JP5734920B2 - 水性ベース塗料組成物及びそれを用いた複層塗膜形成方法 - Google Patents

水性ベース塗料組成物及びそれを用いた複層塗膜形成方法 Download PDF

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JP5734920B2
JP5734920B2 JP2012143576A JP2012143576A JP5734920B2 JP 5734920 B2 JP5734920 B2 JP 5734920B2 JP 2012143576 A JP2012143576 A JP 2012143576A JP 2012143576 A JP2012143576 A JP 2012143576A JP 5734920 B2 JP5734920 B2 JP 5734920B2
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resin
coating film
acid
coating
paint
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JP2013060577A (ja
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陽平 小山
陽平 小山
聡一 森
聡一 森
久之 中嶋
久之 中嶋
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BASF Japan Ltd
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BASF Japan Ltd
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D151/00—Coating compositions based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Coating compositions based on derivatives of such polymers
    • C09D151/08—Coating compositions based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Coating compositions based on derivatives of such polymers grafted on to macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/50—Multilayers
    • B05D7/56—Three layers or more
    • B05D7/57—Three layers or more the last layer being a clear coat
    • B05D7/572—Three layers or more the last layer being a clear coat all layers being cured or baked together
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F283/00—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G
    • C08F283/006—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G on to polymers provided for in C08G18/00
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F287/00—Macromolecular compounds obtained by polymerising monomers on to block polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
    • C08G18/0819—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups
    • C08G18/0823—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups containing carboxylate salt groups or groups forming them
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/34—Carboxylic acids; Esters thereof with monohydroxyl compounds
    • C08G18/348—Hydroxycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4205—Polycondensates having carboxylic or carbonic ester groups in the main chain containing cyclic groups
    • C08G18/4208—Polycondensates having carboxylic or carbonic ester groups in the main chain containing cyclic groups containing aromatic groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4205—Polycondensates having carboxylic or carbonic ester groups in the main chain containing cyclic groups
    • C08G18/4208—Polycondensates having carboxylic or carbonic ester groups in the main chain containing cyclic groups containing aromatic groups
    • C08G18/4211—Polycondensates having carboxylic or carbonic ester groups in the main chain containing cyclic groups containing aromatic groups derived from aromatic dicarboxylic acids and dialcohols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
    • C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
    • C08G18/6633—Compounds of group C08G18/42
    • C08G18/6659—Compounds of group C08G18/42 with compounds of group C08G18/34
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/75—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic
    • C08G18/751—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic containing only one cycloaliphatic ring
    • C08G18/752—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic containing only one cycloaliphatic ring containing at least one isocyanate or isothiocyanate group linked to the cycloaliphatic ring by means of an aliphatic group
    • C08G18/753—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic containing only one cycloaliphatic ring containing at least one isocyanate or isothiocyanate group linked to the cycloaliphatic ring by means of an aliphatic group containing one isocyanate or isothiocyanate group linked to the cycloaliphatic ring by means of an aliphatic group having a primary carbon atom next to the isocyanate or isothiocyanate group
    • C08G18/755—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic containing only one cycloaliphatic ring containing at least one isocyanate or isothiocyanate group linked to the cycloaliphatic ring by means of an aliphatic group containing one isocyanate or isothiocyanate group linked to the cycloaliphatic ring by means of an aliphatic group having a primary carbon atom next to the isocyanate or isothiocyanate group and at least one isocyanate or isothiocyanate group linked to a secondary carbon atom of the cycloaliphatic ring, e.g. isophorone diisocyanate
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04—Homopolymers or copolymers of esters
    • C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09D133/062—Copolymers with monomers not covered by C09D133/06
    • C09D133/066—Copolymers with monomers not covered by C09D133/06 containing -OH groups
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04—Homopolymers or copolymers of esters
    • C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09D133/10—Homopolymers or copolymers of methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04—Polyurethanes
    • C09D175/06—Polyurethanes from polyesters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Paints Or Removers (AREA)
  • Laminated Bodies (AREA)
JP2012143576A 2011-08-22 2012-06-26 水性ベース塗料組成物及びそれを用いた複層塗膜形成方法 Active JP5734920B2 (ja)

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JP2012143576A JP5734920B2 (ja) 2011-08-22 2012-06-26 水性ベース塗料組成物及びそれを用いた複層塗膜形成方法
PCT/EP2013/060480 WO2014000983A1 (en) 2012-06-26 2013-05-22 Aqueous base paint composition and a method of forming a multi-layer paint film using same

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JP2011180650 2011-08-22
JP2011180650 2011-08-22
JP2012143576A JP5734920B2 (ja) 2011-08-22 2012-06-26 水性ベース塗料組成物及びそれを用いた複層塗膜形成方法

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JP2014253290A Active JP5995948B2 (ja) 2011-08-22 2014-12-15 水性ベース塗料組成物及びそれを用いた複層塗膜形成方法

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US (1) US10100220B2 (enExample)
EP (1) EP2748215B1 (enExample)
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WO2017162475A1 (en) 2016-03-22 2017-09-28 Basf Coatings Gmbh Method of forming a multilayer coating film

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JP6067006B2 (ja) * 2012-05-24 2017-01-25 関西ペイント株式会社 水性塗料組成物、複層塗膜形成方法及び複層塗膜を有する物品
WO2014000983A1 (en) * 2012-06-26 2014-01-03 Basf Coatings Gmbh Aqueous base paint composition and a method of forming a multi-layer paint film using same
JP6155738B2 (ja) * 2013-03-22 2017-07-05 セイコーエプソン株式会社 流路ユニット、液体噴射ヘッド、液体噴射装置、及び、流路ユニットの製造方法
JP6104028B2 (ja) 2013-04-17 2017-03-29 Ｂａｓｆジャパン株式会社 複層塗膜形成方法
CN105451824A (zh) * 2013-06-07 2016-03-30 涂层国外知识产权有限公司 喷枪及喷涂方法
CN105555823B (zh) * 2013-08-07 2019-12-20 日本涂料树脂株式会社 聚氨酯、氨基甲酸酯－(甲基)丙烯酸复合树脂及氨基甲酸酯－(甲基)丙烯酸复合树脂水性分散液
JPWO2015107933A1 (ja) * 2014-01-15 2017-03-23 Dic株式会社 水性表面処理剤及びそれを用いた物品
JP2015139925A (ja) * 2014-01-28 2015-08-03 三菱樹脂株式会社 積層ポリエステルフィルム
US20150267077A1 (en) * 2014-03-19 2015-09-24 Ppg Industries Ohio, Inc. Coated metal substrates and methods of preparing them
JP6254970B2 (ja) * 2015-03-31 2017-12-27 株式会社Ｓｕｂａｒｕ 積層塗膜の形成方法
US11554385B2 (en) 2015-11-17 2023-01-17 Ppg Industries Ohio, Inc. Coated substrates prepared with waterborne sealer and primer compositions
US10870765B2 (en) 2015-12-28 2020-12-22 Nippon Paint Automotive Coatings Co., Ltd. Aqueous coating composition and method for forming a coating film
US10695793B2 (en) 2016-01-27 2020-06-30 Nippon Paint Automotive Coatings Co., Ltd. Method for forming multilayer coating film
JP2019056020A (ja) * 2016-01-27 2019-04-11 日本ペイント・オートモーティブコーティングス株式会社 水性塗料組成物
US10696866B2 (en) 2016-01-27 2020-06-30 Nippon Paint Automotive Coatings Co., Ltd. Method for forming multilayer coating film
KR101857857B1 (ko) 2016-01-29 2018-05-15 주식회사 케이씨씨 자동차 중도용 수용성 도료 조성물 및 이를 이용한 자동차 도장 방법
EP3430067B1 (de) * 2016-03-14 2022-05-11 BASF Coatings GmbH Hydroxyfunktionelle polyether-basierte reaktionsprodukte und wässrige basislacke enthaltend die reaktionsprodukte
CN105885666B (zh) * 2016-04-18 2018-06-05 广东工业大学 一种耐黄变高胶膜硬度的水性聚氨酯乳液及其制备方法
CN106046967A (zh) * 2016-07-18 2016-10-26 天长市巨龙车船涂料有限公司 一种注塑塑料件表面自干面漆
WO2018177731A1 (en) * 2017-03-31 2018-10-04 Basf Coatings Gmbh Method for forming multilayer coating film
US10865326B2 (en) * 2017-09-20 2020-12-15 Ppg Industries Ohio, Inc. Coating compositions, elastic barrier coatings formed therefrom, and methods of applying such coatings
US11015084B2 (en) 2017-09-20 2021-05-25 Ppg Industries Ohio, Inc. Coating compositions and elastic barrier coatings formed therefrom
JP6700340B2 (ja) * 2018-06-27 2020-05-27 日本ペイント・オートモーティブコーティングス株式会社 水性塗料組成物および水性塗料組成物の製造方法
JP7106389B2 (ja) * 2018-08-10 2022-07-26 三井化学株式会社 複層膜の製造方法、および、複層膜
US10829664B2 (en) 2019-03-15 2020-11-10 Ppg Industries Ohio, Inc. Coating compositions containing polythioethers and elastic barrier coatings formed therefrom
US10836924B2 (en) 2019-03-15 2020-11-17 Ppg Industries Ohio, Inc. Coating compositions and elastic barrier coatings formed therefrom
CN113874447A (zh) 2019-04-26 2021-12-31 巴斯夫涂料有限公司 水性涂料组合物及使用所述组合物形成多层涂膜的方法
CN114222794A (zh) * 2019-05-13 2022-03-22 Ppg工业俄亥俄公司 涂料组合物以及施加此类涂料组合物的系统和方法
CN110655857B (zh) * 2019-11-05 2022-03-18 立邦涂料（中国）有限公司 一种适用于湿喷湿工艺的水性色漆及其应用
CN113061228B (zh) * 2020-01-02 2022-07-12 万华化学集团股份有限公司 包覆碳黑粒子的交联聚氨酯微球的制备方法及聚氨酯微球及其应用
WO2021172485A1 (ja) * 2020-02-28 2021-09-02 三洋化成工業株式会社 ポリウレタン樹脂水性分散体
CN111825825B (zh) * 2020-06-23 2022-08-05 深圳飞扬骏研新材料股份有限公司 一种紫外光固化水性树脂、制备方法以及使用方法
US20220064476A1 (en) * 2020-08-31 2022-03-03 Axalta Coating Systems Ip Co., Llc Top Coat Composition
JP7472001B2 (ja) 2020-11-13 2024-04-22 日産自動車株式会社 複層塗膜形成方法
CA3240686A1 (en) * 2021-12-14 2023-06-22 Ramanathan S. Lalgudi Bio-based polyols, esters, and surfactants
CN114197212B (zh) * 2022-01-30 2023-11-10 苏州大学 一种水性聚氨酯乳化改性环氧树脂硬挺剂及其制备方法

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US10703934B2 (en) 2016-03-22 2020-07-07 Basf Coatings Gmbh Method of forming a multilayer coating film

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US20180022955A1 (en) 2018-01-25
JP2013060577A (ja) 2013-04-04
CN103608371A (zh) 2014-02-26
EP2748215B1 (en) 2017-03-22
EP2748215A1 (en) 2014-07-02
WO2013027093A1 (en) 2013-02-28

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