JP7818586B2 - 粒子状(オキシ)水酸化物の製造方法、粒子状(オキシ)水酸化物及びその使用方法 - Google Patents

粒子状(オキシ)水酸化物の製造方法、粒子状(オキシ)水酸化物及びその使用方法

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Publication number
JP7818586B2
JP7818586B2 JP2023522780A JP2023522780A JP7818586B2 JP 7818586 B2 JP7818586 B2 JP 7818586B2 JP 2023522780 A JP2023522780 A JP 2023522780A JP 2023522780 A JP2023522780 A JP 2023522780A JP 7818586 B2 JP7818586 B2 JP 7818586B2
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hydroxide
range
oxy
present
particulate
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JP2023550011A (ja
JP2023550011A5 (enExample
Inventor
ベルグナー,ベンヤミン,ヨハネス,ヘルベルト
ベルク,ラファエル,ベンヤミン
ガルフェ,レンナルト,カール,ベルンハルト
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BASF SE
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BASF SE
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/84—Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/05—Hydroxides; Oxyhydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139—Processes of manufacture
    • H01M4/1391—Processes of manufacture of electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/621—Binders
    • H01M4/622—Binders being polymers
    • H01M4/623—Binders being polymers fluorinated polymers
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624—Electric conductive fillers
    • H01M4/625—Carbon or graphite
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C01P2002/54—Solid solutions containing elements as dopants one element only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/53—Particles with a specific particle size distribution bimodal size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/021—Physical characteristics, e.g. porosity, surface area
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
JP2023522780A 2020-10-13 2021-09-16 粒子状(オキシ)水酸化物の製造方法、粒子状(オキシ)水酸化物及びその使用方法 Active JP7818586B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP20201539 2020-10-13
EP20201539.2 2020-10-13
PCT/EP2021/075441 WO2022078702A1 (en) 2020-10-13 2021-09-16 Process for making a particulate (oxy)hydroxide, and particulate (oxy)hydroxide and its use

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JP2023550011A JP2023550011A (ja) 2023-11-30
JP2023550011A5 JP2023550011A5 (enExample) 2024-09-13
JP7818586B2 true JP7818586B2 (ja) 2026-02-20

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US (1) US12570545B2 (enExample)
EP (1) EP4229008B1 (enExample)
JP (1) JP7818586B2 (enExample)
KR (1) KR20230085913A (enExample)
CN (1) CN116157937A (enExample)
CA (1) CA3194883A1 (enExample)
ES (1) ES2988547T3 (enExample)
FI (1) FI4229008T3 (enExample)
PL (1) PL4229008T3 (enExample)
WO (1) WO2022078702A1 (enExample)

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KR102845111B1 (ko) * 2021-07-26 2025-08-12 주식회사 엘 앤 에프 양극 활물질 제조용 전이금속 전구체
CN117003295B (zh) * 2022-04-29 2025-12-12 中伟新材料股份有限公司 一种三元正极材料及其前驱体、锂离子电池
US20260028242A1 (en) * 2022-08-15 2026-01-29 Basf Se Process for making an (oxy)hydroxide, and (oxy)hydroxide
US20260213185A1 (en) * 2023-01-11 2026-07-23 Basf Se Process for making a particulate (oxy)hydroxide or oxide, particulate (oxy)hydroxide or oxide and use
WO2025016808A1 (en) * 2023-07-14 2025-01-23 Basf Se Process for making precursors of cathode active materials, and precursors

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JP2013180917A (ja) 2012-03-01 2013-09-12 Nippon Chem Ind Co Ltd ニッケル含有水酸化物及びその製造方法
JP2014510004A (ja) 2011-01-10 2014-04-24 ビーエーエスエフ ソシエタス・ヨーロピア 遷移金属水酸化物を製造するための方法
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WO2018020845A1 (ja) 2016-07-29 2018-02-01 住友金属鉱山株式会社 ニッケルマンガン複合水酸化物とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、および非水系電解質二次電池
WO2018021555A1 (ja) 2016-07-29 2018-02-01 住友金属鉱山株式会社 ニッケルマンガン複合水酸化物とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、および非水系電解質二次電池
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JP2022519550A (ja) 2019-10-23 2022-03-24 エルジー・ケム・リミテッド 正極活物質前駆体の製造方法および正極活物質前駆体
JP2023513027A (ja) 2020-01-29 2023-03-30 エルジー・ケム・リミテッド 二次電池用正極活物質前駆体、正極活物質およびこれを含むリチウム二次電池

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JP2011501727A (ja) 2007-10-12 2011-01-13 ハー.ツェー.スタルク ゲゼルシャフト ミット ベシュレンクテル ハフツング 粉末状のniambox(oh)y化合物、その製造方法並びにバッテリーにおけるその使用
JP2014510004A (ja) 2011-01-10 2014-04-24 ビーエーエスエフ ソシエタス・ヨーロピア 遷移金属水酸化物を製造するための方法
JP2013180917A (ja) 2012-03-01 2013-09-12 Nippon Chem Ind Co Ltd ニッケル含有水酸化物及びその製造方法
JP2016020283A (ja) 2013-07-18 2016-02-04 東ソー株式会社 ニッケル−マンガン系複合オキシ水酸化物及びその製造方法、並びにその用途
CN104157872A (zh) 2014-08-26 2014-11-19 宁波金和新材料股份有限公司 低成本高容量倍率型镍锰前驱体及其制备方法、正极材料
JP2016117625A (ja) 2014-12-22 2016-06-30 住友金属鉱山株式会社 ニッケルコバルトマンガン複合水酸化物とその製造方法
JP2017178701A (ja) 2016-03-30 2017-10-05 東ソー株式会社 ニッケル−マンガン複合オキシ水酸化物の製造方法
WO2018020845A1 (ja) 2016-07-29 2018-02-01 住友金属鉱山株式会社 ニッケルマンガン複合水酸化物とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、および非水系電解質二次電池
WO2018021555A1 (ja) 2016-07-29 2018-02-01 住友金属鉱山株式会社 ニッケルマンガン複合水酸化物とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、および非水系電解質二次電池
JP2021515966A (ja) 2018-03-02 2021-06-24 ユミコア 充電式リチウムイオン電池用の正極材料
JP2022519550A (ja) 2019-10-23 2022-03-24 エルジー・ケム・リミテッド 正極活物質前駆体の製造方法および正極活物質前駆体
CN112777647A (zh) 2019-11-04 2021-05-11 湖南杉杉能源科技股份有限公司 一种窄粒径分布高镍氢氧化物及其制备方法
JP2023513027A (ja) 2020-01-29 2023-03-30 エルジー・ケム・リミテッド 二次電池用正極活物質前駆体、正極活物質およびこれを含むリチウム二次電池

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CN116157937A (zh) 2023-05-23
ES2988547T3 (es) 2024-11-21
JP2023550011A (ja) 2023-11-30
FI4229008T3 (fi) 2024-10-25
EP4229008A1 (en) 2023-08-23
EP4229008B1 (en) 2024-07-24
US12570545B2 (en) 2026-03-10
PL4229008T3 (pl) 2024-11-25
US20230406722A1 (en) 2023-12-21
CA3194883A1 (en) 2022-04-21
KR20230085913A (ko) 2023-06-14

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