KR20230085913A - 미립자 (옥시)수산화물의 제조 방법, 및 미립자 (옥시)수산화물 및 그 용도 - Google Patents

미립자 (옥시)수산화물의 제조 방법, 및 미립자 (옥시)수산화물 및 그 용도 Download PDF

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Publication number
KR20230085913A
KR20230085913A KR1020237012236A KR20237012236A KR20230085913A KR 20230085913 A KR20230085913 A KR 20230085913A KR 1020237012236 A KR1020237012236 A KR 1020237012236A KR 20237012236 A KR20237012236 A KR 20237012236A KR 20230085913 A KR20230085913 A KR 20230085913A
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South Korea
Prior art keywords
hydroxide
oxy
particulate
present
solution
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Korean (ko)
Inventor
벤야민 요하네스 헤르베르트 베르크너
라파엘 벤야민 베르크
렌나르트 칼 베른하르트 가르페
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바스프 에스이
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    • C01G53/006—
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/84—Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/05—Hydroxides; Oxyhydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139—Processes of manufacture
    • H01M4/1391—Processes of manufacture of electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/621—Binders
    • H01M4/622—Binders being polymers
    • H01M4/623—Binders being polymers fluorinated polymers
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624—Electric conductive fillers
    • H01M4/625—Carbon or graphite
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C01P2002/54—Solid solutions containing elements as dopants one element only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
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    • C—CHEMISTRY; METALLURGY
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    • C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
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    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/021—Physical characteristics, e.g. porosity, surface area
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
KR1020237012236A 2020-10-13 2021-09-16 미립자 (옥시)수산화물의 제조 방법, 및 미립자 (옥시)수산화물 및 그 용도 Pending KR20230085913A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP20201539 2020-10-13
EP20201539.2 2020-10-13
PCT/EP2021/075441 WO2022078702A1 (en) 2020-10-13 2021-09-16 Process for making a particulate (oxy)hydroxide, and particulate (oxy)hydroxide and its use

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Publication Number Publication Date
KR20230085913A true KR20230085913A (ko) 2023-06-14

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Country Link
US (1) US12570545B2 (enExample)
EP (1) EP4229008B1 (enExample)
JP (1) JP7818586B2 (enExample)
KR (1) KR20230085913A (enExample)
CN (1) CN116157937A (enExample)
CA (1) CA3194883A1 (enExample)
ES (1) ES2988547T3 (enExample)
FI (1) FI4229008T3 (enExample)
PL (1) PL4229008T3 (enExample)
WO (1) WO2022078702A1 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102845111B1 (ko) * 2021-07-26 2025-08-12 주식회사 엘 앤 에프 양극 활물질 제조용 전이금속 전구체
CN117003295B (zh) * 2022-04-29 2025-12-12 中伟新材料股份有限公司 一种三元正极材料及其前驱体、锂离子电池
US20260028242A1 (en) * 2022-08-15 2026-01-29 Basf Se Process for making an (oxy)hydroxide, and (oxy)hydroxide
US20260213185A1 (en) * 2023-01-11 2026-07-23 Basf Se Process for making a particulate (oxy)hydroxide or oxide, particulate (oxy)hydroxide or oxide and use
WO2025016808A1 (en) * 2023-07-14 2025-01-23 Basf Se Process for making precursors of cathode active materials, and precursors

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JP3192374B2 (ja) * 1996-07-01 2001-07-23 正同化学工業株式会社 水酸化ニッケルの製造方法
US6660432B2 (en) 2000-09-14 2003-12-09 Ilion Technology Corporation Lithiated oxide materials and methods of manufacture
DE102007049108A1 (de) 2007-10-12 2009-04-16 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Batterien
WO2012095381A2 (de) 2011-01-10 2012-07-19 Basf Se Verfahren zur herstellung von übergangsmetallhydroxiden
KR102057026B1 (ko) 2012-02-08 2019-12-18 바스프 에스이 수산화물(들) 을 함유할 수 있는 혼합 탄산염 제조 방법
JP2013180917A (ja) 2012-03-01 2013-09-12 Nippon Chem Ind Co Ltd ニッケル含有水酸化物及びその製造方法
JP6357928B2 (ja) 2013-07-18 2018-07-18 東ソー株式会社 ニッケル−マンガン系複合オキシ水酸化物及びその製造方法、並びにその用途
TWI636613B (zh) * 2013-07-18 2018-09-21 日商東曹股份有限公司 鎳－錳系複合氧氫氧化物及其製造方法、以及其用途
CN104157873A (zh) 2014-08-04 2014-11-19 北京万源工业有限公司 一种利用聚合反应制备改性磷酸铁锂的方法
CN104157872A (zh) 2014-08-26 2014-11-19 宁波金和新材料股份有限公司 低成本高容量倍率型镍锰前驱体及其制备方法、正极材料
JP6265117B2 (ja) 2014-12-22 2018-01-24 住友金属鉱山株式会社 ニッケルコバルトマンガン複合水酸化物とその製造方法
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Publication number Publication date
WO2022078702A1 (en) 2022-04-21
CN116157937A (zh) 2023-05-23
ES2988547T3 (es) 2024-11-21
JP2023550011A (ja) 2023-11-30
FI4229008T3 (fi) 2024-10-25
EP4229008A1 (en) 2023-08-23
EP4229008B1 (en) 2024-07-24
US12570545B2 (en) 2026-03-10
PL4229008T3 (pl) 2024-11-25
JP7818586B2 (ja) 2026-02-20
US20230406722A1 (en) 2023-12-21
CA3194883A1 (en) 2022-04-21

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