JPS6099127A - 熱可塑性ブロツクポリエ−テルエステルアミドの製造法 - Google Patents
熱可塑性ブロツクポリエ−テルエステルアミドの製造法Info
- Publication number
- JPS6099127A JPS6099127A JP59161639A JP16163984A JPS6099127A JP S6099127 A JPS6099127 A JP S6099127A JP 59161639 A JP59161639 A JP 59161639A JP 16163984 A JP16163984 A JP 16163984A JP S6099127 A JPS6099127 A JP S6099127A
- Authority
- JP
- Japan
- Prior art keywords
- ester amide
- polyether ester
- carbon atoms
- block polyether
- molecular weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920006146 polyetheresteramide block copolymer Polymers 0.000 title claims description 27
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 229920001169 thermoplastic Polymers 0.000 title claims description 4
- 239000004416 thermosoftening plastic Substances 0.000 title claims description 4
- 239000003054 catalyst Substances 0.000 claims description 26
- 238000006068 polycondensation reaction Methods 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 19
- 238000005886 esterification reaction Methods 0.000 claims description 16
- 230000032050 esterification Effects 0.000 claims description 15
- 239000004952 Polyamide Substances 0.000 claims description 14
- 229920002647 polyamide Polymers 0.000 claims description 14
- 125000004432 carbon atom Chemical group C* 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 7
- 239000000178 monomer Substances 0.000 claims description 7
- 229920000570 polyether Polymers 0.000 claims description 7
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 6
- 125000001931 aliphatic group Chemical group 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 150000007513 acids Chemical class 0.000 claims description 4
- 125000003118 aryl group Chemical group 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- -1 ether diol Chemical class 0.000 claims description 2
- 150000004820 halides Chemical class 0.000 claims description 2
- 150000007522 mineralic acids Chemical class 0.000 claims description 2
- 125000004430 oxygen atom Chemical group O* 0.000 claims description 2
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 claims 1
- 229920001577 copolymer Polymers 0.000 claims 1
- 150000002009 diols Chemical class 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000007787 solid Substances 0.000 description 11
- 229920000642 polymer Polymers 0.000 description 8
- 239000002245 particle Substances 0.000 description 7
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical group [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- 239000008187 granular material Substances 0.000 description 5
- 239000011261 inert gas Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 4
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 4
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 4
- 230000003197 catalytic effect Effects 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 241000283690 Bos taurus Species 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical compound C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- RLSSMJSEOOYNOY-UHFFFAOYSA-N m-cresol Chemical compound CC1=CC=CC(O)=C1 RLSSMJSEOOYNOY-UHFFFAOYSA-N 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
- 229920006149 polyester-amide block copolymer Polymers 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- XPGAWFIWCWKDDL-UHFFFAOYSA-N propan-1-olate;zirconium(4+) Chemical compound [Zr+4].CCC[O-].CCC[O-].CCC[O-].CCC[O-] XPGAWFIWCWKDDL-UHFFFAOYSA-N 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 229910001887 tin oxide Inorganic materials 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- MRERMGPPCLQIPD-NBVRZTHBSA-N (3beta,5alpha,9alpha,22E,24R)-3,5,9-Trihydroxy-23-methylergosta-7,22-dien-6-one Chemical compound C1C(O)CCC2(C)C(CCC3(C(C(C)/C=C(\C)C(C)C(C)C)CCC33)C)(O)C3=CC(=O)C21O MRERMGPPCLQIPD-NBVRZTHBSA-N 0.000 description 1
- PBLZLIFKVPJDCO-UHFFFAOYSA-N 12-aminododecanoic acid Chemical compound NCCCCCCCCCCCC(O)=O PBLZLIFKVPJDCO-UHFFFAOYSA-N 0.000 description 1
- ASFAFOSQXBRFMV-LJQANCHMSA-N 3-n-(2-benzyl-1,3-dihydroxypropan-2-yl)-1-n-[(1r)-1-(4-fluorophenyl)ethyl]-5-[methyl(methylsulfonyl)amino]benzene-1,3-dicarboxamide Chemical compound N([C@H](C)C=1C=CC(F)=CC=1)C(=O)C(C=1)=CC(N(C)S(C)(=O)=O)=CC=1C(=O)NC(CO)(CO)CC1=CC=CC=C1 ASFAFOSQXBRFMV-LJQANCHMSA-N 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- 241000251730 Chondrichthyes Species 0.000 description 1
- JHWNWJKBPDFINM-UHFFFAOYSA-N Laurolactam Chemical compound O=C1CCCCCCCCCCCN1 JHWNWJKBPDFINM-UHFFFAOYSA-N 0.000 description 1
- 229920002614 Polyether block amide Polymers 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000001361 adipic acid Substances 0.000 description 1
- 235000011037 adipic acid Nutrition 0.000 description 1
- 125000002723 alicyclic group Chemical group 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001786 chalcogen compounds Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000012760 heat stabilizer Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 150000003951 lactams Chemical class 0.000 description 1
- 239000004611 light stabiliser Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- DPBLXKKOBLCELK-UHFFFAOYSA-N pentan-1-amine Chemical class CCCCCN DPBLXKKOBLCELK-UHFFFAOYSA-N 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920000909 polytetrahydrofuran Polymers 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/44—Polyester-amides
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyamides (AREA)
- Polyesters Or Polycarbonates (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH4228/83A CH658062A5 (de) | 1983-08-04 | 1983-08-04 | Verfahren zur herstellung von blockpolyetheresteramiden. |
| CH4228/83-0 | 1983-08-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6099127A true JPS6099127A (ja) | 1985-06-03 |
| JPH0516454B2 JPH0516454B2 (en, 2012) | 1993-03-04 |
Family
ID=4272198
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59161639A Granted JPS6099127A (ja) | 1983-08-04 | 1984-08-02 | 熱可塑性ブロツクポリエ−テルエステルアミドの製造法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4689393A (en, 2012) |
| JP (1) | JPS6099127A (en, 2012) |
| CH (1) | CH658062A5 (en, 2012) |
| DE (1) | DE3428404A1 (en, 2012) |
| FR (1) | FR2550211B1 (en, 2012) |
| GB (1) | GB2144441B (en, 2012) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60170624A (ja) * | 1984-02-14 | 1985-09-04 | Toray Ind Inc | ポリエ−テルエステルアミドの製法 |
| JP2009526890A (ja) * | 2006-02-16 | 2009-07-23 | アルケマ フランス | 機械的特性が改良されたポリアミドブロックとポリエーテルブロックとを有するコポリマー |
| JP2012251145A (ja) * | 2011-06-06 | 2012-12-20 | Xerox Corp | 芳香族末端基をもつアミドゲル化化合物を調製するためのプロセス |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH668600A5 (de) * | 1986-03-20 | 1989-01-13 | Inventa Ag | Verfahren zur herstellung von thermoplastisch verarbeitbaren blockpolyurethanamiden mit durch esterbindung verknuepften polyurethan- und polyamidsegmenten und deren verwendung. |
| CH669678A5 (en, 2012) * | 1986-11-17 | 1989-03-31 | Inventa Ag | |
| FR2639644A1 (fr) * | 1988-11-25 | 1990-06-01 | Atochem | Film elastomere thermoplastique permeable a la vapeur d'eau a base de polyetheresteramide, son procede de fabrication et articles comprenant un tel film |
| DE3917017A1 (de) * | 1989-05-24 | 1990-11-29 | Inventa Ag | Thermoplastisch verarbeitbare elastomere blockcopolyetheresteretheramide, verfahren zu ihrer herstellung und ihre verwendung |
| EP0438579B1 (de) * | 1989-08-09 | 1995-10-25 | Dr. Frische GmbH | Neuartige monomerbausteine aus hydroxyfettsäuren zur herstellung von kunststoffen |
| US5652326A (en) * | 1993-03-03 | 1997-07-29 | Sanyo Chemical Industries, Ltd. | Polyetheresteramide and antistatic resin composition |
| US6673873B1 (en) | 1999-08-25 | 2004-01-06 | Cyro Industries | Electrostatic-dissipative multipolymer compositions |
| RU2630310C1 (ru) * | 2016-11-22 | 2017-09-07 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Юго-Западный государственный университет" (ЮЗГУ) | Способ получения бензоата олова (II) |
| RU2650893C1 (ru) * | 2017-02-28 | 2018-04-18 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Юго-Западный государственный университет" (ЮЗГУ) | Способ получения основного бензоата олова (II) |
| RU2678092C1 (ru) * | 2017-08-17 | 2019-01-23 | Федеральное государственное бюджетное образовательное учреждение высшего образования " Юго-Западный государственный университет" (ЮЗГУ) | Двухстадийный способ получения карбоксилатов олова (II) из металла |
| RU2670199C1 (ru) * | 2017-11-15 | 2018-10-19 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Юго-Западный государственный университет" (ЮЗГУ) | Способ получения карбоксилатов олова (II) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5645419A (en) * | 1979-09-21 | 1981-04-25 | Teijin Yuka Kk | Preparation of p-xylene |
| JPS5790017A (en) * | 1980-11-25 | 1982-06-04 | Toray Ind Inc | Production of polyether-ester-amide |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3057824A (en) * | 1959-03-31 | 1962-10-09 | Pittsburgh Plate Glass Co | Tin salts as catalysts in forming polyesters |
| US3162616A (en) * | 1959-06-10 | 1964-12-22 | Nopco Chem Co | Esterification process |
| US3055869A (en) * | 1959-12-21 | 1962-09-25 | Eastman Kodak Co | Process for preparing polyesters using free acids |
| US3194791A (en) * | 1962-02-23 | 1965-07-13 | Eastman Kodak Co | Tin salts catalysts for polyesterification process |
| GB1137209A (en) * | 1965-04-05 | 1968-12-18 | Eastman Kodak Co | Polyesteramides |
| GB1282422A (en) * | 1968-12-12 | 1972-07-19 | Ici Ltd | New polyester manufacturing process |
| US3546178A (en) * | 1968-12-23 | 1970-12-08 | Eastman Kodak Co | Preparation of linear poly(ester-amides) |
| DE1921738A1 (de) * | 1969-04-29 | 1970-11-12 | Bayer Ag | Polyesteramidelastomere mit Polyaethersegmenten |
| US3716523A (en) * | 1970-10-21 | 1973-02-13 | Basf Wyandotte Corp | Low concentration stannous carboxylate catalysis of polyesterification |
| FR2273021B1 (en, 2012) * | 1974-05-31 | 1977-03-11 | Ato Chimie | |
| FR2307834A1 (fr) * | 1975-04-15 | 1976-11-12 | Ato Chimie | Copolyesteramides sequences comme produits a mouler |
| FR2401947A1 (fr) * | 1977-09-02 | 1979-03-30 | Ato Chimie | Procede de preparation de polyether-ester-amides sequences utilisables, entre autres, comme produits a mouler, a extruder ou a filer |
| FR2418250A1 (fr) * | 1978-02-24 | 1979-09-21 | Ato Chimie | Enveloppe en matiere polymere thermoplastique pour balles de golf et balles de golf comportant une telle enveloppe |
| DE2932234C2 (de) * | 1979-08-09 | 1982-01-28 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur Herstellung von Polyether(ester)amiden |
| DE2936976C2 (de) * | 1979-09-13 | 1986-09-18 | Hüls AG, 4370 Marl | Verfahren zur Herstellung von Polyether(ester)amiden |
| DE2936977C2 (de) * | 1979-09-13 | 1986-06-12 | Hüls AG, 4370 Marl | Verfahren zur Herstellung von Polyether(ester)amiden |
| GB2063279B (en) * | 1979-10-02 | 1984-01-11 | Ato Chimie | Thermoplastic elastomers based on aliphatic copolyetheresteramide blocks of high molecular weight |
| FR2466478B2 (fr) * | 1979-10-02 | 1986-03-14 | Ato Chimie | Procede de preparation de copolyetheresteramides aliphatiques elastomeres |
| JPS6026028A (ja) * | 1983-07-25 | 1985-02-08 | Daicel Chem Ind Ltd | ポリアミドエラストマ−の製造法 |
-
1983
- 1983-08-04 CH CH4228/83A patent/CH658062A5/de not_active IP Right Cessation
-
1984
- 1984-08-01 DE DE19843428404 patent/DE3428404A1/de active Granted
- 1984-08-02 JP JP59161639A patent/JPS6099127A/ja active Granted
- 1984-08-03 FR FR8412371A patent/FR2550211B1/fr not_active Expired
- 1984-08-03 GB GB08419801A patent/GB2144441B/en not_active Expired
-
1986
- 1986-02-13 US US06/829,470 patent/US4689393A/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5645419A (en) * | 1979-09-21 | 1981-04-25 | Teijin Yuka Kk | Preparation of p-xylene |
| JPS5790017A (en) * | 1980-11-25 | 1982-06-04 | Toray Ind Inc | Production of polyether-ester-amide |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60170624A (ja) * | 1984-02-14 | 1985-09-04 | Toray Ind Inc | ポリエ−テルエステルアミドの製法 |
| JP2009526890A (ja) * | 2006-02-16 | 2009-07-23 | アルケマ フランス | 機械的特性が改良されたポリアミドブロックとポリエーテルブロックとを有するコポリマー |
| JP2012251145A (ja) * | 2011-06-06 | 2012-12-20 | Xerox Corp | 芳香族末端基をもつアミドゲル化化合物を調製するためのプロセス |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3428404C2 (en, 2012) | 1990-02-22 |
| DE3428404A1 (de) | 1985-02-21 |
| GB2144441B (en) | 1987-01-28 |
| JPH0516454B2 (en, 2012) | 1993-03-04 |
| US4689393A (en) | 1987-08-25 |
| FR2550211B1 (fr) | 1987-08-21 |
| GB2144441A (en) | 1985-03-06 |
| CH658062A5 (de) | 1986-10-15 |
| FR2550211A1 (fr) | 1985-02-08 |
| GB8419801D0 (en) | 1984-09-05 |
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