JP5099409B2 - アリールシラン化合物とその用途 - Google Patents
アリールシラン化合物とその用途 Download PDFInfo
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- JP5099409B2 JP5099409B2 JP2006542942A JP2006542942A JP5099409B2 JP 5099409 B2 JP5099409 B2 JP 5099409B2 JP 2006542942 A JP2006542942 A JP 2006542942A JP 2006542942 A JP2006542942 A JP 2006542942A JP 5099409 B2 JP5099409 B2 JP 5099409B2
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- organic
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- arylsilane
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- C07F7/02—Silicon compounds
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- C07F7/0803—Compounds with Si-C or Si-Si linkages
- C07F7/081—Compounds with Si-C or Si-Si linkages comprising at least one atom selected from the elements N, O, halogen, S, Se or Te
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- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
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- C07F7/081—Compounds with Si-C or Si-Si linkages comprising at least one atom selected from the elements N, O, halogen, S, Se or Te
- C07F7/0812—Compounds with Si-C or Si-Si linkages comprising at least one atom selected from the elements N, O, halogen, S, Se or Te comprising a heterocyclic ring
- C07F7/0814—Compounds with Si-C or Si-Si linkages comprising at least one atom selected from the elements N, O, halogen, S, Se or Te comprising a heterocyclic ring said ring is substituted at a C ring atom by Si
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Description
2、14 陽極
3、16 正孔注入/輸送層
4、18 発光層
5 電子注入/輸送層
6、20 陰極
30 直流電源
32、34 昇圧回路
36、46 ドライバ回路
38 マイクロコンピューター
40 クロック発生回路
42、44 発振回路
48 表示パネル
反応容器に化学式18で表される化合物3.6g、4−ジエチルアミノサリチルアルデヒド3.3g、酢酸5.9g及びピペリジン10mlをとり、170℃で4時間加熱して反応させた後、反応混合物にクロロホルムを加えて抽出した。傾斜によりクロロホルム層を採取し、水及び飽和食塩水で洗浄し、無水硫酸マグネシウムにより乾燥し、濾過した後、クロロホルムを留去した。得られた油状物をクロロホルム/酢酸エチル混液を展開溶剤とするシリカゲルカラムクロマトグラフィーにより精製し、結晶化したところ、化学式4で表されるこの発明のアリールシラン化合物の結晶が3g得られた。
実施例1の方法により得たアリールシラン化合物を水冷式昇華精製装置内へ仕込み、常法により、装置内を減圧に保ちながら加熱することによって精製した。
この発明によるアリールシラン化合物を発光層用材として用い、図1に示す構造の積層型有機EL素子を作製した。すなわち、常法により、臭化水素酸によりパターン化した厚さ160nmの透明ITO電極を有するガラス製基板を有機アルカリ洗浄剤、純水、アセトン及びエタノールを用いて超音波洗浄し、乾燥し、紫外線オゾンによりITO電極表面の有機物を除去した後、真空蒸着装置における前処理室内へ移した。前処理室内を1×10−6Torrまで減圧した後、アルゴン/酸素混合気を1×10−2Torrまで導入し、ITO電極表面をプラズマ処理することによって、陽極2としてのITO電極を有する清浄な基板1を得た。
図2に示すのは、この発明の有機EL素子を主体とする単純マトリックス方式による表示パネル(水平方向に20電極列、垂直方向に30電極列)の1例であり、斯かる表示パネルは次のようにして作製することができる。
図3のブロックダイヤグラムに示すのは、実施例4の方法により作製した表示パネルを用いる情報表示機器の1例である。図3において、30は出力電圧4.5Vの直流電源であり、その出力端には二つの昇圧回路32、34が接続されている。昇圧回路32は5乃至12Vの範囲の直流電圧を供給することができ、その出力端はドライバ回路36へ接続されている。もう一方の昇圧回路34は、5Vの定電圧をマイクロコンピューター38へ供給するものである。
Claims (3)
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JP2006542942A JP5099409B2 (ja) | 2004-10-28 | 2005-10-14 | アリールシラン化合物とその用途 |
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PCT/JP2005/018940 WO2006046416A1 (ja) | 2004-10-28 | 2005-10-14 | アリールシラン化合物とその用途 |
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JP4762527B2 (ja) * | 2004-11-10 | 2011-08-31 | 富士フイルム株式会社 | 有機電界発光素子 |
JP4625324B2 (ja) * | 2004-12-28 | 2011-02-02 | 東レ・ダウコーニング株式会社 | o−ヒドロキシフェニル基含有有機基を有するオルガノポリシロキサン及びその製造方法 |
US8581262B2 (en) * | 2009-08-04 | 2013-11-12 | Merck Patent Gmbh | Electronic devices comprising multi cyclic hydrocarbons |
CN111039910A (zh) * | 2019-12-31 | 2020-04-21 | 云南大学 | 一种光引发的合成3-芳基黄酮或香豆素类化合物的方法及应用 |
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JPS5527182A (en) * | 1978-07-24 | 1980-02-27 | Gen Electric | Silylcarbonylether and its manufacture |
JPH0987630A (ja) * | 1995-09-28 | 1997-03-31 | Toshiba Corp | 二色性色素化合物及び液晶表示装置 |
JPH09124733A (ja) * | 1995-10-02 | 1997-05-13 | Bayer Ag | ビニル単位を基とする(コ)ポリマー類および電界発光装置におけるそれらの使用 |
JP2003268107A (ja) * | 2002-03-14 | 2003-09-25 | National Institute Of Advanced Industrial & Technology | オクタシロキサンポリマーおよびその製法 |
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- 2005-10-14 WO PCT/JP2005/018940 patent/WO2006046416A1/ja active Application Filing
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JPS5527182A (en) * | 1978-07-24 | 1980-02-27 | Gen Electric | Silylcarbonylether and its manufacture |
JPH0987630A (ja) * | 1995-09-28 | 1997-03-31 | Toshiba Corp | 二色性色素化合物及び液晶表示装置 |
JPH09124733A (ja) * | 1995-10-02 | 1997-05-13 | Bayer Ag | ビニル単位を基とする(コ)ポリマー類および電界発光装置におけるそれらの使用 |
JP2003268107A (ja) * | 2002-03-14 | 2003-09-25 | National Institute Of Advanced Industrial & Technology | オクタシロキサンポリマーおよびその製法 |
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