JP5624989B2 - 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法 - Google Patents

合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法 Download PDF

Info

Publication number
JP5624989B2
JP5624989B2 JP2011533307A JP2011533307A JP5624989B2 JP 5624989 B2 JP5624989 B2 JP 5624989B2 JP 2011533307 A JP2011533307 A JP 2011533307A JP 2011533307 A JP2011533307 A JP 2011533307A JP 5624989 B2 JP5624989 B2 JP 5624989B2
Authority
JP
Japan
Prior art keywords
reaction
scheme
compound
synthesis
formula
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2011533307A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012506447A (ja
JP2012506447A5 (enExample
Inventor
トンプソン，アンドリュー
チャン，ションジ
ロバージュ，ロニー
Original Assignee
ステラ エルエルシー
ステラ エルエルシー
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ステラ エルエルシー, ステラ エルエルシー filed Critical ステラ エルエルシー
Publication of JP2012506447A publication Critical patent/JP2012506447A/ja
Publication of JP2012506447A5 publication Critical patent/JP2012506447A5/ja
Application granted granted Critical
Publication of JP5624989B2 publication Critical patent/JP5624989B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/42—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrolysis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/44—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by addition reactions, i.e. reactions involving at least one carbon-to-carbon double or triple bond
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/58—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by elimination of halogen, e.g. by hydrogenolysis, splitting-off
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/48—Preparation of compounds having groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/48—Preparation of compounds having groups
    • C07C41/50—Preparation of compounds having groups by reactions producing groups
    • C07C41/56—Preparation of compounds having groups by reactions producing groups by condensation of aldehydes, paraformaldehyde, or ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/511—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups
    • C07C45/515—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups the singly bound functional group being an acetalised, ketalised hemi-acetalised, or hemi-ketalised hydroxyl group

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2011533307A 2008-10-22 2009-10-21 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法 Active JP5624989B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/255,951 US7737306B2 (en) 2008-10-22 2008-10-22 Synthetic navel orangeworm pheromone composition and methods relating to production of same
US12/255,951 2008-10-22
PCT/US2009/061535 WO2010048327A1 (en) 2008-10-22 2009-10-21 Synthetic navel orangeworm pheromone composition and methods relating to production of same

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2014118813A Division JP2014208666A (ja) 2008-10-22 2014-06-09 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法

Publications (3)

Publication Number Publication Date
JP2012506447A JP2012506447A (ja) 2012-03-15
JP2012506447A5 JP2012506447A5 (enExample) 2012-12-06
JP5624989B2 true JP5624989B2 (ja) 2014-11-12

Family

ID=42109201

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2011533307A Active JP5624989B2 (ja) 2008-10-22 2009-10-21 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法
JP2014118813A Pending JP2014208666A (ja) 2008-10-22 2014-06-09 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2014118813A Pending JP2014208666A (ja) 2008-10-22 2014-06-09 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法

Country Status (5)

Country Link
US (6) US7737306B2 (enExample)
JP (2) JP5624989B2 (enExample)
CN (1) CN102203039B (enExample)
AR (1) AR075287A1 (enExample)
WO (1) WO2010048327A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014208666A (ja) * 2008-10-22 2014-11-06 ステラ エルエルシー 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100206521A1 (en) * 2009-02-17 2010-08-19 Aacotek Company Limited Heat dissipating fin and heat sink
US9181164B1 (en) * 2014-05-29 2015-11-10 Suterra, Llc Method of preparing Z-alkene-containing insect pheromones
CN105198695A (zh) * 2014-06-30 2015-12-30 乐威（泰州）医药化学品有限公司 1-卤代-1-炔烃的制备方法
CN104130091B (zh) * 2014-07-16 2016-01-20 中美华世通生物医药科技（武汉）有限公司 还原二炔类化合物的方法
CN105622698B (zh) * 2014-10-27 2020-02-18 天津金耀集团有限公司 一种甾体11位酮基氧化合成新工艺
JP6208161B2 (ja) * 2015-02-06 2017-10-04 信越化学工業株式会社 非対称共役ジイン化合物の製造方法及びこれを用いたｚ，ｚ−共役ジエン化合物の製造方法
CN106431878A (zh) * 2016-09-08 2017-02-22 中美华世通生物医药科技（武汉）有限公司 纯化10‑氯癸醛的方法
CN110885284A (zh) * 2019-10-31 2020-03-17 苏州诚和医药化学有限公司 一种2-溴丙二醛合成方法

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4070184A (en) * 1976-09-24 1978-01-24 Gte Sylvania Incorporated Process for producing refractory carbide grade powder
US4198533A (en) * 1979-02-26 1980-04-15 Zoecon Corporation (11Z,13Z)-11,13-Hexadecadien-1-ol and derivatives
US4228093A (en) * 1979-10-18 1980-10-14 Zoecon Corporation (11Z,13Z)-11,13-Hexadecadiyn-1-ol and (11Z,13Z)-11,13-hexadecadien-1-ol and trimethylsilyl ethers thereof
US4400550A (en) * 1982-02-12 1983-08-23 Albany International Corp. Synthesis of the navel orange worm pheromone (Z,Z)-11,13-hexadecadienal
ATE67066T1 (de) * 1985-03-15 1991-09-15 Immanuel J Wilk Verfahren und vorrichtungen zur gesteuerten freisetzung.
US4760198A (en) * 1985-11-08 1988-07-26 Exfluor Research Corporation 1:1 copolymer of difluoromethylene oxide and tetrafluoroethylene oxide and synthesis
JPS62265240A (ja) * 1986-05-12 1987-11-18 Shin Etsu Chem Co Ltd カルボン酸の還元方法
JPH0737400B2 (ja) * 1988-04-12 1995-04-26 信越化学工業株式会社 １−ハロー（ｚ，ｅ）−７，１０−ドデカジエンおよびその製造方法
JPH07116075B2 (ja) * 1988-06-06 1995-12-13 信越化学工業株式会社 不飽和アルコール化合物の製造方法
JP2528972B2 (ja) * 1989-09-19 1996-08-28 信越化学工業株式会社 アルキニル化合物の連続製造方法
JP2735397B2 (ja) * 1991-02-19 1998-04-02 信越化学工業株式会社 Ｚ−１２−ヘプタデセン−１−イン
JP2798324B2 (ja) * 1992-07-03 1998-09-17 信越化学工業株式会社 害虫防除方法
US6001346A (en) * 1993-02-25 1999-12-14 The Regents Of The University Of California Aqueous emulsion comprising biodegradable carrier for insect pheromones and methods for controlled release thereof
EP0630877B1 (en) * 1993-06-21 1997-03-12 Shin-Etsu Chemical Co., Ltd. Workup of Wittig reaction products
JP3356495B2 (ja) * 1993-07-20 2002-12-16 信越化学工業株式会社 １−ハロ−シス−３−テトラデセンおよびこれを用いるシス−オレフィン化合物の製造方法
JP3340517B2 (ja) * 1993-07-21 2002-11-05 信越化学工業株式会社 シス−アルケニル化合物からトランス体の製造方法
JP3467307B2 (ja) * 1994-03-31 2003-11-17 信越化学工業株式会社 ホスホニウム塩の製造方法
DE69504277T2 (de) * 1994-11-04 1999-01-07 Nitto Denko Corp., Ibaraki, Osaka Material zur Störung der Kommunikation von Insekten
CN1047378C (zh) * 1996-07-01 1999-12-15 北京工业大学 一种棉铃虫性信息激素的合成方法
JP4139448B2 (ja) * 1996-08-13 2008-08-27 信越化学工業株式会社 α−ブロモ，ω−クロロアルカンの製造方法
DE69836318T2 (de) * 1997-09-05 2007-05-24 Shin-Etsu Chemical Co., Ltd. Kommunikationsstörende mittel und verfahren zur kommunikationsstörung
JPH11192676A (ja) * 1997-12-26 1999-07-21 Kyoraku Co Ltd 布貼り成形品およびその再処理方法
US6986854B2 (en) * 1997-12-26 2006-01-17 Kyoraku Co. Ltd. Molded article laminated with fabric and method for reprocessing the same
US6562331B1 (en) * 1999-08-13 2003-05-13 Shin-Etsu Chemical Co., Ltd. Mating disruption methods for the control of insect pests
US6264939B1 (en) * 1999-10-21 2001-07-24 The United States Of America, As Represented By The Secretary Of Agriculture Bisexual attractants, aggregants and arrestants for adults and larvae of codling moth and other species of lepidoptera
US7655253B2 (en) * 2004-11-24 2010-02-02 Bedoukian Research, Inc. Navel orangeworm pheromone composition
US20060110420A1 (en) * 2004-11-24 2006-05-25 The Regents Of The University Of California Synthetic pheromone compositions
US7737306B2 (en) * 2008-10-22 2010-06-15 Suterra, Llc Synthetic navel orangeworm pheromone composition and methods relating to production of same

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014208666A (ja) * 2008-10-22 2014-11-06 ステラ エルエルシー 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法

Also Published As

Publication number Publication date
US8115035B2 (en) 2012-02-14
JP2012506447A (ja) 2012-03-15
US20150197474A1 (en) 2015-07-16
AR075287A1 (es) 2011-03-23
CN102203039A (zh) 2011-09-28
US20110098508A1 (en) 2011-04-28
WO2010048327A1 (en) 2010-04-29
US9233901B2 (en) 2016-01-12
US20120142972A1 (en) 2012-06-07
US20100099920A1 (en) 2010-04-22
US8940942B2 (en) 2015-01-27
US8648216B2 (en) 2014-02-11
JP2014208666A (ja) 2014-11-06
US7737306B2 (en) 2010-06-15
WO2010048327A4 (en) 2010-06-17
CN102203039B (zh) 2014-12-17
US8329957B2 (en) 2012-12-11
US20130144086A1 (en) 2013-06-06
US20140206906A1 (en) 2014-07-24

Similar Documents

Publication Publication Date Title
JP5624989B2 (ja) 合成ネーブルオレンジ虫のフェロモン組成物および同一物の生産に関連する方法
WO2009141053A1 (de) Herstellung von cf3o-gruppen enthaltenden verbindungen
US20120116113A1 (en) PROCESS FOR MAKING NEO-ENRICHED p-MENTHANE COMPOUNDS
Capella et al. Silylcupration-mediated Synthesis of 2-substituted Allylamines
JP5680009B2 (ja) ５−アセトキシ−（ｅ３）−３−ペンテニル−メトキシメチルエーテルを用いた（ｅ３）−３−アルケニルアセタートの製造方法
TWI739789B (zh) 製備經取代的２－芳基乙醇之方法
CN115490589B (zh) 马铃薯块茎蛾性诱剂的合成方法
JP5664779B2 (ja) ヘキサフルオロアセトンまたはその水和物の製造法
Beier et al. An efficient and highly selective synthesis of (z)-fluoroenol phosphates from hydroxy difluorophosphonates
CN101932545A (zh) 取代的环己烯酮
JP2011140474A (ja) ジフルオロシクロプロパン化合物の製造方法
Hill et al. Grignard Reagents and Unsaturated Ethers. II. 1 Reaction of Grignard Reagents with β, γ-Unsaturated Ethers2
Baharfar et al. The novel one-pot synthesis of functionalized vinyl sulfides using triphenylphosphine catalyzed nucleophilic addition of thiols to acetylenes
CN106631686A (zh) 一种β‑苯乙醇的制备方法
ES2914058T3 (es) Proceso para preparar 4-penten-2-inal
JP4786267B2 (ja) ラクトンの製造方法及び製造されたラクトンの芳香物質としての用途
ES2922573T3 (es) Compuesto dialcoxialcadienino y un proceso para preparar el mismo y un proceso para preparar un compuesto dieninal
JP3825489B2 (ja) 不飽和ハロゲン化合物およびそれを用いた性フェロモンの製造方法
WO2018154244A1 (fr) Procédé de synthèse de phéromones
JP5573079B2 (ja) ３−メルカプト−１−プロパノールの製造方法
KR101019787B1 (ko) 칸타잔틴의 제조방법
JP3634874B2 (ja) トリフルオロメチルアセチレン誘導体、その製造方法およびその中間体の製造方法
JP2003040819A (ja) アセチレンアルコールの製造方法
Andreica et al. Convenient Synthesis of (Z)-7-and (E)-9-dodecene-1-yl Acetate, Components of Some Lepidoptera Insect Sex Pheromone
JP2005179270A (ja) ピラン化合物の製造法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20121019

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20121019

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20131023

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20131029

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20140117

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20140210

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20140609

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20140724

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20140814

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20140902

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20140929

R150 Certificate of patent or registration of utility model

Ref document number: 5624989

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250