JPH01225322A - パーティクルが少ないか又は含まない液化二酸化炭素の供給 - Google Patents

パーティクルが少ないか又は含まない液化二酸化炭素の供給

Info

Publication number
JPH01225322A
JPH01225322A JP63051870A JP5187088A JPH01225322A JP H01225322 A JPH01225322 A JP H01225322A JP 63051870 A JP63051870 A JP 63051870A JP 5187088 A JP5187088 A JP 5187088A JP H01225322 A JPH01225322 A JP H01225322A
Authority
JP
Japan
Prior art keywords
liquefied
gas
particles
filter
wafer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP63051870A
Other languages
English (en)
Other versions
JPH0622224B2 (ja
Inventor
Kozo Moriya
守屋 晃三
Tadashi Okatsu
大勝 正
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Osaka Oxygen Industries Ltd
Original Assignee
Osaka Oxygen Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Osaka Oxygen Industries Ltd filed Critical Osaka Oxygen Industries Ltd
Priority to JP63051870A priority Critical patent/JPH0622224B2/ja
Priority to US07/308,856 priority patent/US4972677A/en
Priority to DE8989302176T priority patent/DE68906293T2/de
Priority to EP89302176A priority patent/EP0332356B1/en
Publication of JPH01225322A publication Critical patent/JPH01225322A/ja
Publication of JPH0622224B2 publication Critical patent/JPH0622224B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02041Cleaning
    • H01L21/02043Cleaning before device manufacture, i.e. Begin-Of-Line process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B7/00Cleaning by methods not provided for in a single other subclass or a single group in this subclass
    • B08B7/0064Cleaning by methods not provided for in a single other subclass or a single group in this subclass by temperature changes
    • B08B7/0092Cleaning by methods not provided for in a single other subclass or a single group in this subclass by temperature changes by cooling
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C7/00Methods or apparatus for discharging liquefied, solidified, or compressed gases from pressure vessels, not covered by another subclass
    • F17C7/02Discharging liquefied gases
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02041Cleaning
    • H01L21/02043Cleaning before device manufacture, i.e. Begin-Of-Line process
    • H01L21/02052Wet cleaning only
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/67005Apparatus not specifically provided for elsewhere
    • H01L21/67011Apparatus for manufacture or treatment
    • H01L21/67017Apparatus for fluid treatment
    • H01L21/67028Apparatus for fluid treatment for cleaning followed by drying, rinsing, stripping, blasting or the like
    • H01L21/6704Apparatus for fluid treatment for cleaning followed by drying, rinsing, stripping, blasting or the like for wet cleaning or washing
    • H01L21/67051Apparatus for fluid treatment for cleaning followed by drying, rinsing, stripping, blasting or the like for wet cleaning or washing using mainly spraying means, e.g. nozzles
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/03Fluid connections, filters, valves, closure means or other attachments
    • F17C2205/0302Fittings, valves, filters, or components in connection with the gas storage device
    • F17C2205/0341Filters
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2221/00Handled fluid, in particular type of fluid
    • F17C2221/01Pure fluids
    • F17C2221/013Carbone dioxide
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/01Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the phase
    • F17C2223/0146Two-phase
    • F17C2223/0153Liquefied gas, e.g. LPG, GPL
    • F17C2223/0161Liquefied gas, e.g. LPG, GPL cryogenic, e.g. LNG, GNL, PLNG
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/03Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the pressure level
    • F17C2223/033Small pressure, e.g. for liquefied gas
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/04Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by other properties of handled fluid before transfer
    • F17C2223/042Localisation of the removal point
    • F17C2223/046Localisation of the removal point in the liquid
    • F17C2223/047Localisation of the removal point in the liquid with a dip tube
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2225/00Handled fluid after transfer, i.e. state of fluid after transfer from the vessel
    • F17C2225/01Handled fluid after transfer, i.e. state of fluid after transfer from the vessel characterised by the phase
    • F17C2225/0146Two-phase
    • F17C2225/0153Liquefied gas, e.g. LPG, GPL
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2225/00Handled fluid after transfer, i.e. state of fluid after transfer from the vessel
    • F17C2225/04Handled fluid after transfer, i.e. state of fluid after transfer from the vessel characterised by other properties of handled fluid after transfer
    • F17C2225/042Localisation of the filling point
    • F17C2225/043Localisation of the filling point in the gas
    • F17C2225/044Localisation of the filling point in the gas at several points, e.g. with a device for recondensing gas
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2227/00Transfer of fluids, i.e. method or means for transferring the fluid; Heat exchange with the fluid
    • F17C2227/03Heat exchange with the fluid
    • F17C2227/0302Heat exchange with the fluid by heating
    • F17C2227/0304Heat exchange with the fluid by heating using an electric heater
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2227/00Transfer of fluids, i.e. method or means for transferring the fluid; Heat exchange with the fluid
    • F17C2227/03Heat exchange with the fluid
    • F17C2227/0337Heat exchange with the fluid by cooling
    • F17C2227/0341Heat exchange with the fluid by cooling using another fluid
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2227/00Transfer of fluids, i.e. method or means for transferring the fluid; Heat exchange with the fluid
    • F17C2227/03Heat exchange with the fluid
    • F17C2227/0367Localisation of heat exchange
    • F17C2227/0388Localisation of heat exchange separate
    • F17C2227/039Localisation of heat exchange separate on the pipes
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2265/00Effects achieved by gas storage or gas handling
    • F17C2265/01Purifying the fluid
    • F17C2265/012Purifying the fluid by filtering

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Cleaning Or Drying Semiconductors (AREA)
  • Cleaning In General (AREA)

Abstract

(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。

Description

【発明の詳細な説明】 発明の分野 本発明は、パーティクルの少ない液化炭酸ガスの供給方
法及びその液化炭酸ガスを使用しての被洗浄物の表面上
のパーティクル、油分等を除去する方法に関する。
発明が解決すべき課題 液化CO□は溶剤としてすぐれた性質を有し、被洗浄物
表面のパーティクル、油分等を容易に除去することがで
きることは知られている。特に半導体工業に使用される
ウェーハーは、表面上に付着しているわずかな量のパー
ティクルを実質上完全に除去する必要がある。
本発明は市販の5ナイン(N)高純度液化COZ中には
以下の表−1に示すような多量のパーティクルが混入し
ていることを発見した。
表   −1 市販5N液化CO2中のパーティクル このようなCO2のドライアイススノーによるウェーハ
ー等洗浄では、パーティクルを除去すると同時にパーテ
ィクルを新たに付着させてしまう為使用できなかった。
課題を解決すべき手段 一般に液化CO2中のパーティクルはフィルターで除去
するのが一般的である。液化CO3を液体のままフィル
ターに通じてみた結果を表−2に示す。すなわち液化C
O2中のパーティクルはフィルターではほとんど除去で
きない。
表   −2 そこで本発明者は液化CO□を蒸発させた後ガス状にて
フィルターを通した結果を表−3に示はパーティクルを
ほぼ100%除去できることを発見した。
表  −3 すなわち液化Co  を−度蒸発させた後CO□ガスと
してフィルターに通じパーティクルをほぼ100%除去
した後、再液化すればパーティクルの少い液化CO2を
得ることが出来る。
本発明は上記発見に基づいてなされた。
本発明は、液化COを蒸発させ、CO□ガスとした後、
そのCO2ガスをフィルターに通しCO2ガス中のパー
ティクルを除去した後、冷却して再液化を行ない、その
パーティクルの少い又はパーティクルを含まない液化C
O2をノズルより噴出させ、微細なドライアイススノー
を含むCO□ガス及び/又は液化CO2を吹きつけるこ
とにより被洗浄物の表面上のパーティクル等を除去する
方法に関する。
本発明の方法を第1図により説明する。第1図にパーテ
ィクルの少い液化炭酸ガスの供給方法を示す。
液化CO3貯槽1よりの液化CO2は蒸発器2によりC
O2ガスとなりフィルター3によりパーティクルを除去
された後、液化器4により再液化されニードル弁5、フ
ィルター6を通りノズル7より噴出され微細なドライア
イススノーとなりウェーハー等上に吹きつけられ、ウェ
ーハー等上のパーティクルを除去する。
フィルター3以後の配管、弁、ノズルはパーティクルの
発生を抑える為、内面が平滑で清浄な電解又は化学研磨
管を使用する。
CO貯槽1の代りに、市販のCO2収用容器(ガス取り
用又は液取り用)を使用しても良い。
本発明において被洗浄物とはウェーハー、コンパクトデ
ィスク、レーザーディスク、レンズ等である。
一般に、ウェーハー等の表面に液体CO2を吹きつける
とウェーハー等に急冷され表面に露かできて、ウェーハ
ー等は水で濡れる。これはこのような水を乾燥するのに
時間がかかり、又このような水分の耐着によってウェー
ハー等の表面が汚れる可能性もある。このような不備を
避けるためにウェーハー等をN2雰囲気の室に置き、液
化CO2を吹きかけても良い。又ウェーハー等を電気ヒ
ーターによって加熱しても良い。上記両方の手段を同時
に採用しても良い。
このパーティクルの少い液化CO2を清浄な容器に充填
し供給すれば同一の目的を達成できるように思われるが
、この場合液化CO2保存タンクの内面を複合電解研磨
した後超純水洗浄をする必要があり、容器の製作に多く
の費用がかかり実際的でない。第1図に示す様にウェー
ハー洗浄を行う現場に液化器4を設置しそのまま液化C
O2を供給すれば費用もかかわらず実際的である。液化
器4を電解研磨管にて製作するのは容易である。
本方法によりウェーハー洗浄等に使用するパーティクル
の少い液化CO2を現場にて安く供給できる。
【図面の簡単な説明】
第1図は本発明方法を実施するための好ましい態様の装
置を示す。 1・・・液化Co  貯槽   2・・・CO3蒸発器
3・・・フィルター     4・・・液化器5・・・
ニードル弁     6・・・フィルター7・・・ノズ
ル 特許出願人 大阪酸素工業株式会社 (外4名)

Claims (1)

  1. 【特許請求の範囲】 1、液化CO_2を蒸発させ、CO_2ガスとした後、
    そのCO_2ガスをフィルターに通しCO_2ガス中の
    パーティクルを除去した後、冷却して再液化することを
    特徴とするパーティクルの少ない又はパーティクルを含
    まない液化CO_2を供給する方法。 2、特許請求の範囲第1項記載のパーティクルの少ない
    又はパーティクルを含まない液化CO_2をノズルより
    噴出させ、ドライアイススノーを含むCO_2ガス及び
    /又は液化CO_2を吹きつけることにより被洗浄物の
    表面上のパーティクル等を除去する方法。 3、その被洗浄物が窒素雰囲気中で保持された状態でド
    ライアイススノーを吹きつける特許請求の範囲第2項記
    載の方法。 4、その被洗浄物が加熱された状態で、ドライアイスス
    ノーを吹きつける特許請求の範囲2又は3項記載の方法
JP63051870A 1988-03-05 1988-03-05 パーティクルが少ないか又は含まない液化二酸化炭素の供給 Expired - Lifetime JPH0622224B2 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP63051870A JPH0622224B2 (ja) 1988-03-05 1988-03-05 パーティクルが少ないか又は含まない液化二酸化炭素の供給
US07/308,856 US4972677A (en) 1988-03-05 1989-02-09 Method of cleaning wafers or the like
DE8989302176T DE68906293T2 (de) 1988-03-05 1989-03-03 Zufuhr von kohlendioxid.
EP89302176A EP0332356B1 (en) 1988-03-05 1989-03-03 Supply of carbon dioxide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP63051870A JPH0622224B2 (ja) 1988-03-05 1988-03-05 パーティクルが少ないか又は含まない液化二酸化炭素の供給

Publications (2)

Publication Number Publication Date
JPH01225322A true JPH01225322A (ja) 1989-09-08
JPH0622224B2 JPH0622224B2 (ja) 1994-03-23

Family

ID=12898914

Family Applications (1)

Application Number Title Priority Date Filing Date
JP63051870A Expired - Lifetime JPH0622224B2 (ja) 1988-03-05 1988-03-05 パーティクルが少ないか又は含まない液化二酸化炭素の供給

Country Status (4)

Country Link
US (1) US4972677A (ja)
EP (1) EP0332356B1 (ja)
JP (1) JPH0622224B2 (ja)
DE (1) DE68906293T2 (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH037984U (ja) * 1989-06-06 1991-01-25
CN112709061A (zh) * 2020-12-22 2021-04-27 抚州市鸿源纺织科技有限公司 一种纺织设备

Families Citing this family (27)

* Cited by examiner, † Cited by third party
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US5179840A (en) * 1989-10-16 1993-01-19 The Boc Group Plc Cryogenic treatment methods
US5062898A (en) * 1990-06-05 1991-11-05 Air Products And Chemicals, Inc. Surface cleaning using a cryogenic aerosol
US5140822A (en) * 1991-02-08 1992-08-25 The Coca-Cola Company Method and apparatus for chilling and carbonating a liquid using liquid carbon dioxide
JP2863663B2 (ja) * 1991-04-18 1999-03-03 大阪酸素工業株式会社 光学式露点計の反射鏡の洗浄方法及び洗浄装置付き光学式露点計
US5482371A (en) * 1991-04-18 1996-01-09 Osaka Sanso Kogyo Ltd. Method and apparatus for measuring the dew point and/or frost point of a gas having low water content
US5470154A (en) * 1991-04-18 1995-11-28 Osaka Sanso Kogyo Ltd. Method of cleaning the reflector mirror in an optical dew point meter and an optical dew point meter equipped with a cleaning device
US5315793A (en) 1991-10-01 1994-05-31 Hughes Aircraft Company System for precision cleaning by jet spray
US5294261A (en) * 1992-11-02 1994-03-15 Air Products And Chemicals, Inc. Surface cleaning using an argon or nitrogen aerosol
US5354384A (en) * 1993-04-30 1994-10-11 Hughes Aircraft Company Method for cleaning surface by heating and a stream of snow
US5931721A (en) * 1994-11-07 1999-08-03 Sumitomo Heavy Industries, Ltd. Aerosol surface processing
US5967156A (en) * 1994-11-07 1999-10-19 Krytek Corporation Processing a surface
FR2747595B1 (fr) * 1996-04-19 1998-08-21 Air Liquide Procede et installation de fourniture d'helium ultra-pur
US5961732A (en) * 1997-06-11 1999-10-05 Fsi International, Inc Treating substrates by producing and controlling a cryogenic aerosol
US6036786A (en) * 1997-06-11 2000-03-14 Fsi International Inc. Eliminating stiction with the use of cryogenic aerosol
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US4972677A (en) 1990-11-27
EP0332356B1 (en) 1993-05-05
EP0332356A3 (en) 1990-04-04
DE68906293D1 (de) 1993-06-09
JPH0622224B2 (ja) 1994-03-23
EP0332356A2 (en) 1989-09-13
DE68906293T2 (de) 1993-08-12

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