JP6445438B2 - アシルホスファン類の製造方法 - Google Patents

アシルホスファン類の製造方法 Download PDF

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JP6445438B2
JP6445438B2 JP2015533630A JP2015533630A JP6445438B2 JP 6445438 B2 JP6445438 B2 JP 6445438B2 JP 2015533630 A JP2015533630 A JP 2015533630A JP 2015533630 A JP2015533630 A JP 2015533630A JP 6445438 B2 JP6445438 B2 JP 6445438B2
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JP2015532275A (ja
JP2015532275A5 (OSRAM
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ハンスイェルク・グリューツマッハー
ゲオルギーナ・ミュラー
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イーティーエイチ・チューリッヒ
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/53Organo-phosphine oxides; Organo-phosphine thioxides
    • C07F9/5337Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/5036Phosphines containing the structure -C(=X)-P or NC-P
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/505Preparation; Separation; Purification; Stabilisation
    • C07F9/5063Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds
    • C07F9/5072Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds from starting materials having the structure P-H
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/53Organo-phosphine oxides; Organo-phosphine thioxides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C07F9/572Five-membered rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C07F9/576Six-membered rings
    • C07F9/58Pyridine rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/655Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
    • C07F9/65515Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a five-membered ring
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/46Polymerisation initiated by wave energy or particle radiation
    • C08F2/48Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
    • C08F2/50Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light with sensitising agents
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F218/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid or of a haloformic acid
    • C08F218/02Esters of monocarboxylic acids
    • C08F218/04Vinyl esters
    • C08F218/08Vinyl acetate

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Polymerisation Methods In General (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
JP2015533630A 2012-10-01 2013-09-30 アシルホスファン類の製造方法 Active JP6445438B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP12006822 2012-10-01
EP12006822.6 2012-10-01
EP13003616.3 2013-07-18
EP13003616 2013-07-18
PCT/EP2013/070378 WO2014053455A1 (en) 2012-10-01 2013-09-30 A process for the preparation of acylphosphanes

Publications (3)

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JP2015532275A JP2015532275A (ja) 2015-11-09
JP2015532275A5 JP2015532275A5 (OSRAM) 2018-03-08
JP6445438B2 true JP6445438B2 (ja) 2018-12-26

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JP2015533630A Active JP6445438B2 (ja) 2012-10-01 2013-09-30 アシルホスファン類の製造方法

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US (2) US9701700B2 (OSRAM)
EP (2) EP2903995B1 (OSRAM)
JP (1) JP6445438B2 (OSRAM)
KR (1) KR102135300B1 (OSRAM)
CN (2) CN104703995B (OSRAM)
BR (1) BR112015007295B1 (OSRAM)
ES (2) ES2720760T3 (OSRAM)
RU (1) RU2719592C2 (OSRAM)
WO (1) WO2014053455A1 (OSRAM)

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EP3031798B1 (en) 2014-12-10 2017-09-27 Belenos Clean Power Holding AG A novel cross-linker for the preparation of a new family of single ion conduction polymers for electrochemical devices and such polymers
EP3296301A1 (en) * 2016-09-19 2018-03-21 ETH Zürich A versatile process for the preparation of acylphosphines
JP2020500092A (ja) 2016-11-16 2020-01-09 エコール・ポリテクニーク・フェデラル・ドゥ・ローザンヌ (ウ・ペ・エフ・エル)Ecole Polytechnique Federale De Lausanne (Epfl) 光重合性骨充填材材料
EP3409680B1 (en) * 2017-05-30 2021-01-06 IGM Group B.V. Synthesis of bis(acyl)phosphines by activation of unreactive metal phosphides
CN107400144B (zh) * 2017-08-03 2020-04-14 深圳有为技术控股集团有限公司 酰基膦(氧)化合物及其制备方法和应用
EP3539969A1 (en) 2018-03-14 2019-09-18 ETH Zurich Novel photo-initiators and their application
EP3539924A1 (en) 2018-03-14 2019-09-18 ETH Zurich Novel vinyl phosphines and photo-initiators obtainable therefrom
WO2020049378A1 (en) 2018-09-07 2020-03-12 Igm Resins Italia S.R.L. Multifunctional bisacylphosphine oxide photoinitiators
EP3747942A1 (en) 2019-06-05 2020-12-09 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Bridged phosphorus based flame retardants
WO2021095580A1 (ja) 2019-11-11 2021-05-20 富士フイルム株式会社 活性エネルギー線硬化型インク及び画像記録方法
CN115697278B (zh) 2020-05-29 2025-08-19 奥德内股份公司 用于化学稳定的聚合物凝胶的可交联的预聚物
CN112547122A (zh) * 2020-12-18 2021-03-26 商河知济新材料技术中心 叔丁醇盐和吡啶盐在制备一种光引发剂中的用途
WO2024056948A1 (fr) 2022-09-15 2024-03-21 Elkem Silicones France Sas Méthode de fabrication additive pour produire un article en élastomère silicone
CN120365331B (zh) * 2025-06-26 2025-11-04 北京大学深圳研究生院 一种光引发剂及其制备方法

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US2822376A (en) * 1957-02-27 1958-02-04 American Cyanamid Co Reaction of phosphine with alpha, beta-unsatu-rated compounds
TW303379B (OSRAM) * 1994-03-02 1997-04-21 Ciba Sc Holding Ag
RU2141962C1 (ru) * 1994-07-29 1999-11-27 Пферси Хеми ГмбХ Способ получения диэфиров производных фосфонкарбоновых кислот
SG53043A1 (en) 1996-08-28 1998-09-28 Ciba Geigy Ag Molecular complex compounds as photoinitiators
SK286152B6 (sk) 1998-11-30 2008-04-07 Ciba Specialty Chemicals Holding Inc. Spôsob prípravy acylfosfínov, acylfosfínoxidov a acylfosfínsulfidov
JP2001200007A (ja) * 2000-01-19 2001-07-24 Shin Etsu Chem Co Ltd 光硬化性樹脂組成物及び光ファイバー用被覆材
GB2360283B (en) * 2000-02-08 2002-08-21 Ciba Sc Holding Ag Monoacylarylphosphines and acylphosphine oxides and sulphides
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JP2003228150A (ja) * 2002-02-04 2003-08-15 Konica Corp 光熱写真画像形成材料
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ES2720760T3 (es) 2019-07-24
EP3508489A1 (en) 2019-07-10
KR102135300B1 (ko) 2020-08-27
JP2015532275A (ja) 2015-11-09
US20150299231A1 (en) 2015-10-22
BR112015007295A2 (pt) 2017-07-04
KR20150064747A (ko) 2015-06-11
BR112015007295B1 (pt) 2021-12-14
EP3508489B1 (en) 2021-04-14
CN108383874B (zh) 2021-10-08
CN108383874A (zh) 2018-08-10
RU2719592C2 (ru) 2020-04-21
US10273258B2 (en) 2019-04-30
RU2015116292A (ru) 2016-11-27
EP2903995A1 (en) 2015-08-12
WO2014053455A1 (en) 2014-04-10
ES2881686T3 (es) 2021-11-30
US20180002357A1 (en) 2018-01-04
EP2903995B1 (en) 2019-01-16
CN104703995A (zh) 2015-06-10
US9701700B2 (en) 2017-07-11
CN104703995B (zh) 2018-04-20

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