JPS61221299A - 動植物材料から有機質成分を抽出・分離する方法 - Google Patents
動植物材料から有機質成分を抽出・分離する方法Info
- Publication number
- JPS61221299A JPS61221299A JP6188585A JP6188585A JPS61221299A JP S61221299 A JPS61221299 A JP S61221299A JP 6188585 A JP6188585 A JP 6188585A JP 6188585 A JP6188585 A JP 6188585A JP S61221299 A JPS61221299 A JP S61221299A
- Authority
- JP
- Japan
- Prior art keywords
- carbon dioxide
- container
- extraction
- organic components
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000605 extraction Methods 0.000 title claims description 88
- 238000000926 separation method Methods 0.000 title claims description 42
- 241001465754 Metazoa Species 0.000 title claims description 26
- 239000005418 vegetable material Substances 0.000 title 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 250
- 239000001569 carbon dioxide Substances 0.000 claims description 125
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 125
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 74
- 239000000203 mixture Substances 0.000 claims description 56
- 238000000034 method Methods 0.000 claims description 48
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 31
- 235000019441 ethanol Nutrition 0.000 claims description 29
- 239000007787 solid Substances 0.000 claims description 26
- 239000000463 material Substances 0.000 claims description 22
- 239000007788 liquid Substances 0.000 claims description 19
- 230000001737 promoting effect Effects 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 13
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 3
- 238000000859 sublimation Methods 0.000 claims description 3
- 230000008022 sublimation Effects 0.000 claims description 3
- 239000003507 refrigerant Substances 0.000 claims description 2
- 238000009834 vaporization Methods 0.000 claims description 2
- 230000008016 vaporization Effects 0.000 claims description 2
- 239000000284 extract Substances 0.000 description 36
- 239000007789 gas Substances 0.000 description 34
- 241000196324 Embryophyta Species 0.000 description 18
- 239000003921 oil Substances 0.000 description 15
- 235000019198 oils Nutrition 0.000 description 15
- 244000290333 Vanilla fragrans Species 0.000 description 14
- 235000009499 Vanilla fragrans Nutrition 0.000 description 14
- 235000012036 Vanilla tahitensis Nutrition 0.000 description 14
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 description 10
- 239000000126 substance Substances 0.000 description 10
- 241000533293 Sesbania emerus Species 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 7
- 210000004185 liver Anatomy 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 description 5
- 229960001948 caffeine Drugs 0.000 description 5
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 description 5
- 244000068988 Glycine max Species 0.000 description 4
- 235000010469 Glycine max Nutrition 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 239000008601 oleoresin Substances 0.000 description 4
- 238000000638 solvent extraction Methods 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000010903 husk Substances 0.000 description 3
- 239000012046 mixed solvent Substances 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- 241000251730 Chondrichthyes Species 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 239000012267 brine Substances 0.000 description 2
- 230000006835 compression Effects 0.000 description 2
- 238000007906 compression Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 235000015243 ice cream Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- 235000019645 odor Nutrition 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 2
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 description 2
- 235000012141 vanillin Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 102100024452 DNA-directed RNA polymerase III subunit RPC1 Human genes 0.000 description 1
- 241000276438 Gadus morhua Species 0.000 description 1
- 101000689002 Homo sapiens DNA-directed RNA polymerase III subunit RPC1 Proteins 0.000 description 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical group OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 1
- 241000745768 Pluchea carolinensis Species 0.000 description 1
- 238000000944 Soxhlet extraction Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000003949 liquefied natural gas Substances 0.000 description 1
- 210000005228 liver tissue Anatomy 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000004382 potting Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- YQUVCSBJEUQKSH-UHFFFAOYSA-N protochatechuic acid Natural products OC(=O)C1=CC=C(O)C(O)=C1 YQUVCSBJEUQKSH-UHFFFAOYSA-N 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000013557 residual solvent Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- WKOLLVMJNQIZCI-UHFFFAOYSA-N vanillic acid Chemical compound COC1=CC(C(O)=O)=CC=C1O WKOLLVMJNQIZCI-UHFFFAOYSA-N 0.000 description 1
- TUUBOHWZSQXCSW-UHFFFAOYSA-N vanillic acid Natural products COC1=CC(O)=CC(C(O)=O)=C1 TUUBOHWZSQXCSW-UHFFFAOYSA-N 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Landscapes
- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6188585A JPS61221299A (ja) | 1985-03-28 | 1985-03-28 | 動植物材料から有機質成分を抽出・分離する方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6188585A JPS61221299A (ja) | 1985-03-28 | 1985-03-28 | 動植物材料から有機質成分を抽出・分離する方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61221299A true JPS61221299A (ja) | 1986-10-01 |
| JPH0254880B2 JPH0254880B2 (enrdf_load_stackoverflow) | 1990-11-22 |
Family
ID=13184045
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP6188585A Granted JPS61221299A (ja) | 1985-03-28 | 1985-03-28 | 動植物材料から有機質成分を抽出・分離する方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61221299A (enrdf_load_stackoverflow) |
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6456793A (en) * | 1987-08-27 | 1989-03-03 | Mori Seiyu Kk | Method for extracting and separating vegetable fat and oil |
| JPH02135069A (ja) * | 1988-11-17 | 1990-05-23 | T Hasegawa Co Ltd | 香辛料エキスの製造方法 |
| JPH02235998A (ja) * | 1989-03-09 | 1990-09-18 | T Hasegawa Co Ltd | ロースト種実類フレーバーの製造方法 |
| JPH02235995A (ja) * | 1989-03-09 | 1990-09-18 | T Hasegawa Co Ltd | 植物油の抽出法 |
| JPH02235996A (ja) * | 1989-03-09 | 1990-09-18 | T Hasegawa Co Ltd | 植物油の抽出方法 |
| JPH02235997A (ja) * | 1989-03-09 | 1990-09-18 | T Hasegawa Co Ltd | 海藻類フレーバーの製造方法 |
| JPH02283256A (ja) * | 1988-12-13 | 1990-11-20 | T Hasegawa Co Ltd | 甲殻類フレーバーの製法 |
| JPH0387160A (ja) * | 1989-08-31 | 1991-04-11 | T Hasegawa Co Ltd | 濃厚加熱調理フレーバーの製法 |
| JPH0394651A (ja) * | 1989-09-08 | 1991-04-19 | T Hasegawa Co Ltd | 獣鳥肉類焙焼調理加工品フレーバーの製法 |
| JPH03127961A (ja) * | 1989-10-12 | 1991-05-31 | T Hasegawa Co Ltd | 穀類焙焼フレーバーの製造方法 |
| JPH04214799A (ja) * | 1990-11-22 | 1992-08-05 | T Hasegawa Co Ltd | 新規なバニラエキスの製法 |
| JPH04246500A (ja) * | 1991-01-31 | 1992-09-02 | Showa Tansan Kk | ジンコウ木より芳香性有機質成分の抽出分離法 |
| JPH0559391A (ja) * | 1991-08-30 | 1993-03-09 | Mitsui & Co Ltd | 精製プロポリスおよび精製プロポリス成分含有ｏ／ｗ型乳化物の製造法 |
| JPH06184591A (ja) * | 1986-06-23 | 1994-07-05 | House Foods Corp | 茶葉香気成分の抽出方法 |
| JP2003512481A (ja) * | 1999-10-21 | 2003-04-02 | ラボラトイレス ラヴィファーム エス．エー． | 超臨界圧溶剤を用いた数種の成分からなる原料の分留方法 |
| JP2006097011A (ja) * | 2004-09-01 | 2006-04-13 | Malaysian Palm Oil Board | 特殊なパーム油製品およびその他の特殊な植物油製品 |
| JP2006223239A (ja) * | 2005-02-21 | 2006-08-31 | Kaneo Chiba | 酸素ナノバブルを利用した魚介類焙焼有効成分抽出方法およびその抽出方法によって得られた有効成分を添加した魚肉加工品素材 |
| JP2007111693A (ja) * | 2003-11-19 | 2007-05-10 | Scf Technologies As | 高密度流体プロセスの温度、圧力、密度を制御する方法とプロセス |
| US8580116B2 (en) | 2006-02-07 | 2013-11-12 | Industrial Research Limited | Near-critical fluid extraction process |
| JP2014505586A (ja) * | 2010-12-30 | 2014-03-06 | フェイェコン・ビー．ブイ． | イオン液体のコリン塩を使用する脱水方法 |
| JP2015168718A (ja) * | 2014-03-05 | 2015-09-28 | 一般財団法人電力中央研究所 | 油脂抽出方法 |
| CN106852158A (zh) * | 2014-07-07 | 2017-06-13 | 联邦科学技术研究组织 | 从植物脂质生产工业产品的方法 |
-
1985
- 1985-03-28 JP JP6188585A patent/JPS61221299A/ja active Granted
Cited By (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06184591A (ja) * | 1986-06-23 | 1994-07-05 | House Foods Corp | 茶葉香気成分の抽出方法 |
| JPS6456793A (en) * | 1987-08-27 | 1989-03-03 | Mori Seiyu Kk | Method for extracting and separating vegetable fat and oil |
| JPH02135069A (ja) * | 1988-11-17 | 1990-05-23 | T Hasegawa Co Ltd | 香辛料エキスの製造方法 |
| JPH02283256A (ja) * | 1988-12-13 | 1990-11-20 | T Hasegawa Co Ltd | 甲殻類フレーバーの製法 |
| JPH02235995A (ja) * | 1989-03-09 | 1990-09-18 | T Hasegawa Co Ltd | 植物油の抽出法 |
| JPH02235997A (ja) * | 1989-03-09 | 1990-09-18 | T Hasegawa Co Ltd | 海藻類フレーバーの製造方法 |
| JPH02235996A (ja) * | 1989-03-09 | 1990-09-18 | T Hasegawa Co Ltd | 植物油の抽出方法 |
| JPH02235998A (ja) * | 1989-03-09 | 1990-09-18 | T Hasegawa Co Ltd | ロースト種実類フレーバーの製造方法 |
| JPH0387160A (ja) * | 1989-08-31 | 1991-04-11 | T Hasegawa Co Ltd | 濃厚加熱調理フレーバーの製法 |
| JPH0394651A (ja) * | 1989-09-08 | 1991-04-19 | T Hasegawa Co Ltd | 獣鳥肉類焙焼調理加工品フレーバーの製法 |
| JPH03127961A (ja) * | 1989-10-12 | 1991-05-31 | T Hasegawa Co Ltd | 穀類焙焼フレーバーの製造方法 |
| JPH04214799A (ja) * | 1990-11-22 | 1992-08-05 | T Hasegawa Co Ltd | 新規なバニラエキスの製法 |
| JPH04246500A (ja) * | 1991-01-31 | 1992-09-02 | Showa Tansan Kk | ジンコウ木より芳香性有機質成分の抽出分離法 |
| JPH0559391A (ja) * | 1991-08-30 | 1993-03-09 | Mitsui & Co Ltd | 精製プロポリスおよび精製プロポリス成分含有ｏ／ｗ型乳化物の製造法 |
| JP2003512481A (ja) * | 1999-10-21 | 2003-04-02 | ラボラトイレス ラヴィファーム エス．エー． | 超臨界圧溶剤を用いた数種の成分からなる原料の分留方法 |
| JP2007111693A (ja) * | 2003-11-19 | 2007-05-10 | Scf Technologies As | 高密度流体プロセスの温度、圧力、密度を制御する方法とプロセス |
| JP2007511357A (ja) * | 2003-11-19 | 2007-05-10 | エスセーエフ テクノロジーズ アクティーゼルスカブ | 高密度流体プロセスの温度、圧力、密度を制御する方法とプロセス |
| JP2006097011A (ja) * | 2004-09-01 | 2006-04-13 | Malaysian Palm Oil Board | 特殊なパーム油製品およびその他の特殊な植物油製品 |
| JP2013100506A (ja) * | 2004-09-01 | 2013-05-23 | Malaysian Palm Oil Board | 特殊なパーム油製品およびその他の特殊な植物油製品 |
| JP2006223239A (ja) * | 2005-02-21 | 2006-08-31 | Kaneo Chiba | 酸素ナノバブルを利用した魚介類焙焼有効成分抽出方法およびその抽出方法によって得られた有効成分を添加した魚肉加工品素材 |
| US8580116B2 (en) | 2006-02-07 | 2013-11-12 | Industrial Research Limited | Near-critical fluid extraction process |
| JP2014505586A (ja) * | 2010-12-30 | 2014-03-06 | フェイェコン・ビー．ブイ． | イオン液体のコリン塩を使用する脱水方法 |
| JP2015168718A (ja) * | 2014-03-05 | 2015-09-28 | 一般財団法人電力中央研究所 | 油脂抽出方法 |
| CN106852158A (zh) * | 2014-07-07 | 2017-06-13 | 联邦科学技术研究组织 | 从植物脂质生产工业产品的方法 |
| JP2017529060A (ja) * | 2014-07-07 | 2017-10-05 | コモンウェルス サイエンティフィック アンド インダストリアル リサーチ オーガナイゼーション | 植物脂質から工業製品を製造する工程 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0254880B2 (enrdf_load_stackoverflow) | 1990-11-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |