JP5361739B2 - パラタングステン酸アンモニウム四水和物及び高純度のパラタングステン酸アンモニウム四水和物を製造する方法 - Google Patents

パラタングステン酸アンモニウム四水和物及び高純度のパラタングステン酸アンモニウム四水和物を製造する方法 Download PDF

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JP5361739B2
JP5361739B2 JP2009547659A JP2009547659A JP5361739B2 JP 5361739 B2 JP5361739 B2 JP 5361739B2 JP 2009547659 A JP2009547659 A JP 2009547659A JP 2009547659 A JP2009547659 A JP 2009547659A JP 5361739 B2 JP5361739 B2 JP 5361739B2
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ammonium paratungstate
tetrahydrate
decahydrate
phase
ammonia
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JP2010517903A5 (zh
JP2010517903A (ja
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シュトラー ヴィクトーア
エアプ ミヒャエル
メーゼ−マルクトシェフェル ユリアーネ
ローゼ ミヒャエル
マティ ヴォルフガング
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HC Starck GmbH
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HC Starck GmbH
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00—Compounds of tungsten
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/60—Compounds characterised by their crystallite size
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/88—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by thermal analysis data, e.g. TGA, DTA, DSC
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
JP2009547659A 2007-02-02 2008-01-29 パラタングステン酸アンモニウム四水和物及び高純度のパラタングステン酸アンモニウム四水和物を製造する方法 Active JP5361739B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102007005287.3 2007-02-02
DE102007005287A DE102007005287B4 (de) 2007-02-02 2007-02-02 Verfahren zur Herstellung von Ammoniumparawolframattetrahydrat und hochreines Ammoniumparawolframattetrahydrat
PCT/EP2008/051000 WO2008092838A1 (de) 2007-02-02 2008-01-29 Verfahren zur herstellung von ammoniumparawolframattetrahydrat und hoch reines ammoniumparawolframattetrahydrat

Related Child Applications (1)

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JP2013143060A Division JP5940025B2 (ja) 2007-02-02 2013-07-08 高純度のパラタングステン酸アンモニウム四水和物

Publications (3)

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JP2010517903A JP2010517903A (ja) 2010-05-27
JP2010517903A5 JP2010517903A5 (zh) 2013-08-29
JP5361739B2 true JP5361739B2 (ja) 2013-12-04

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JP2009547659A Active JP5361739B2 (ja) 2007-02-02 2008-01-29 パラタングステン酸アンモニウム四水和物及び高純度のパラタングステン酸アンモニウム四水和物を製造する方法
JP2013143060A Active JP5940025B2 (ja) 2007-02-02 2013-07-08 高純度のパラタングステン酸アンモニウム四水和物

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JP2013143060A Active JP5940025B2 (ja) 2007-02-02 2013-07-08 高純度のパラタングステン酸アンモニウム四水和物

Country Status (8)

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US (2) US8168155B2 (zh)
EP (1) EP2118018B1 (zh)
JP (2) JP5361739B2 (zh)
CN (2) CN103030178B (zh)
DE (1) DE102007005287B4 (zh)
ES (1) ES2745085T3 (zh)
PT (1) PT2118018T (zh)
WO (1) WO2008092838A1 (zh)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007005286B4 (de) 2007-02-02 2009-08-27 H.C. Starck Gmbh Verfahren zur Herstellung von Ammoniumparawolframathydraten und Ammoniumparawolframatdekahydrat
JP5636142B2 (ja) * 2009-03-02 2014-12-03 三菱マテリアル株式会社 高純度パラタングステン酸アンモニウムの製造方法
JP4797099B2 (ja) 2009-10-01 2011-10-19 Ｊｘ日鉱日石金属株式会社 高純度タングステン粉末の製造方法
CN105849837B (zh) 2013-12-27 2018-05-04 昭和电工株式会社 钨电容器用阳极体
CN109289940B (zh) * 2018-10-24 2021-03-05 赣州海创钨业有限公司 一种仲钨酸铵生产用离子交换装置
CN111689520B (zh) * 2020-06-17 2023-04-18 赣州有色冶金研究所有限公司 一种二段真空制备十水合仲钨酸铵的方法
CN113816428A (zh) * 2021-10-26 2021-12-21 赣州市海龙钨钼有限公司 一种制备仲钨酸铵的工艺
CN113816429B (zh) * 2021-11-12 2023-04-18 江西钨业股份有限公司 仲钨酸铵的颗粒粗化方法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1150962B (de) * 1959-02-10 1963-07-04 Gen Mills Inc Verfahren zur Abtrennung von Wolframverbindungen aus waessrigen, wolframhaltigen Loesungen
DE1244141B (de) 1962-10-26 1967-07-13 Blair Burwell Verfahren zur Herstellung von hochreinem Ammoniumparawolframat
US4092400A (en) * 1977-04-11 1978-05-30 Engelhard Minerals & Chemicals Corp. Process for recovering high purity tungsten compositions from wolframite ores
US4115513A (en) 1977-08-16 1978-09-19 Westinghouse Electric Corp. Processing of ammonium paratungstate from tungsten ores
JPS5761632A (en) * 1980-10-02 1982-04-14 Toshiba Corp Production of crude particles of ammonium paratungstenate crystal
US4450144A (en) * 1981-01-19 1984-05-22 Amax Inc. Ammonium hydroxide stripping of tungsten from organic solvents
US4623534A (en) * 1985-03-21 1986-11-18 Gte Products Corporation Method for producing ammonium paratungstate
JPH0227287B2 (ja) * 1985-11-07 1990-06-15 Nippon Mining Co Kojundoparatangusutensananmoniumuketsushonoseizohoho
JPH07121807B2 (ja) * 1987-12-25 1995-12-25 株式会社ジャパンエナジー 高純度パラタングステン酸アンモニウム結晶の製造方法
US4969336A (en) * 1989-08-04 1990-11-13 Cryo-Cell International, Inc. Cryogenic storage apparatus, particularly with automatic retrieval
DE19724183C2 (de) * 1996-07-05 1999-03-25 Starck H C Gmbh Co Kg Verfahren zur Herstellung reiner Alkali- und/oder Ammonium-Wolframat-Lösungen
DE19628816A1 (de) 1996-07-17 1998-01-22 Sawatzki Viktor Verfahren zur Herstellung von Parawolframat
CN1377980A (zh) * 2002-02-06 2002-11-06 王旭升 一种用高钼钨矿制备高纯仲钨酸铵的方法
JP2005126321A (ja) * 2003-09-30 2005-05-19 Jfe Mineral Co Ltd タングステン酸アンモニウムの製造方法
DE102007005286B4 (de) * 2007-02-02 2009-08-27 H.C. Starck Gmbh Verfahren zur Herstellung von Ammoniumparawolframathydraten und Ammoniumparawolframatdekahydrat

Also Published As

Publication number Publication date
PT2118018T (pt) 2019-09-17
ES2745085T3 (es) 2020-02-27
US20100028250A1 (en) 2010-02-04
DE102007005287B4 (de) 2009-10-01
US20110070148A1 (en) 2011-03-24
EP2118018B1 (de) 2019-06-26
CN103030178B (zh) 2015-11-18
CN101600653B (zh) 2013-07-17
US8168155B2 (en) 2012-05-01
WO2008092838A1 (de) 2008-08-07
US8226923B2 (en) 2012-07-24
CN103030178A (zh) 2013-04-10
JP2010517903A (ja) 2010-05-27
JP2013212985A (ja) 2013-10-17
EP2118018A1 (de) 2009-11-18
JP5940025B2 (ja) 2016-06-29
DE102007005287A1 (de) 2008-08-14
CN101600653A (zh) 2009-12-09

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