JP2011518880A5 - - Google Patents
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- Publication number
- JP2011518880A5 JP2011518880A5 JP2011507417A JP2011507417A JP2011518880A5 JP 2011518880 A5 JP2011518880 A5 JP 2011518880A5 JP 2011507417 A JP2011507417 A JP 2011507417A JP 2011507417 A JP2011507417 A JP 2011507417A JP 2011518880 A5 JP2011518880 A5 JP 2011518880A5
- Authority
- JP
- Japan
- Prior art keywords
- reaction mixture
- crude product
- stream
- temperature
- carbonylation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 33
- 239000011541 reaction mixture Substances 0.000 claims 30
- 230000006315 carbonylation Effects 0.000 claims 22
- 238000005810 carbonylation reaction Methods 0.000 claims 22
- 238000000034 method Methods 0.000 claims 21
- 239000012043 crude product Substances 0.000 claims 19
- 239000007788 liquid Substances 0.000 claims 10
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 9
- 239000003054 catalyst Substances 0.000 claims 9
- INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 claims 7
- 229910052751 metal Inorganic materials 0.000 claims 6
- 239000002184 metal Substances 0.000 claims 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 6
- XMBWDFGMSWQBCA-UHFFFAOYSA-M iodide Chemical compound [I-] XMBWDFGMSWQBCA-UHFFFAOYSA-M 0.000 claims 5
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims 4
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 claims 4
- 238000011010 flushing procedure Methods 0.000 claims 3
- 238000010438 heat treatment Methods 0.000 claims 2
- 150000004694 iodide salts Chemical class 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- 239000012264 purified product Substances 0.000 claims 2
- 229910052703 rhodium Inorganic materials 0.000 claims 2
- 239000010948 rhodium Substances 0.000 claims 2
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 1
- 229910052741 iridium Inorganic materials 0.000 claims 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 claims 1
- 239000003446 ligand Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000002243 precursor Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/150,481 US7820855B2 (en) | 2008-04-29 | 2008-04-29 | Method and apparatus for carbonylating methanol with acetic acid enriched flash stream |
| US12/150,481 | 2008-04-29 | ||
| PCT/US2009/002506 WO2009134333A1 (en) | 2008-04-29 | 2009-04-23 | Method and apparatus for carbonylating methanol with acetic acid enriched flash stream |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011518880A JP2011518880A (ja) | 2011-06-30 |
| JP2011518880A5 true JP2011518880A5 (enExample) | 2012-03-01 |
| JP5507544B2 JP5507544B2 (ja) | 2014-05-28 |
Family
ID=41018460
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011507417A Active JP5507544B2 (ja) | 2008-04-29 | 2009-04-23 | 酢酸に富むフラッシュ流を与えるメタノールをカルボニル化するための方法及び装置 |
Country Status (19)
| Country | Link |
|---|---|
| US (7) | US7820855B2 (enExample) |
| EP (2) | EP3002057B1 (enExample) |
| JP (1) | JP5507544B2 (enExample) |
| KR (1) | KR20110003555A (enExample) |
| CN (1) | CN102015088B (enExample) |
| AR (1) | AR074141A1 (enExample) |
| AU (1) | AU2009241844A1 (enExample) |
| BR (1) | BRPI0911487B1 (enExample) |
| CA (1) | CA2721922C (enExample) |
| CL (1) | CL2009001003A1 (enExample) |
| DE (1) | DE09739136T1 (enExample) |
| ES (2) | ES2365906T3 (enExample) |
| MX (3) | MX2010011852A (enExample) |
| NZ (1) | NZ588701A (enExample) |
| RU (1) | RU2508162C2 (enExample) |
| SG (1) | SG190600A1 (enExample) |
| TW (1) | TW200946493A (enExample) |
| WO (1) | WO2009134333A1 (enExample) |
| ZA (2) | ZA201007491B (enExample) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7820855B2 (en) | 2008-04-29 | 2010-10-26 | Celanese International Corporation | Method and apparatus for carbonylating methanol with acetic acid enriched flash stream |
| KR101020844B1 (ko) * | 2008-09-04 | 2011-03-09 | 삼성전기주식회사 | 구리 나노입자의 저온 환원 소결을 위한 환원제 및 이를이용한 저온 소결 방법 |
| CN102093198B (zh) * | 2009-12-15 | 2012-12-05 | 上海吴泾化工有限公司 | 一种生产乙酸的方法 |
| CN102093196B (zh) * | 2009-12-15 | 2013-03-06 | 上海吴泾化工有限公司 | 一种链烷醇和/或其活性衍生物的羰基化制备羧酸的方法 |
| US8877963B2 (en) * | 2010-09-28 | 2014-11-04 | Celanese International Corporation | Production of acetic acid with high conversion rate |
| US8394988B2 (en) | 2010-09-28 | 2013-03-12 | Celanese International Corporation | Production of acetic acid with high conversion rate |
| US8637698B2 (en) * | 2010-11-19 | 2014-01-28 | Celanese International Corporation | Production of acetic acid with an increased production rate |
| MY161174A (en) | 2010-12-15 | 2017-04-14 | Daicel Corp | Process for producing acetic acid |
| WO2012081417A1 (ja) | 2010-12-15 | 2012-06-21 | 株式会社ダイセル | 酢酸の製造方法 |
| US9663437B2 (en) | 2011-09-13 | 2017-05-30 | Celanese International Corporation | Production of acetic acid with high conversion rate |
| BR112013007324B1 (pt) * | 2012-02-08 | 2020-10-20 | Celanese International Corporation | produção de ácido acético com alta taxa de conversão |
| TWI547477B (zh) * | 2012-03-14 | 2016-09-01 | 大賽璐股份有限公司 | 醋酸之製造方法 |
| AR094541A1 (es) * | 2013-01-25 | 2015-08-12 | Daicel Corp | Procedimiento para producir ácido carboxílico |
| US9340481B1 (en) | 2014-11-14 | 2016-05-17 | Celanese International Corporation | Process for flashing a reaction medium comprising lithium acetate |
| US9302975B1 (en) | 2015-07-01 | 2016-04-05 | Celanese International Corporation | Process for flashing a reaction medium |
| ES2773602T3 (es) * | 2014-11-14 | 2020-07-13 | Celanese Int Corp | Procedimiento de vaporización instantánea de un medio de reacción que comprende acetato de litio |
| US9540303B2 (en) | 2015-04-01 | 2017-01-10 | Celanese International Corporation | Processes for producing acetic acid |
| US9382186B1 (en) | 2015-07-01 | 2016-07-05 | Celanese International Corporation | Process for producing acetic acid |
| US9382183B1 (en) | 2015-07-01 | 2016-07-05 | Celanese International Corporation | Process for flashing a reaction medium |
| US9302974B1 (en) | 2015-07-01 | 2016-04-05 | Celanese International Corporation | Process for producing acetic acid |
| WO2017057142A1 (ja) * | 2015-09-30 | 2017-04-06 | 株式会社ダイセル | 酢酸の製造方法及び製造装置 |
| US9416088B1 (en) | 2015-10-02 | 2016-08-16 | Celanese International Corporation | Process to produce acetic acid with recycle of water |
| WO2018163448A1 (ja) * | 2017-03-08 | 2018-09-13 | 株式会社ダイセル | 酢酸の製造方法 |
| US10457622B2 (en) | 2017-03-08 | 2019-10-29 | Daicel Corporation | Method for producing acetic acid |
| CN110191874A (zh) * | 2017-03-28 | 2019-08-30 | 株式会社大赛璐 | 乙酸的制备方法 |
| US10308581B2 (en) | 2017-03-28 | 2019-06-04 | Daicel Corporation | Method for producing acetic acid |
| CN111646894B (zh) * | 2019-09-10 | 2021-12-10 | 上海浦景化工技术股份有限公司 | 一种低压甲醇羰基化合成醋酸的方法 |
| GB202015833D0 (en) | 2020-10-06 | 2020-11-18 | Bp Chem Int Ltd | Separation process and apparatus |
| CN117120408B (zh) * | 2021-04-02 | 2024-05-07 | 利安德巴塞尔乙酰有限责任公司 | 用于生产乙酸的方法和系统 |
Family Cites Families (51)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3769329A (en) | 1970-03-12 | 1973-10-30 | Monsanto Co | Production of carboxylic acids and esters |
| SU791735A1 (ru) * | 1977-07-27 | 1980-12-30 | Ереванский ордена Трудового Красного Знамени государственный университет | Способ очистки соли карбоновой кислоты |
| NL8204901A (nl) | 1981-12-30 | 1983-07-18 | Halcon Sd Group Inc | Zuivering van carbonyleringsprodukten. |
| US5144068A (en) * | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5026908A (en) * | 1984-05-03 | 1991-06-25 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5001259A (en) * | 1984-05-03 | 1991-03-19 | Hoechst Celanese Corporation | Methanol carbonylation process |
| JP2839367B2 (ja) * | 1989-04-06 | 1998-12-16 | ビーピー ケミカルズ リミテッド | カルボン酸類の製造方法 |
| US4976947A (en) * | 1990-02-20 | 1990-12-11 | Eastman Kodak Company | Process for the recovery of elemental iodine from alkyl iodides |
| GB9120902D0 (en) * | 1991-10-02 | 1991-11-13 | Bp Chem Int Ltd | Purification process |
| US5334755A (en) | 1992-04-24 | 1994-08-02 | Chiyoda Corporation | Process for the production of acetic acid from methanol and carbon monoxide using supported rhodium catalyst |
| GB9211671D0 (en) * | 1992-06-02 | 1992-07-15 | Bp Chem Int Ltd | Process |
| CN1043525C (zh) | 1992-08-13 | 1999-06-02 | 化学工业部西南化工研究院 | 甲醇低压液相羰基合成醋酸反应方法 |
| GB9306409D0 (en) * | 1993-03-26 | 1993-05-19 | Bp Chem Int Ltd | Process |
| US5672743A (en) | 1993-09-10 | 1997-09-30 | Bp Chemicals Limited | Process for the production of acetic acid |
| US5990347A (en) * | 1993-03-26 | 1999-11-23 | Bp Chemicals Limited | Process for preparing a carboxylic acid |
| US5352415A (en) | 1993-09-29 | 1994-10-04 | Hoechst Celanese Corporation | Control system for acetic acid manufacturing process |
| JP3308392B2 (ja) * | 1994-06-02 | 2002-07-29 | ダイセル化学工業株式会社 | カルボニル化反応方法 |
| JP3306227B2 (ja) | 1994-07-06 | 2002-07-24 | ダイセル化学工業株式会社 | 酢酸および／または無水酢酸の製造法 |
| JP3413536B2 (ja) | 1994-06-20 | 2003-06-03 | 石川島播磨重工業株式会社 | 液圧駆動型水中音源装置 |
| FR2726556B1 (fr) * | 1994-11-04 | 1996-12-20 | Rhone Poulenc Chimie | Procede de preparation d'acides carboxyliques par carbonylation en presence d'iridium |
| GB9503385D0 (en) * | 1995-02-21 | 1995-04-12 | Bp Chem Int Ltd | Process |
| DE69609796T2 (de) * | 1995-04-27 | 2000-12-28 | Daicel Chem | Verfahren zur herstellung von essigsäure |
| US5696284A (en) * | 1995-06-21 | 1997-12-09 | Bp Chemicals Limited | Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof |
| GB9517184D0 (en) | 1995-08-22 | 1995-10-25 | Bp Chem Int Ltd | Process |
| IN189249B (enExample) * | 1995-10-27 | 2003-01-18 | Hoechst Celanese Corp | |
| IN192600B (enExample) | 1996-10-18 | 2004-05-08 | Hoechst Celanese Corp | |
| GB9625335D0 (en) * | 1996-12-05 | 1997-01-22 | Bp Chem Int Ltd | Process |
| GB9626317D0 (en) * | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626429D0 (en) * | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626428D0 (en) * | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626324D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| SG65716A1 (en) * | 1996-12-30 | 1999-06-22 | Chiyoda Chem Eng Construct Co | Process for the production of carbonyl compound |
| US6114576A (en) * | 1997-12-18 | 2000-09-05 | Uop Llc | Carbonylation process with integrated heat exchange |
| US6153792A (en) * | 1997-12-18 | 2000-11-28 | Uop Llc | Carbonylation process using a flash step with washing |
| JP4242952B2 (ja) | 1998-08-31 | 2009-03-25 | ダイセル化学工業株式会社 | 酢酸の製造方法 |
| US6552221B1 (en) | 1998-12-18 | 2003-04-22 | Millenium Petrochemicals, Inc. | Process control for acetic acid manufacture |
| US6221405B1 (en) | 1999-05-11 | 2001-04-24 | Jac Pac Foods, Ltd. | Method of bonding and tenderizing meat |
| US6303813B1 (en) | 1999-08-31 | 2001-10-16 | Celanese International Corporation | Rhodium/inorganic iodide catalyst system for methanol carbonylation process with improved impurity profile |
| US6627770B1 (en) * | 2000-08-24 | 2003-09-30 | Celanese International Corporation | Method and apparatus for sequesting entrained and volatile catalyst species in a carbonylation process |
| US6657078B2 (en) * | 2001-02-07 | 2003-12-02 | Celanese International Corporation | Low energy carbonylation process |
| US7005541B2 (en) | 2002-12-23 | 2006-02-28 | Celanese International Corporation | Low water methanol carbonylation process for high acetic acid production and for water balance control |
| JP4489487B2 (ja) | 2004-04-02 | 2010-06-23 | ダイセル化学工業株式会社 | ヨウ化水素の分離方法 |
| JP4732743B2 (ja) | 2004-12-06 | 2011-07-27 | ダイセル化学工業株式会社 | 蒸留方法 |
| US7855306B2 (en) | 2005-04-28 | 2010-12-21 | Celanese International Corporation | Process for the production of acetic acid |
| EP2093209A1 (en) * | 2008-02-19 | 2009-08-26 | BP Chemicals Limited | Process for the production of acetic acid |
| US7820855B2 (en) * | 2008-04-29 | 2010-10-26 | Celanese International Corporation | Method and apparatus for carbonylating methanol with acetic acid enriched flash stream |
| EA019325B1 (ru) | 2008-06-28 | 2014-02-28 | Претиум Венчез Аа, Ллс | Композиции для получения карбоновой кислоты, способы их получения и применение |
| US7790920B2 (en) | 2008-09-11 | 2010-09-07 | Lyondell Chemical Technology, L.P. | Preparation of acetic acid |
| US8637699B2 (en) | 2011-04-15 | 2014-01-28 | Lyondell Chemical Technology, L.P. | Process for the manufacture of acetic acid |
| JP5802550B2 (ja) | 2011-12-28 | 2015-10-28 | 株式会社東芝 | 水位計測装置 |
| TWI547477B (zh) | 2012-03-14 | 2016-09-01 | 大賽璐股份有限公司 | 醋酸之製造方法 |
-
2008
- 2008-04-29 US US12/150,481 patent/US7820855B2/en active Active
-
2009
- 2009-04-08 TW TW098111613A patent/TW200946493A/zh unknown
- 2009-04-23 CN CN200980115410.8A patent/CN102015088B/zh active Active
- 2009-04-23 MX MX2010011852A patent/MX2010011852A/es active IP Right Grant
- 2009-04-23 WO PCT/US2009/002506 patent/WO2009134333A1/en not_active Ceased
- 2009-04-23 SG SG2013032586A patent/SG190600A1/en unknown
- 2009-04-23 BR BRPI0911487-4A patent/BRPI0911487B1/pt active IP Right Grant
- 2009-04-23 AU AU2009241844A patent/AU2009241844A1/en not_active Abandoned
- 2009-04-23 EP EP15002793.6A patent/EP3002057B1/en active Active
- 2009-04-23 ES ES09739136.1T patent/ES2365906T3/es active Active
- 2009-04-23 CA CA2721922A patent/CA2721922C/en active Active
- 2009-04-23 DE DE9739136T patent/DE09739136T1/de active Pending
- 2009-04-23 JP JP2011507417A patent/JP5507544B2/ja active Active
- 2009-04-23 NZ NZ588701A patent/NZ588701A/en not_active IP Right Cessation
- 2009-04-23 RU RU2010148399/05A patent/RU2508162C2/ru not_active IP Right Cessation
- 2009-04-23 MX MX2015017656A patent/MX364125B/es unknown
- 2009-04-23 ES ES15002793.6T patent/ES2694014T3/es active Active
- 2009-04-23 KR KR1020107026617A patent/KR20110003555A/ko not_active Withdrawn
- 2009-04-23 MX MX2014001618A patent/MX338852B/es unknown
- 2009-04-23 EP EP09739136.1A patent/EP2323755B1/en active Active
- 2009-04-28 CL CL2009001003A patent/CL2009001003A1/es unknown
- 2009-04-29 AR ARP090101531A patent/AR074141A1/es not_active Application Discontinuation
-
2010
- 2010-09-23 US US12/924,234 patent/US8329944B2/en active Active
- 2010-10-20 ZA ZA2010/07491A patent/ZA201007491B/en unknown
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2011
- 2011-03-22 ZA ZA2011/02114A patent/ZA201102114B/en unknown
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2012
- 2012-11-05 US US13/668,577 patent/US8771616B2/en active Active
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2014
- 2014-07-08 US US14/325,773 patent/US8987512B2/en active Active
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2015
- 2015-03-09 US US14/642,327 patent/US9840451B2/en active Active
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2017
- 2017-11-09 US US15/808,401 patent/US10118885B2/en active Active
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2018
- 2018-10-25 US US16/170,781 patent/US10519089B2/en active Active
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