JP5507544B2 - 酢酸に富むフラッシュ流を与えるメタノールをカルボニル化するための方法及び装置 - Google Patents

酢酸に富むフラッシュ流を与えるメタノールをカルボニル化するための方法及び装置 Download PDF

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JP5507544B2
JP5507544B2 JP2011507417A JP2011507417A JP5507544B2 JP 5507544 B2 JP5507544 B2 JP 5507544B2 JP 2011507417 A JP2011507417 A JP 2011507417A JP 2011507417 A JP2011507417 A JP 2011507417A JP 5507544 B2 JP5507544 B2 JP 5507544B2
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reaction mixture
temperature
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crude product
carbonylation
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JP2011518880A (ja
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パット，ジェレミー・ジェイ
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セラニーズ・インターナショナル・コーポレーション
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06—Flash distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B01J14/005—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L3/00—Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
    • B01L3/06—Crystallising dishes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/445—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by steam distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08—Acetic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00193—Sensing a parameter
    • B01J2219/00195—Sensing a parameter of the reaction system
    • B01J2219/00202—Sensing a parameter of the reaction system at the reactor outlet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00211—Control algorithm comparing a sensed parameter with a pre-set value
    • B01J2219/00213—Fixed parameter value
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00222—Control algorithm taking actions
    • B01J2219/00227—Control algorithm taking actions modifying the operating conditions
    • B01J2219/0024—Control algorithm taking actions modifying the operating conditions other than of the reactor or heat exchange system
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/822—Rhodium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/827—Iridium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0231—Halogen-containing compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/20—Carbonyls

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Clinical Laboratory Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
JP2011507417A 2008-04-29 2009-04-23 酢酸に富むフラッシュ流を与えるメタノールをカルボニル化するための方法及び装置 Active JP5507544B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/150,481 US7820855B2 (en) 2008-04-29 2008-04-29 Method and apparatus for carbonylating methanol with acetic acid enriched flash stream
US12/150,481 2008-04-29
PCT/US2009/002506 WO2009134333A1 (en) 2008-04-29 2009-04-23 Method and apparatus for carbonylating methanol with acetic acid enriched flash stream

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JP2011518880A JP2011518880A (ja) 2011-06-30
JP2011518880A5 JP2011518880A5 (enExample) 2012-03-01
JP5507544B2 true JP5507544B2 (ja) 2014-05-28

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US (7) US7820855B2 (enExample)
EP (2) EP3002057B1 (enExample)
JP (1) JP5507544B2 (enExample)
KR (1) KR20110003555A (enExample)
CN (1) CN102015088B (enExample)
AR (1) AR074141A1 (enExample)
AU (1) AU2009241844A1 (enExample)
BR (1) BRPI0911487B1 (enExample)
CA (1) CA2721922C (enExample)
CL (1) CL2009001003A1 (enExample)
DE (1) DE09739136T1 (enExample)
ES (2) ES2365906T3 (enExample)
MX (3) MX2010011852A (enExample)
NZ (1) NZ588701A (enExample)
RU (1) RU2508162C2 (enExample)
SG (1) SG190600A1 (enExample)
TW (1) TW200946493A (enExample)
WO (1) WO2009134333A1 (enExample)
ZA (2) ZA201007491B (enExample)

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ES2365906T3 (es) 2017-11-30
US8987512B2 (en) 2015-03-24
NZ588701A (en) 2012-03-30
EP2323755B1 (en) 2017-07-26
CL2009001003A1 (es) 2010-06-04
TW200946493A (en) 2009-11-16
US20150175516A1 (en) 2015-06-25
US20130058842A1 (en) 2013-03-07
DE09739136T1 (de) 2012-01-19
US10118885B2 (en) 2018-11-06
BRPI0911487B1 (pt) 2018-02-06
SG190600A1 (en) 2013-06-28
JP2011518880A (ja) 2011-06-30
AU2009241844A1 (en) 2009-11-05
US20140323760A1 (en) 2014-10-30
ZA201102114B (en) 2012-01-25
US20180065911A1 (en) 2018-03-08
ES2694014T3 (es) 2018-12-17
CN102015088A (zh) 2011-04-13
WO2009134333A1 (en) 2009-11-05
RU2010148399A (ru) 2012-06-10
US8771616B2 (en) 2014-07-08
ZA201007491B (en) 2012-01-25
MX364125B (es) 2019-04-12
US9840451B2 (en) 2017-12-12
EP3002057B1 (en) 2018-10-24
US20190062249A1 (en) 2019-02-28
ES2365906T1 (es) 2011-10-13
CA2721922C (en) 2013-09-24
HK1156560A1 (en) 2012-06-15
EP2323755A1 (en) 2011-05-25
EP3002057A1 (en) 2016-04-06
US20110021817A1 (en) 2011-01-27
US20090270650A1 (en) 2009-10-29
BRPI0911487A2 (pt) 2016-01-05
AR074141A1 (es) 2010-12-29
CN102015088B (zh) 2014-06-11
MX2010011852A (es) 2010-12-02
CA2721922A1 (en) 2009-11-05
US10519089B2 (en) 2019-12-31
MX338852B (es) 2016-05-02
RU2508162C2 (ru) 2014-02-27
KR20110003555A (ko) 2011-01-12
US8329944B2 (en) 2012-12-11
US7820855B2 (en) 2010-10-26

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