JP5158088B2 - エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、並びに一液性エポキシ樹脂組成物及びその硬化物 - Google Patents

エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、並びに一液性エポキシ樹脂組成物及びその硬化物 Download PDF

Info

Publication number
JP5158088B2
JP5158088B2 JP2009533162A JP2009533162A JP5158088B2 JP 5158088 B2 JP5158088 B2 JP 5158088B2 JP 2009533162 A JP2009533162 A JP 2009533162A JP 2009533162 A JP2009533162 A JP 2009533162A JP 5158088 B2 JP5158088 B2 JP 5158088B2
Authority
JP
Japan
Prior art keywords
epoxy resin
curing agent
microcapsule
latent curing
type latent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2009533162A
Other languages
English (en)
Japanese (ja)
Other versions
JPWO2009038097A1 (ja
Inventor
重昭 舟生
穣 岡田
芳伊 森下
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Showa Denko Materials Co Ltd
Original Assignee
Hitachi Chemical Co Ltd
Showa Denko Materials Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Chemical Co Ltd, Showa Denko Materials Co Ltd filed Critical Hitachi Chemical Co Ltd
Priority to JP2009533162A priority Critical patent/JP5158088B2/ja
Publication of JPWO2009038097A1 publication Critical patent/JPWO2009038097A1/ja
Application granted granted Critical
Publication of JP5158088B2 publication Critical patent/JP5158088B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00Use of pretreated ingredients
    • C08K9/10Encapsulated ingredients
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/182Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing using pre-adducts of epoxy compounds with curing agents
    • C08G59/184Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing using pre-adducts of epoxy compounds with curing agents with amines
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • C08G59/50Amines
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00Compositions of epoxy resins; Compositions of derivatives of epoxy resins

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Epoxy Resins (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Adhesives Or Adhesive Processes (AREA)
JP2009533162A 2007-09-20 2008-09-17 エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、並びに一液性エポキシ樹脂組成物及びその硬化物 Expired - Fee Related JP5158088B2 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2009533162A JP5158088B2 (ja) 2007-09-20 2008-09-17 エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、並びに一液性エポキシ樹脂組成物及びその硬化物

Applications Claiming Priority (10)

Application Number Priority Date Filing Date Title
JP2007243852 2007-09-20
JP2007243852 2007-09-20
JP2007243851 2007-09-20
JP2007243851 2007-09-20
JP2008043346 2008-02-25
JP2008043346 2008-02-25
JP2008166246 2008-06-25
JP2008166246 2008-06-25
PCT/JP2008/066774 WO2009038097A1 (ja) 2007-09-20 2008-09-17 エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、並びに一液性エポキシ樹脂組成物及びその硬化物
JP2009533162A JP5158088B2 (ja) 2007-09-20 2008-09-17 エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、並びに一液性エポキシ樹脂組成物及びその硬化物

Publications (2)

Publication Number Publication Date
JPWO2009038097A1 JPWO2009038097A1 (ja) 2011-01-06
JP5158088B2 true JP5158088B2 (ja) 2013-03-06

Family

ID=40467907

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2009533162A Expired - Fee Related JP5158088B2 (ja) 2007-09-20 2008-09-17 エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、並びに一液性エポキシ樹脂組成物及びその硬化物

Country Status (5)

Country Link
JP (1) JP5158088B2 (ko)
KR (2) KR101243511B1 (ko)
CN (2) CN101802050A (ko)
TW (2) TW201008971A (ko)
WO (1) WO2009038097A1 (ko)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101086701B1 (ko) * 2009-06-10 2011-11-25 한국과학기술연구원 물리화학적 결합 시스템을 이용한 향상된 보존안정성을 갖는 잠재성 경화제 복합체 입자와 그 제조 방법
KR102270461B1 (ko) * 2016-03-10 2021-06-29 한국전자기술연구원 점접착제 조성물 및 그의 제조방법
KR101870777B1 (ko) * 2017-03-28 2018-06-26 한국신발피혁연구원 마이크로캡슐형 잠재성 경화제의 제조방법 및 이 방법에 의해 제조된 마이크로캡슐형 잠재성 경화제
KR102095115B1 (ko) * 2018-07-27 2020-03-30 한국전력공사 자가치유 실리콘 절연체 및 그 제조방법
CN111087576A (zh) * 2019-12-31 2020-05-01 芜湖天道绿色新材料有限公司 一种可降解微胶囊固化剂的制备及应用
CN111171285B (zh) * 2020-02-15 2022-04-26 常州大学 一种以聚氨酯为壳材的环氧树脂固化剂微胶囊及其制备方法
CN111518500B (zh) * 2020-04-22 2023-04-11 湖北回天新材料股份有限公司 溶剂型单组分环氧微胶囊预涂螺纹锁固胶及其制备方法
CN111389317B (zh) * 2020-04-28 2022-04-12 西北工业大学 基于巯基-异氰酸酯点击反应和油包油界面聚合的咪唑微胶囊的制备方法
CN116323837A (zh) * 2020-09-30 2023-06-23 旭化成株式会社 聚氨酯系固化剂及其应用
JPWO2023286499A1 (ko) * 2021-07-12 2023-01-19
CN114230767B (zh) * 2021-12-13 2024-03-19 江苏钛得新材料技术有限公司 胶粘剂用咪唑类衍生物微胶囊型潜伏固化剂及其制备方法

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11199655A (ja) * 1998-01-12 1999-07-27 Hitachi Ltd マイクロカプセル型りん系硬化促進剤とそれを用いた半導体封止用エポキシ樹脂組成物
JP2005344046A (ja) * 2004-06-04 2005-12-15 Asahi Kasei Chemicals Corp 潜在性硬化剤および組成物
WO2007037378A1 (ja) * 2005-09-29 2007-04-05 Asahi Kasei Chemicals Corporation 高安定性マイクロカプセル型エポキシ樹脂用硬化剤及びエポキシ樹脂組成物
JP2007091900A (ja) * 2005-09-29 2007-04-12 Asahi Kasei Chemicals Corp 速硬化性エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
JP2007091899A (ja) * 2005-09-29 2007-04-12 Asahi Kasei Chemicals Corp 高安定性エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
JP2007091901A (ja) * 2005-09-29 2007-04-12 Asahi Kasei Chemicals Corp 緩反応性エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
WO2007088889A1 (ja) * 2006-02-03 2007-08-09 Asahi Kasei Chemicals Corporation マイクロカプセル型エポキシ樹脂用硬化剤、マスタ-バッチ型エポキシ樹脂用硬化剤組成物、一液性エポキシ樹脂組成物、および加工品
JP2007204670A (ja) * 2006-02-03 2007-08-16 Asahi Kasei Chemicals Corp 高含水含溶剤エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
JP2007204669A (ja) * 2006-02-03 2007-08-16 Asahi Kasei Chemicals Corp 特定小粒径粒度分布エポキシ樹脂用硬化剤およびエポキシ樹脂組成物

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11199655A (ja) * 1998-01-12 1999-07-27 Hitachi Ltd マイクロカプセル型りん系硬化促進剤とそれを用いた半導体封止用エポキシ樹脂組成物
JP2005344046A (ja) * 2004-06-04 2005-12-15 Asahi Kasei Chemicals Corp 潜在性硬化剤および組成物
WO2007037378A1 (ja) * 2005-09-29 2007-04-05 Asahi Kasei Chemicals Corporation 高安定性マイクロカプセル型エポキシ樹脂用硬化剤及びエポキシ樹脂組成物
JP2007091900A (ja) * 2005-09-29 2007-04-12 Asahi Kasei Chemicals Corp 速硬化性エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
JP2007091899A (ja) * 2005-09-29 2007-04-12 Asahi Kasei Chemicals Corp 高安定性エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
JP2007091901A (ja) * 2005-09-29 2007-04-12 Asahi Kasei Chemicals Corp 緩反応性エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
WO2007088889A1 (ja) * 2006-02-03 2007-08-09 Asahi Kasei Chemicals Corporation マイクロカプセル型エポキシ樹脂用硬化剤、マスタ-バッチ型エポキシ樹脂用硬化剤組成物、一液性エポキシ樹脂組成物、および加工品
JP2007204670A (ja) * 2006-02-03 2007-08-16 Asahi Kasei Chemicals Corp 高含水含溶剤エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
JP2007204669A (ja) * 2006-02-03 2007-08-16 Asahi Kasei Chemicals Corp 特定小粒径粒度分布エポキシ樹脂用硬化剤およびエポキシ樹脂組成物

Also Published As

Publication number Publication date
TW201008971A (en) 2010-03-01
KR20120024963A (ko) 2012-03-14
WO2009038097A1 (ja) 2009-03-26
JPWO2009038097A1 (ja) 2011-01-06
KR20100072030A (ko) 2010-06-29
KR101243511B1 (ko) 2013-03-20
CN101802050A (zh) 2010-08-11
TW201244814A (en) 2012-11-16
CN102936331A (zh) 2013-02-20

Similar Documents

Publication Publication Date Title
JP5158088B2 (ja) エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、並びに一液性エポキシ樹脂組成物及びその硬化物
JP4326524B2 (ja) カプセル型硬化剤及び組成物
JP5763527B2 (ja) イミダゾール化合物含有マイクロカプセル化組成物、それを用いた硬化性組成物及びマスターバッチ型硬化剤
KR100938523B1 (ko) 에폭시 수지용 잠재성 경화제 및 에폭시 수지 조성물
JP4583373B2 (ja) エポキシ樹脂用硬化剤及びエポキシ樹脂組成物
JP2010053353A (ja) エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、一液性エポキシ樹脂組成物、エポキシ樹脂硬化物、接着剤、接合用フィルム、導電性材料並びに異方導電性材料
JP5558118B2 (ja) マイクロカプセル型エポキシ樹脂用硬化剤、及びそれを含むマスターバッチ型エポキシ樹脂用硬化剤組成物
WO2007088889A1 (ja) マイクロカプセル型エポキシ樹脂用硬化剤、マスタ-バッチ型エポキシ樹脂用硬化剤組成物、一液性エポキシ樹脂組成物、および加工品
JP2007204670A (ja) 高含水含溶剤エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
JP4877716B2 (ja) 速硬化性エポキシ樹脂用硬化剤およびエポキシ樹脂組成物
JP4463208B2 (ja) 潜在性硬化剤および組成物
JP5228644B2 (ja) エポキシ樹脂用マイクロカプセル型潜在性硬化剤及びその製造方法、一液性エポキシ樹脂組成物並びにエポキシ樹脂硬化物
JP5138685B2 (ja) エポキシ樹脂用硬化剤及びエポキシ樹脂用硬化剤組成物
JP5266936B2 (ja) エポキシ樹脂用マイクロカプセル型潜在性硬化剤、一液性エポキシ樹脂組成物及びエポキシ樹脂硬化物
JP2011208098A (ja) イミダゾール化合物含有マイクロカプセル化組成物、それを用いた硬化性組成物及びマスターバッチ型硬化剤
JP5245790B2 (ja) 一液性エポキシ樹脂組成物
JP4567377B2 (ja) 潜在性硬化剤および組成物
JP2015221859A (ja) エポキシ樹脂用硬化剤、マイクロカプセル型エポキシ樹脂用硬化剤、マスターバッチ型エポキシ樹脂用硬化剤組成物、一液性エポキシ樹脂組成物及び加工品
JP6114037B2 (ja) エポキシ樹脂用硬化剤及びエポキシ樹脂組成物
JP2013053228A (ja) エポキシ樹脂用硬化剤及びマイクロカプセル型エポキシ樹脂用硬化剤
CN117580888A (zh) 环氧树脂组合物、薄膜、薄膜的制造方法和固化物
JP2019189834A (ja) エポキシ樹脂用硬化剤、マスターバッチ型エポキシ樹脂用硬化剤組成物、一液性エポキシ樹脂組成物、及び加工品
JP2013053230A (ja) エポキシ樹脂組成物、及びこれを用いたペースト状組成物、フィルム状組成物
JP2023137042A (ja) 一液性エポキシ樹脂組成物用マスターバッチ型硬化剤、及びエポキシ樹脂組成物
TW202305025A (zh) 環氧樹脂組合物、膜、膜之製造方法及硬化物

Legal Events

Date Code Title Description
A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20120724

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20120920

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20121113

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20121126

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20151221

Year of fee payment: 3

S531 Written request for registration of change of domicile

Free format text: JAPANESE INTERMEDIATE CODE: R313531

S533 Written request for registration of change of name

Free format text: JAPANESE INTERMEDIATE CODE: R313533

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20151221

Year of fee payment: 3

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

LAPS Cancellation because of no payment of annual fees