymers 0.000 description 9
- 229960001545 hydrotalcite Drugs 0.000 description 9
- 229910001701 hydrotalcite Inorganic materials 0.000 description 9
- 0 CC(C)(C1)NC(C2)(CC2(C2)NC(C)(C)CC2OC(*(C)=*)=O)CC1OC(*)=O Chemical compound CC(C)(C1)NC(C2)(CC2(C2)NC(C)(C)CC2OC(*(C)=*)=O)CC1OC(*)=O 0.000 description 8
- 239000007983 Tris buffer Substances 0.000 description 8
- 235000014113 dietary fatty acids Nutrition 0.000 description 8
- 239000000194 fatty acid Substances 0.000 description 8
- 229930195729 fatty acid Natural products 0.000 description 8
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 7
- 239000013078 crystal Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 7
- 229920000642 polymer Polymers 0.000 description 7
- 239000005060 rubber Substances 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 6
- 239000003963 antioxidant agent Substances 0.000 description 6
- 235000006708 antioxidants Nutrition 0.000 description 6
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 description 6
- 239000012964 benzotriazole Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- 239000003063 flame retardant Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 5
- 239000002253 acid Substances 0.000 description 5
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 5
- 125000003187 heptyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 5
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 5
- 229910052749 magnesium Inorganic materials 0.000 description 5
- 239000011777 magnesium Substances 0.000 description 5
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 5
- 229910052698 phosphorus Inorganic materials 0.000 description 5
- 239000011574 phosphorus Substances 0.000 description 5
- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 5
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 4
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 4
- 230000003078 antioxidant effect Effects 0.000 description 4
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 4
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 4
- 150000004665 fatty acids Chemical class 0.000 description 4
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 4
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 4
- 239000000314 lubricant Substances 0.000 description 4
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 description 4
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 4
- ZHROMWXOTYBIMF-UHFFFAOYSA-M sodium;1,3,7,9-tetratert-butyl-11-oxido-5h-benzo[d][1,3,2]benzodioxaphosphocine 11-oxide Chemical compound [Na+].C1C2=CC(C(C)(C)C)=CC(C(C)(C)C)=C2OP([O-])(=O)OC2=C1C=C(C(C)(C)C)C=C2C(C)(C)C ZHROMWXOTYBIMF-UHFFFAOYSA-M 0.000 description 4
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 4
- 239000004711 α-olefin Substances 0.000 description 4
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 3
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Natural products CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 3
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Chemical group CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 3
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 3
- 239000004743 Polypropylene Substances 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 3
- 239000006096 absorbing agent Substances 0.000 description 3
- 150000001450 anions Chemical group 0.000 description 3
- 150000001993 dienes Chemical class 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 239000000945 filler Substances 0.000 description 3
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 3
- 238000004898 kneading Methods 0.000 description 3
- 125000001421 myristyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
- UKJARPDLRWBRAX-UHFFFAOYSA-N n,n'-bis(2,2,6,6-tetramethylpiperidin-4-yl)hexane-1,6-diamine Chemical compound C1C(C)(C)NC(C)(C)CC1NCCCCCCNC1CC(C)(C)NC(C)(C)C1 UKJARPDLRWBRAX-UHFFFAOYSA-N 0.000 description 3
- GKTNLYAAZKKMTQ-UHFFFAOYSA-N n-[bis(dimethylamino)phosphinimyl]-n-methylmethanamine Chemical class CN(C)P(=N)(N(C)C)N(C)C GKTNLYAAZKKMTQ-UHFFFAOYSA-N 0.000 description 3
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
- 239000002530 phenolic antioxidant Substances 0.000 description 3
- 229920000728 polyester Polymers 0.000 description 3
- 229920000139 polyethylene terephthalate Polymers 0.000 description 3
- 239000005020 polyethylene terephthalate Substances 0.000 description 3
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- 229920005629 polypropylene homopolymer Polymers 0.000 description 3
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 3
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- 230000002194 synthesizing effect Effects 0.000 description 3
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 3
- 150000003568 thioethers Chemical class 0.000 description 3
- HVLLSGMXQDNUAL-UHFFFAOYSA-N triphenyl phosphite Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)OC1=CC=CC=C1 HVLLSGMXQDNUAL-UHFFFAOYSA-N 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
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- ONTODYXHFBKCDK-UHFFFAOYSA-N 2-(2,4-dimethylphenyl)-1,3,5-triazine Chemical compound CC1=CC(C)=CC=C1C1=NC=NC=N1 ONTODYXHFBKCDK-UHFFFAOYSA-N 0.000 description 2
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- ZEEBGORNQSEQBE-UHFFFAOYSA-N [2-(3-phenylphenoxy)-6-(trifluoromethyl)pyridin-4-yl]methanamine Chemical compound C1(=CC(=CC=C1)OC1=NC(=CC(=C1)CN)C(F)(F)F)C1=CC=CC=C1 ZEEBGORNQSEQBE-UHFFFAOYSA-N 0.000 description 2
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- ZJIPHXXDPROMEF-UHFFFAOYSA-N dihydroxyphosphanyl dihydrogen phosphite Chemical compound OP(O)OP(O)O ZJIPHXXDPROMEF-UHFFFAOYSA-N 0.000 description 2
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- 239000004299 sodium benzoate Substances 0.000 description 1
- 239000012321 sodium triacetoxyborohydride Substances 0.000 description 1
- REENPYPZHGUSQE-UHFFFAOYSA-M sodium;bis(2,4-ditert-butylphenyl) phosphate Chemical compound [Na+].CC(C)(C)C1=CC(C(C)(C)C)=CC=C1OP([O-])(=O)OC1=CC=C(C(C)(C)C)C=C1C(C)(C)C REENPYPZHGUSQE-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 1
- DJZKNOVUNYPPEE-UHFFFAOYSA-N tetradecane-1,4,11,14-tetracarboxamide Chemical compound NC(=O)CCCC(C(N)=O)CCCCCCC(C(N)=O)CCCC(N)=O DJZKNOVUNYPPEE-UHFFFAOYSA-N 0.000 description 1
- LVEOKSIILWWVEO-UHFFFAOYSA-N tetradecyl 3-(3-oxo-3-tetradecoxypropyl)sulfanylpropanoate Chemical compound CCCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCCC LVEOKSIILWWVEO-UHFFFAOYSA-N 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
- MZHULIWXRDLGRR-UHFFFAOYSA-N tridecyl 3-(3-oxo-3-tridecoxypropyl)sulfanylpropanoate Chemical compound CCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCC MZHULIWXRDLGRR-UHFFFAOYSA-N 0.000 description 1
- IVIIAEVMQHEPAY-UHFFFAOYSA-N tridodecyl phosphite Chemical compound CCCCCCCCCCCCOP(OCCCCCCCCCCCC)OCCCCCCCCCCCC IVIIAEVMQHEPAY-UHFFFAOYSA-N 0.000 description 1
- CENHPXAQKISCGD-UHFFFAOYSA-N trioxathietane 4,4-dioxide Chemical compound O=S1(=O)OOO1 CENHPXAQKISCGD-UHFFFAOYSA-N 0.000 description 1
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 description 1
- KOWVWXQNQNCRRS-UHFFFAOYSA-N tris(2,4-dimethylphenyl) phosphate Chemical compound CC1=CC(C)=CC=C1OP(=O)(OC=1C(=CC(C)=CC=1)C)OC1=CC=C(C)C=C1C KOWVWXQNQNCRRS-UHFFFAOYSA-N 0.000 description 1
- LTXMJHWSYUANCC-UHFFFAOYSA-N tris(2,4-ditert-butyl-5-methylphenyl) phosphite Chemical compound C1=C(C(C)(C)C)C(C)=CC(OP(OC=2C(=CC(=C(C)C=2)C(C)(C)C)C(C)(C)C)OC=2C(=CC(=C(C)C=2)C(C)(C)C)C(C)(C)C)=C1C(C)(C)C LTXMJHWSYUANCC-UHFFFAOYSA-N 0.000 description 1
- DECPGQLXYYCNEZ-UHFFFAOYSA-N tris(6-methylheptyl) phosphite Chemical compound CC(C)CCCCCOP(OCCCCCC(C)C)OCCCCCC(C)C DECPGQLXYYCNEZ-UHFFFAOYSA-N 0.000 description 1
- JZNDMMGBXUYFNQ-UHFFFAOYSA-N tris(dodecylsulfanyl)phosphane Chemical compound CCCCCCCCCCCCSP(SCCCCCCCCCCCC)SCCCCCCCCCCCC JZNDMMGBXUYFNQ-UHFFFAOYSA-N 0.000 description 1
- QQBLOZGVRHAYGT-UHFFFAOYSA-N tris-decyl phosphite Chemical compound CCCCCCCCCCOP(OCCCCCCCCCC)OCCCCCCCCCC QQBLOZGVRHAYGT-UHFFFAOYSA-N 0.000 description 1
- SGKKYCDALBXNCG-UHFFFAOYSA-N tris[2-tert-butyl-4-(3-tert-butyl-4-hydroxy-5-methylphenyl)sulfanyl-5-methylphenyl] phosphite Chemical compound CC(C)(C)C1=C(O)C(C)=CC(SC=2C(=CC(OP(OC=3C(=CC(SC=4C=C(C(O)=C(C)C=4)C(C)(C)C)=C(C)C=3)C(C)(C)C)OC=3C(=CC(SC=4C=C(C(O)=C(C)C=4)C(C)(C)C)=C(C)C=3)C(C)(C)C)=C(C=2)C(C)(C)C)C)=C1 SGKKYCDALBXNCG-UHFFFAOYSA-N 0.000 description 1
- PEXOFOFLXOCMDX-UHFFFAOYSA-N tritridecyl phosphite Chemical compound CCCCCCCCCCCCCOP(OCCCCCCCCCCCCC)OCCCCCCCCCCCCC PEXOFOFLXOCMDX-UHFFFAOYSA-N 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 229920006337 unsaturated polyester resin Polymers 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 239000010456 wollastonite Substances 0.000 description 1
- 229910052882 wollastonite Inorganic materials 0.000 description 1
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Abstract
Description
(式(1)中、R1は水素原子、ヒドロキシ基、炭素原子数1〜30のアルキル基、ヒドロキシアルキル基、アルコキシ基、ヒドロキシアルコキシ基またはオキシラジカルを表し、R2は炭素原子数1〜30のアルキル基又は炭素原子数2〜30のアルケニル基を表す)
(式(2)中、R3及びR4は各々独立に水素原子、炭素原子数1〜12のアルキル基または炭素原子数7〜30のアリールアルキル基、R5は炭素原子数1〜30のアルキル基を表す)
(式(3)中、R6は、炭素原子数4〜8のアルキル基を表し、R7は水素原子または炭素原子数1〜8のアルキル基を表し、R8は炭素原子数1〜4のアルキリデン基を表し、Mはアルカリ金属、アルカリ土類金属またはアルミニウムを表し、Mがアルカリ金属の場合、nは1であって、かつqは0であり、Mがアルカリ土類金属の場合、nは2であって、かつqは0であり、Mがアルミニウムの場合、nは1または2であって、かつqは3−nを表す)
本発明に用いられるポリオレフィン樹脂としては、ポリオレフィンであれば特に制限されずに用いることが可能であり、ポリプロピレン、低密度ポリエチレン、直鎖低密度ポリエチレン、高密度ポリエチレン、ポリブテン−1、ポリ−3−メチルペンテン、ポリ−4−メチルペンテン、エチレン−プロピレン共重合体等のα−オレフィンの単重合体または共重合体等が挙げられる。
(式(3)中、R6は、炭素原子数4〜8のアルキル基を表し、R7は水素原子または炭素原子数1〜8のアルキル基を表し、R8は炭素原子数1〜4のアルキリデン基を表し、Mはアルカリ金属、アルカリ土類金属またはアルミニウムを表し、Mがアルカリ金属の場合、nは1であって、かつqは0であり、Mがアルカリ土類金属の場合、nは2であって、かつqは0であり、Mがアルミニウムの場合、nは1または2であって、かつqは3−nを表す)
(式中、x1およびx2は各々下記式で表される条件を満たす数を表し、pは0または正の数を表す。0≦x2/x1<10,2≦x1+x2≦20である。)
(式中、Aq−は、q価のアニオンを表し、pは0または正の数を表す。)
また、上記ハイドロタルサイトにおける炭酸アニオンは、一部を他のアニオンで置換したものでもよい。
ホモポリプロピレン(メルトフローレート(MFR)=11g/10min)、芳香族リン酸エステル金属塩:化合物3−7(株式会社ADEKA製 商品名;アデカスタブNA−11)、及び、ヒンダードアミン化合物:化合物1−1と化合物1−2の混合物(株式会社ADEKA製 商品名:アデカスタブLA−40)を表1記載の配合量で加え、ヘンシェルミキサーで1分間混合後、二軸押出機(日本製鋼所製 TEX30α)を用い、200℃、ダイス温度170℃の条件で、直径3mmのストランド状に押出し、長さ3mmになるようにストランドを切断してマスターバッチペレットを製造した。なお、表1記載の数値は全て質量部である。
ホモポリプロピレン(MFR=11g/10min)、芳香族リン酸エステル金属塩:化合物3−7(株式会社ADEKA製 商品名;アデカスタブNA−11)、及び、ベンゾエート化合物:(化合物2−1)を表1記載の配合量で加え、ヘンシェルミキサーで1分間混合後、二軸押出機(日本製鋼所製 TEX30α)を用い、200℃、ダイス温度170℃の条件で、直径3mmのストランド状に押出し、長さ3mmになるようにストランドを切断してマスターバッチペレットを製造した。
ホモポリプロピレン(MFR=11g/10min)、芳香族リン酸エステル金属塩:化合物3−7(株式会社ADEKA製 商品名;アデカスタブNA−11)、ヒンダードアミン化合物:化合物1−1と化合物1−2の混合物(株式会社ADEKA製 商品名:アデカスタブLA−40)及びベンゾエート化合物:化合物2−1を表1記載の配合量で加え、ヘンシェルミキサーで1分間混合後、二軸押出機(日本製鋼所製 TEX30α)を用い、200℃、ダイス温度170℃の条件で、直径3mmのストランド状に押出し、長さ3mmになるようにストランドを切断して、マスターバッチペレットを製造した。
上記の方法で得られたマスターバッチ20gを、底面積12.6cm2、高さ6cmの75ml容量のガラス製サンプル瓶の中に入れ、密栓して、50℃の恒温器に24時間、5℃の恒温器に12時間、25℃の恒温器に3時間の順番でサンプル瓶を放置した。次に、サンプル瓶の上下を静かに逆さにして、マスターバッチの落下状態から、耐ブロッキング性を評価した。評価基準は以下の通りである。レベル1が最も耐ブロッキング性に優れ、2,3,4と劣っていき、レベル5が最も劣る。
レベル1:サンプル瓶の上下を静かに逆さにして、マスターバッチが落下する。
レベル2:レベル1で落ちず、逆さにしたサンプル瓶を5mm上空から、平らな台上に落として振動を与えると、マスターバッチが落下する。
レベル3:レベル2で落ちず、逆さにしたサンプル瓶を30mm上空から、平らな台上に落として振動を与えると、マスターバッチが落下する。
レベル4:レベル3で落ちず、サンプル瓶を何回か上下に振ると、マスターバッチが落下する。
レベル5:レベル4でもマスターバッチが落下しない。
Claims (5)
- (A)ポリオレフィン樹脂100質量部に対して、下記一般式(1)で表されるヒンダードアミン化合物を30質量部以上含有するマスターバッチペレットと、(B)ポリオレフィン100質量部に対して、下記一般式(2)で表されるベンゾエート化合物を30質量部以上含有するマスターバッチペレットと、を混合してなる混合ペレットであって、混合ペレット全体のうち70質量%以上が、(A)及び(B)のマスターバッチペレットであることを特徴とする混合ペレット。
(式(1)中、R1は水素原子、ヒドロキシ基、炭素原子数1〜30のアルキル基、ヒドロキシアルキル基、アルコキシ基、ヒドロキシアルコキシ基またはオキシラジカルを表し、R2は炭素原子数1〜30のアルキル基又は炭素原子数2〜30のアルケニル基を表す)
(式(2)中、R3及びR4は各々独立に水素原子、炭素原子数1〜12のアルキル基または炭素原子数7〜30のアリールアルキル基、R5は炭素原子数1〜30のアルキル基を表す) - 前記ヒンダードアミン化合物及び前記ベンゾエート化合物の混合ペレット全体における含有割合が、30〜60質量%である請求項1記載の混合ペレット。
- 前記(A)又は(B)のいずれか一方、若しくは(A)及び(B)の双方のマスターバッチペレットが、下記一般式(3)で表される芳香族リン酸エステル金属塩の一種以上を含み、かつ、該芳香族リン酸エステルを含有する場合の(A)および(B)それぞれのマスターバッチペレットにおける含有量が、ポリオレフィン樹脂100質量部に対して0.3〜5質量部である請求項1記載の混合ペレット。
(式(3)中、R6は、炭素原子数4〜8のアルキル基を表し、R7は水素原子または炭素原子数1〜8のアルキル基を表し、R8は炭素原子数1〜4のアルキリデン基を表し、Mはアルカリ金属、アルカリ土類金属またはアルミニウムを表し、Mがアルカリ金属の場合、nは1であって、かつqは0であり、Mがアルカリ土類金属の場合、nは2であって、かつqは0であり、Mがアルミニウムの場合、nは1または2であって、かつqは3−nを表す) - ポリオレフィン樹脂に対し、請求項1記載の混合ペレットを配合してなるポリオレフィン樹脂組成物。
- 請求項4記載のポリオレフィン樹脂組成物を成形してなる成形品。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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JP2012154504 | 2012-07-10 | ||
JP2012154504 | 2012-07-10 | ||
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CN (1) | CN104428350B (ja) |
BR (1) | BR112015000600B1 (ja) |
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US10972530B2 (en) | 2016-12-30 | 2021-04-06 | Google Llc | Audio-based data structure generation |
JP2016172832A (ja) * | 2015-03-18 | 2016-09-29 | 株式会社Adeka | 樹脂添加剤マスターバッチ |
US10246563B2 (en) | 2015-03-30 | 2019-04-02 | Adeka Corporation | Photostabilizer master batch and method for manufacturing same |
CA2993973C (en) | 2015-07-31 | 2021-06-22 | Cytec Industries Inc. | Encapsulated stabilizer compositions |
CN105733158B (zh) * | 2016-04-21 | 2017-10-10 | 上海宏盎实业发展有限公司 | 新型塑料填充母粒 |
JP7033843B2 (ja) * | 2016-10-12 | 2022-03-11 | 株式会社Adeka | ポリオレフィン系樹脂組成物およびこれを用いた成形品 |
JP7288840B2 (ja) * | 2019-11-14 | 2023-06-08 | 信越ポリマー株式会社 | 熱可塑性ポリウレタンエラストマー組成物の製造方法 |
WO2022054893A1 (ja) * | 2020-09-11 | 2022-03-17 | 大阪ガスケミカル株式会社 | 樹脂混練用添加剤 |
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JPH062280B2 (ja) | 1984-12-28 | 1994-01-12 | 大同特殊鋼株式会社 | 溶 融 処 理 方 法 |
JPS61174270A (ja) | 1985-01-29 | 1986-08-05 | Kyowa Chem Ind Co Ltd | 耐発錆性ないし耐着色性賦与剤 |
JPH072858B2 (ja) | 1991-12-27 | 1995-01-18 | 水澤化学工業株式会社 | 樹脂用安定剤 |
JPH10195258A (ja) | 1997-01-08 | 1998-07-28 | Asahi Denka Kogyo Kk | 農業用フィルム組成物 |
JP2000159940A (ja) | 1998-11-27 | 2000-06-13 | Asahi Denka Kogyo Kk | ポリオレフィン樹脂組成物 |
JP4785228B2 (ja) | 2000-04-21 | 2011-10-05 | 株式会社Adeka | 繊維用ポリオレフィン樹脂組成物 |
JP4530327B2 (ja) | 2003-07-29 | 2010-08-25 | 株式会社Adeka | 耐候性の改善された硫化亜鉛配合合成樹脂組成物 |
JP4462867B2 (ja) | 2003-08-06 | 2010-05-12 | 株式会社Adeka | 耐候性の改善された合成樹脂組成物及び内外装材 |
JP2006342257A (ja) | 2005-06-09 | 2006-12-21 | Adeka Corp | アルミニウム顔料配合樹脂組成物 |
WO2007069760A1 (ja) * | 2005-12-14 | 2007-06-21 | Sumitomo Chemical Company, Limited | ポリオレフィン樹脂組成物、それからなる成形品、およびポリオレフィン樹脂組成物の製造方法 |
JP5456237B2 (ja) | 2007-02-05 | 2014-03-26 | 株式会社Adeka | 樹脂添加剤マスターバッチ |
JP5478013B2 (ja) | 2007-12-18 | 2014-04-23 | 株式会社Adeka | オレフィン系弾性樹脂組成物 |
JP2011190345A (ja) | 2010-03-15 | 2011-09-29 | Sumitomo Chemical Co Ltd | ポリプロピレン樹脂組成物及びポリプロピレン樹脂製フィルム |
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JP6067458B2 (ja) | 2013-03-29 | 2017-01-25 | 株式会社Adeka | 樹脂添加剤マスターバッチおよび該樹脂添加剤マスターバッチが配合されたポリオレフィン樹脂組成物 |
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JP2007186687A (ja) * | 2005-12-14 | 2007-07-26 | Sumitomo Chemical Co Ltd | ポリオレフィン樹脂組成物およびその成形品 |
WO2011148868A1 (ja) * | 2010-05-26 | 2011-12-01 | 株式会社Adeka | 樹脂添加剤マスターバッチ |
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EP2873686A1 (en) | 2015-05-20 |
KR20150033605A (ko) | 2015-04-01 |
KR102076101B1 (ko) | 2020-02-11 |
JP6226387B2 (ja) | 2017-11-08 |
EP2873686B1 (en) | 2018-09-05 |
TWI588195B (zh) | 2017-06-21 |
EP2873686A4 (en) | 2016-03-23 |
US20150158996A1 (en) | 2015-06-11 |
US9376550B2 (en) | 2016-06-28 |
TW201418347A (zh) | 2014-05-16 |
WO2014010492A1 (ja) | 2014-01-16 |
BR112015000600B1 (pt) | 2021-03-02 |
ES2689471T3 (es) | 2018-11-14 |
CN104428350B (zh) | 2017-05-31 |
CN104428350A (zh) | 2015-03-18 |
BR112015000600A2 (ja) | 2019-12-31 |
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