JPS6033231A - 球状多孔性ガラスの製造方法 - Google Patents
球状多孔性ガラスの製造方法Info
- Publication number
- JPS6033231A JPS6033231A JP14223183A JP14223183A JPS6033231A JP S6033231 A JPS6033231 A JP S6033231A JP 14223183 A JP14223183 A JP 14223183A JP 14223183 A JP14223183 A JP 14223183A JP S6033231 A JPS6033231 A JP S6033231A
- Authority
- JP
- Japan
- Prior art keywords
- glass
- porous glass
- spherical porous
- treated
- spherical
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000005373 porous glass Substances 0.000 title claims abstract description 41
- 239000011521 glass Substances 0.000 claims abstract description 64
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 37
- 239000000843 powder Substances 0.000 claims abstract description 34
- 239000002245 particle Substances 0.000 claims abstract description 29
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 17
- 239000006229 carbon black Substances 0.000 claims abstract description 6
- 238000002844 melting Methods 0.000 claims abstract description 6
- 230000008018 melting Effects 0.000 claims abstract description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000010438 heat treatment Methods 0.000 claims description 35
- 239000006121 base glass Substances 0.000 claims description 29
- 239000000243 solution Substances 0.000 claims description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 16
- 239000002253 acid Substances 0.000 claims description 14
- 238000004519 manufacturing process Methods 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 239000012670 alkaline solution Substances 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 7
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 3
- 238000010276 construction Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 11
- 239000007788 liquid Substances 0.000 abstract description 7
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 abstract description 5
- 235000012239 silicon dioxide Nutrition 0.000 abstract description 4
- 238000010298 pulverizing process Methods 0.000 abstract description 2
- 238000003466 welding Methods 0.000 abstract description 2
- 229910052681 coesite Inorganic materials 0.000 abstract 3
- 229910052906 cristobalite Inorganic materials 0.000 abstract 3
- 229910052682 stishovite Inorganic materials 0.000 abstract 3
- 229910052905 tridymite Inorganic materials 0.000 abstract 3
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 239000006060 molten glass Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 33
- 238000003756 stirring Methods 0.000 description 15
- 238000005406 washing Methods 0.000 description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 11
- 230000005484 gravity Effects 0.000 description 8
- 238000005191 phase separation Methods 0.000 description 7
- 239000011148 porous material Substances 0.000 description 7
- 238000001035 drying Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 230000000704 physical effect Effects 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 239000004809 Teflon Substances 0.000 description 3
- 229920006362 Teflon® Polymers 0.000 description 3
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 3
- 239000004327 boric acid Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 230000007935 neutral effect Effects 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000000969 carrier Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000000635 electron micrograph Methods 0.000 description 2
- 230000005496 eutectics Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 239000011802 pulverized particle Substances 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000012798 spherical particle Substances 0.000 description 2
- 229910002012 Aerosil® Inorganic materials 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 101100348017 Drosophila melanogaster Nazo gene Proteins 0.000 description 1
- 108010093096 Immobilized Enzymes Proteins 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 239000008119 colloidal silica Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000005227 gel permeation chromatography Methods 0.000 description 1
- 238000005816 glass manufacturing process Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 238000007602 hot air drying Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000003303 reheating Methods 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 238000011172 small scale experimental method Methods 0.000 description 1
- 238000010129 solution processing Methods 0.000 description 1
- 238000005563 spheronization Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 210000001685 thyroid gland Anatomy 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
Landscapes
- Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
- Glass Compositions (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14223183A JPS6033231A (ja) | 1983-08-03 | 1983-08-03 | 球状多孔性ガラスの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14223183A JPS6033231A (ja) | 1983-08-03 | 1983-08-03 | 球状多孔性ガラスの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6033231A true JPS6033231A (ja) | 1985-02-20 |
| JPH0261423B2 JPH0261423B2 (enrdf_load_html_response) | 1990-12-20 |
Family
ID=15310469
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP14223183A Granted JPS6033231A (ja) | 1983-08-03 | 1983-08-03 | 球状多孔性ガラスの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6033231A (enrdf_load_html_response) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63176337A (ja) * | 1987-01-14 | 1988-07-20 | Kirin Brewery Co Ltd | 液体含浸粒状泡硝子 |
| JPH0196043A (ja) * | 1987-10-06 | 1989-04-14 | Kirin Brewery Co Ltd | 粒状泡硝子の物性制御方法及びこの方法により製造された粒状泡硝子 |
| CN112028496A (zh) * | 2020-08-14 | 2020-12-04 | 河北迪纳兴科生物科技有限公司 | 一种用于寡核苷酸合成的纳米多孔玻璃的生产方法 |
| WO2023017772A1 (ja) * | 2021-08-12 | 2023-02-16 | 日本電気硝子株式会社 | 多孔質ガラス粒子及びその製造方法 |
-
1983
- 1983-08-03 JP JP14223183A patent/JPS6033231A/ja active Granted
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63176337A (ja) * | 1987-01-14 | 1988-07-20 | Kirin Brewery Co Ltd | 液体含浸粒状泡硝子 |
| JPH0196043A (ja) * | 1987-10-06 | 1989-04-14 | Kirin Brewery Co Ltd | 粒状泡硝子の物性制御方法及びこの方法により製造された粒状泡硝子 |
| CN112028496A (zh) * | 2020-08-14 | 2020-12-04 | 河北迪纳兴科生物科技有限公司 | 一种用于寡核苷酸合成的纳米多孔玻璃的生产方法 |
| WO2023017772A1 (ja) * | 2021-08-12 | 2023-02-16 | 日本電気硝子株式会社 | 多孔質ガラス粒子及びその製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0261423B2 (enrdf_load_html_response) | 1990-12-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP3241752B2 (ja) | クリストバル石を含まない極めて透水性に優れた仮焼した珪藻土濾過剤の製造方法と、この方法で得られる濾過剤 | |
| US5017523A (en) | Method for the preparation of ultra-fine hollow glass spheres | |
| JPH04219310A (ja) | 非焼結状クリストバライト粒子の製造方法 | |
| JPS6033231A (ja) | 球状多孔性ガラスの製造方法 | |
| JPH06277423A (ja) | 高温用濾材の製法及び使用方法 | |
| US3235635A (en) | Method of preparing perlite products | |
| US3233740A (en) | High flow rate perlite filter aids | |
| JP3115162B2 (ja) | 石英ガラス粉の製造方法 | |
| JPH0316925A (ja) | 高純度溶融石英の製造方法 | |
| JP2670628B2 (ja) | 微細な溶融球状シリカの製造方法 | |
| CN110386608B (zh) | 一种轻质球形二氧化硅的制备方法 | |
| RU2690830C1 (ru) | Способ получения ультрадисперсного порошка диоксида кремния | |
| JP2004237288A (ja) | 人工焼結砂およびその製造方法 | |
| JPH08208272A (ja) | 微細中空ガラス球状体の製造方法 | |
| JPH0280329A (ja) | 合成石英ガラスの製造方法 | |
| JPH07315869A (ja) | 微細中空ガラス球状体の製造方法 | |
| JP2857365B2 (ja) | 微細中空ガラス球状体の製造方法 | |
| JP2733860B2 (ja) | 耐摩耗性シリカメディアの製造法 | |
| JP4822550B2 (ja) | 球状多成分ガラス微粒子 | |
| JP3071363B2 (ja) | 合成石英ガラスの製造方法 | |
| WO1999001521A1 (en) | GRINDING MEDIA CONSISTING ESSENTIALLY OF SINTERED TiO2 PARTICLES | |
| JP7587089B1 (ja) | 多孔質球状シリカ、触媒担体、化粧品、分析カラム、研磨剤、樹脂組成物、および、多孔質球状シリカの製造方法 | |
| JPS61295221A (ja) | セピオライト微粉末の製造方法 | |
| JPH03262504A (ja) | 金属超微粒子から分離液及び金属微粒子の製造方法 | |
| JPH03193619A (ja) | 球状シリカの製造方法 |