JP6189413B2 - ハシゴ状シルセスキオキサン高分子を含む光学フィルム用樹脂組成物 - Google Patents
ハシゴ状シルセスキオキサン高分子を含む光学フィルム用樹脂組成物 Download PDFInfo
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- JP6189413B2 JP6189413B2 JP2015503110A JP2015503110A JP6189413B2 JP 6189413 B2 JP6189413 B2 JP 6189413B2 JP 2015503110 A JP2015503110 A JP 2015503110A JP 2015503110 A JP2015503110 A JP 2015503110A JP 6189413 B2 JP6189413 B2 JP 6189413B2
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- optical film
- cellulose
- resin composition
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- Prior art date
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- 239000012788 optical film Substances 0.000 title claims description 42
- 229920000642 polymer Polymers 0.000 title claims description 39
- 239000011342 resin composition Substances 0.000 title claims description 34
- 239000010408 film Substances 0.000 claims description 48
- 229920002678 cellulose Polymers 0.000 claims description 27
- 239000001913 cellulose Substances 0.000 claims description 27
- 239000012461 cellulose resin Substances 0.000 claims description 20
- 125000003118 aryl group Chemical group 0.000 claims description 16
- 125000000524 functional group Chemical group 0.000 claims description 15
- -1 alkyl halogen Chemical class 0.000 claims description 13
- 239000011347 resin Substances 0.000 claims description 12
- 229920005989 resin Polymers 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 11
- 230000003287 optical effect Effects 0.000 claims description 11
- 238000002834 transmittance Methods 0.000 claims description 11
- 125000000217 alkyl group Chemical group 0.000 claims description 9
- 125000003545 alkoxy group Chemical group 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 229910052736 halogen Inorganic materials 0.000 claims description 6
- 230000001681 protective effect Effects 0.000 claims description 6
- 229920002284 Cellulose triacetate Polymers 0.000 claims description 5
- NNLVGZFZQQXQNW-ADJNRHBOSA-N [(2r,3r,4s,5r,6s)-4,5-diacetyloxy-3-[(2s,3r,4s,5r,6r)-3,4,5-triacetyloxy-6-(acetyloxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6s)-4,5,6-triacetyloxy-2-(acetyloxymethyl)oxan-3-yl]oxyoxan-2-yl]methyl acetate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](OC(C)=O)[C@H]1OC(C)=O)O[C@H]1[C@@H]([C@@H](OC(C)=O)[C@H](OC(C)=O)[C@@H](COC(C)=O)O1)OC(C)=O)COC(=O)C)[C@@H]1[C@@H](COC(C)=O)O[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]1OC(C)=O NNLVGZFZQQXQNW-ADJNRHBOSA-N 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 239000001257 hydrogen Substances 0.000 claims description 5
- 150000002431 hydrogen Chemical class 0.000 claims description 5
- 239000006097 ultraviolet radiation absorber Substances 0.000 claims description 5
- 125000006376 (C3-C10) cycloalkyl group Chemical group 0.000 claims description 4
- 125000003277 amino group Chemical group 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- 125000004122 cyclic group Chemical group 0.000 claims description 4
- 125000003700 epoxy group Chemical group 0.000 claims description 4
- 230000035699 permeability Effects 0.000 claims description 4
- 125000003396 thiol group Chemical group [H]S* 0.000 claims description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 4
- ODIGIKRIUKFKHP-UHFFFAOYSA-N (n-propan-2-yloxycarbonylanilino) acetate Chemical compound CC(C)OC(=O)N(OC(C)=O)C1=CC=CC=C1 ODIGIKRIUKFKHP-UHFFFAOYSA-N 0.000 claims description 3
- 230000008859 change Effects 0.000 claims description 3
- 239000004014 plasticizer Substances 0.000 claims description 3
- 239000000758 substrate Substances 0.000 claims description 3
- 125000003161 (C1-C6) alkylene group Chemical group 0.000 claims description 2
- 229920008347 Cellulose acetate propionate Polymers 0.000 claims description 2
- 125000005529 alkyleneoxy group Chemical group 0.000 claims description 2
- 229920006217 cellulose acetate butyrate Polymers 0.000 claims description 2
- 238000006482 condensation reaction Methods 0.000 claims description 2
- 239000013538 functional additive Substances 0.000 claims description 2
- 230000003301 hydrolyzing effect Effects 0.000 claims description 2
- 229920002554 vinyl polymer Polymers 0.000 claims description 2
- 239000002981 blocking agent Substances 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
- 239000000243 solution Substances 0.000 description 14
- 230000015572 biosynthetic process Effects 0.000 description 13
- 238000000034 method Methods 0.000 description 13
- 238000003786 synthesis reaction Methods 0.000 description 13
- 238000004519 manufacturing process Methods 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 230000000694 effects Effects 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 8
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 7
- 229910000077 silane Inorganic materials 0.000 description 7
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- 230000000903 blocking effect Effects 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- 230000000704 physical effect Effects 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- 230000000996 additive effect Effects 0.000 description 5
- ONTODYXHFBKCDK-UHFFFAOYSA-N 2-(2,4-dimethylphenyl)-1,3,5-triazine Chemical compound CC1=CC(C)=CC=C1C1=NC=NC=N1 ONTODYXHFBKCDK-UHFFFAOYSA-N 0.000 description 4
- 239000000178 monomer Substances 0.000 description 4
- 229920003023 plastic Polymers 0.000 description 4
- 239000004033 plastic Substances 0.000 description 4
- WGTYBPLFGIVFAS-UHFFFAOYSA-M tetramethylammonium hydroxide Chemical compound [OH-].C[N+](C)(C)C WGTYBPLFGIVFAS-UHFFFAOYSA-M 0.000 description 4
- 239000012153 distilled water Substances 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 description 2
- XDLMVUHYZWKMMD-UHFFFAOYSA-N 3-trimethoxysilylpropyl 2-methylprop-2-enoate Chemical compound CO[Si](OC)(OC)CCCOC(=O)C(C)=C XDLMVUHYZWKMMD-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000005033 Fourier transform infrared spectroscopy Methods 0.000 description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 239000007810 chemical reaction solvent Substances 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 239000012046 mixed solvent Substances 0.000 description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- ZNOCGWVLWPVKAO-UHFFFAOYSA-N trimethoxy(phenyl)silane Chemical compound CO[Si](OC)(OC)C1=CC=CC=C1 ZNOCGWVLWPVKAO-UHFFFAOYSA-N 0.000 description 2
- HPFMMFGKGWOEPG-UHFFFAOYSA-N 2-(benzotriazol-2-yl)-4-(2,4,4-trimethylpentan-2-yl)phenol Chemical compound OC1=C(C=C(C=C1)C(C)(C)CC(C)(C)C)N1N=C2C(=N1)C=CC=C2.OC2=C(C=C(C=C2)C(CC(C)(C)C)(C)C)N2N=C1C(=N2)C=CC=C1 HPFMMFGKGWOEPG-UHFFFAOYSA-N 0.000 description 1
- UZUNCLSDTUBVCN-UHFFFAOYSA-N 2-(benzotriazol-2-yl)-6-(2-phenylpropan-2-yl)-4-(2,4,4-trimethylpentan-2-yl)phenol Chemical compound C=1C(C(C)(C)CC(C)(C)C)=CC(N2N=C3C=CC=CC3=N2)=C(O)C=1C(C)(C)C1=CC=CC=C1 UZUNCLSDTUBVCN-UHFFFAOYSA-N 0.000 description 1
- UHGULLIUJBCTEF-UHFFFAOYSA-N 2-aminobenzothiazole Chemical compound C1=CC=C2SC(N)=NC2=C1 UHGULLIUJBCTEF-UHFFFAOYSA-N 0.000 description 1
- RBROWEJWZCQIMP-UHFFFAOYSA-N 2-tert-butyl-6-(5-chlorobenzotriazol-2-yl)-4-methylphenol Chemical compound CC(C)(C)C1=CC(C)=CC(N2N=C3C=C(Cl)C=CC3=N2)=C1O.CC(C)(C)C1=CC(C)=CC(N2N=C3C=C(Cl)C=CC3=N2)=C1O RBROWEJWZCQIMP-UHFFFAOYSA-N 0.000 description 1
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- 238000012935 Averaging Methods 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 235000010724 Wisteria floribunda Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 230000002902 bimodal effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000032798 delamination Effects 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 238000005227 gel permeation chromatography Methods 0.000 description 1
- 238000007602 hot air drying Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 230000031700 light absorption Effects 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- DMFXLIFZVRXRRR-UHFFFAOYSA-N octyl 3-[3-tert-butyl-5-(5-chlorobenzotriazol-2-yl)-4-hydroxyphenyl]propanoate Chemical compound CC(C)(C)C1=CC(CCC(=O)OCCCCCCCC)=CC(N2N=C3C=C(Cl)C=CC3=N2)=C1O DMFXLIFZVRXRRR-UHFFFAOYSA-N 0.000 description 1
- 239000002952 polymeric resin Substances 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000000807 solvent casting Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000004528 spin coating Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000010977 unit operation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/18—Manufacture of films or sheets
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L1/00—Compositions of cellulose, modified cellulose or cellulose derivatives
- C08L1/08—Cellulose derivatives
- C08L1/10—Esters of organic acids, i.e. acylates
- C08L1/12—Cellulose acetate
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/30—Polarising elements
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Optics & Photonics (AREA)
- General Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Polarising Elements (AREA)
- Silicon Polymers (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR10-2012-0031146 | 2012-03-27 | ||
| KR20120031146 | 2012-03-27 | ||
| KR1020130023227A KR102004493B1 (ko) | 2012-03-27 | 2013-03-05 | 사다리형 실세스퀴옥산 고분자를 포함하는 광학필름용 수지 조성물 |
| KR10-2013-0023227 | 2013-03-05 | ||
| PCT/KR2013/002043 WO2013147443A1 (ko) | 2012-03-27 | 2013-03-14 | 사다리형 실세스퀴옥산 고분자를 포함하는 광학필름용 수지 조성물 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2015518502A JP2015518502A (ja) | 2015-07-02 |
| JP6189413B2 true JP6189413B2 (ja) | 2017-08-30 |
Family
ID=49632049
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015503110A Active JP6189413B2 (ja) | 2012-03-27 | 2013-03-14 | ハシゴ状シルセスキオキサン高分子を含む光学フィルム用樹脂組成物 |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JP6189413B2 (zh) |
| KR (1) | KR102004493B1 (zh) |
| CN (1) | CN104220531B (zh) |
| TW (1) | TWI616487B (zh) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102367120B1 (ko) * | 2014-02-28 | 2022-02-25 | 주식회사 동진쎄미켐 | 표면강화 투명기판 및 이의 제조방법 |
| WO2015130146A1 (ko) * | 2014-02-28 | 2015-09-03 | 주식회사 동진쎄미켐 | 표면강화 투명기판 및 이의 제조방법 |
| KR102363819B1 (ko) * | 2014-02-28 | 2022-02-17 | 주식회사 동진쎄미켐 | 실세스퀴옥산 복합 고분자 및 이의 제조방법 |
| KR102325278B1 (ko) * | 2014-03-07 | 2021-11-16 | 주식회사 동진쎄미켐 | 실세스퀴옥산 복합 고분자를 포함하는 열가소성 수지 조성물 |
| KR101698868B1 (ko) * | 2014-11-06 | 2017-01-24 | (주)다솜뜰 | 생분해성 고분자 필름 및 이의 제조방법 |
| WO2016122191A1 (ko) * | 2015-01-26 | 2016-08-04 | 주식회사 동진쎄미켐 | 코팅제품 및 고경도 곡면 하드코팅 방법 |
| JP2020514465A (ja) * | 2016-12-30 | 2020-05-21 | ドンジン セミケム カンパニー リミテッドＤｏｎｇｊｉｎ Ｓｅｍｉｃｈｅｍ Ｃｏ．， Ｌｔｄ． | コーティング組成物およびこれから製造されるフィルム |
| US11628998B2 (en) * | 2018-12-13 | 2023-04-18 | Johnson & Johnson Vision Care, Inc. | Ultraviolet light inhibiting contact lens package |
| KR102554549B1 (ko) * | 2020-12-11 | 2023-07-12 | 엔씨케이 주식회사 | 유기발광소자 오버코트용 저굴절률 조성물 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20000063142A (ko) * | 2000-02-17 | 2000-11-06 | 이응찬 | 폴리오르가노실세스키옥산 제조용 출발물질,폴리오르가노실세스키옥산 및 폴리오르가노실세스키옥산제조방법 |
| JP2006096806A (ja) | 2004-09-28 | 2006-04-13 | Fuji Photo Film Co Ltd | セルロースアシレートフィルム並びにそれを用いた光学フィルム、画像表示装置 |
| JP4945892B2 (ja) * | 2004-11-11 | 2012-06-06 | コニカミノルタオプト株式会社 | 有機無機ハイブリッド材料の製造方法 |
| JP2007204611A (ja) * | 2006-02-02 | 2007-08-16 | Kri Inc | シルセスキオキサン含有セルロース誘導体樹脂組成物 |
| JP5275589B2 (ja) * | 2007-08-02 | 2013-08-28 | 日本曹達株式会社 | シルセスキオキサンを含有する組成物及びシルセスキオキサン含有ヒドロキシアルキルセルロース樹脂組成物 |
| CN101747573B (zh) * | 2008-12-22 | 2011-07-06 | 财团法人工业技术研究院 | 聚乙烯醇膜组合物及包含其的偏光板 |
| TW201038681A (en) * | 2009-02-17 | 2010-11-01 | Nippon Steel Chemical Co | Polarizing plate having a silicone coated hardened film and a liquid crystal display device |
| JP5814512B2 (ja) * | 2009-03-31 | 2015-11-17 | キヤノン株式会社 | 光学用部材、その製造方法及び光学系 |
| CN101906231B (zh) * | 2009-06-02 | 2012-07-04 | 财团法人工业技术研究院 | 聚乙烯醇膜组合物及包含其的偏光板 |
| JP5616147B2 (ja) * | 2010-07-05 | 2014-10-29 | 株式会社カネカ | オルガノポリシロキサン系組成物および、それを用いてなる光学デバイス。 |
-
2013
- 2013-03-05 KR KR1020130023227A patent/KR102004493B1/ko active IP Right Grant
- 2013-03-14 JP JP2015503110A patent/JP6189413B2/ja active Active
- 2013-03-14 TW TW102109039A patent/TWI616487B/zh active
- 2013-03-14 CN CN201380017528.3A patent/CN104220531B/zh active Active
Also Published As
| Publication number | Publication date |
|---|---|
| KR20130110018A (ko) | 2013-10-08 |
| CN104220531B (zh) | 2018-08-14 |
| KR102004493B1 (ko) | 2019-07-26 |
| TWI616487B (zh) | 2018-03-01 |
| JP2015518502A (ja) | 2015-07-02 |
| CN104220531A (zh) | 2014-12-17 |
| TW201343791A (zh) | 2013-11-01 |
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