JP5013622B2 - リチウムボレート系化合物の製造方法 - Google Patents

リチウムボレート系化合物の製造方法 Download PDF

Info

Publication number
JP5013622B2
JP5013622B2 JP2009054842A JP2009054842A JP5013622B2 JP 5013622 B2 JP5013622 B2 JP 5013622B2 JP 2009054842 A JP2009054842 A JP 2009054842A JP 2009054842 A JP2009054842 A JP 2009054842A JP 5013622 B2 JP5013622 B2 JP 5013622B2
Authority
JP
Japan
Prior art keywords
compound
lithium
lithium borate
carbonate
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2009054842A
Other languages
English (en)
Japanese (ja)
Other versions
JP2010208876A (ja
JP2010208876A5 (enExample
Inventor
敏勝 小島
哲男 境
琢寛 幸
晶 小島
淳一 丹羽
仁俊 村瀬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toyota Industries Corp
National Institute of Advanced Industrial Science and Technology AIST
Original Assignee
Toyota Industries Corp
National Institute of Advanced Industrial Science and Technology AIST
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to JP2009054842A priority Critical patent/JP5013622B2/ja
Application filed by Toyota Industries Corp, National Institute of Advanced Industrial Science and Technology AIST filed Critical Toyota Industries Corp
Priority to CN201080011418.2A priority patent/CN102348640B/zh
Priority to US13/255,447 priority patent/US20110315919A1/en
Priority to KR1020117020913A priority patent/KR101331916B1/ko
Priority to PCT/JP2010/054075 priority patent/WO2010104137A1/ja
Priority to EP10750890A priority patent/EP2407426A1/en
Publication of JP2010208876A publication Critical patent/JP2010208876A/ja
Publication of JP2010208876A5 publication Critical patent/JP2010208876A5/ja
Application granted granted Critical
Publication of JP5013622B2 publication Critical patent/JP5013622B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/10—Compounds containing boron and oxygen
    • C01B35/12—Borates
    • C01B35/128—Borates containing plural metal or metal and ammonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/10—Compounds containing boron and oxygen
    • C01B35/12—Borates
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139—Processes of manufacture
    • H01M4/1397—Processes of manufacture of electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
JP2009054842A 2009-03-09 2009-03-09 リチウムボレート系化合物の製造方法 Expired - Fee Related JP5013622B2 (ja)

Priority Applications (6)

Application Number Priority Date Filing Date Title
JP2009054842A JP5013622B2 (ja) 2009-03-09 2009-03-09 リチウムボレート系化合物の製造方法
US13/255,447 US20110315919A1 (en) 2009-03-09 2010-03-04 Production process for lithium-borate-system compound
KR1020117020913A KR101331916B1 (ko) 2009-03-09 2010-03-04 리튬 보레이트계 화합물의 제조 방법, 리튬 이온 2차 전지용 정극 활물질, 리튬 이온 2차 전지용 정극 및 리튬 이온 2차 전지
PCT/JP2010/054075 WO2010104137A1 (ja) 2009-03-09 2010-03-04 リチウムボレート系化合物の製造方法
CN201080011418.2A CN102348640B (zh) 2009-03-09 2010-03-04 硼酸锂系化合物的制备方法
EP10750890A EP2407426A1 (en) 2009-03-09 2010-03-04 Process for producing lithium borate compound

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2009054842A JP5013622B2 (ja) 2009-03-09 2009-03-09 リチウムボレート系化合物の製造方法

Publications (3)

Publication Number Publication Date
JP2010208876A JP2010208876A (ja) 2010-09-24
JP2010208876A5 JP2010208876A5 (enExample) 2012-01-05
JP5013622B2 true JP5013622B2 (ja) 2012-08-29

Family

ID=42728425

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2009054842A Expired - Fee Related JP5013622B2 (ja) 2009-03-09 2009-03-09 リチウムボレート系化合物の製造方法

Country Status (6)

Country Link
US (1) US20110315919A1 (enExample)
EP (1) EP2407426A1 (enExample)
JP (1) JP5013622B2 (enExample)
KR (1) KR101331916B1 (enExample)
CN (1) CN102348640B (enExample)
WO (1) WO2010104137A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107039643A (zh) * 2017-03-27 2017-08-11 上海应用技术大学 一种锂离子电池用正极材料及其制备方法

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9172090B2 (en) * 2010-05-07 2015-10-27 Massachusetts Institute Of Technoloy Electrochemical device comprising lithium manganese borate compounds
JP5164287B2 (ja) * 2010-11-05 2013-03-21 株式会社豊田自動織機 リチウムシリケート系化合物およびその製造方法
JP5110664B2 (ja) * 2010-11-05 2012-12-26 株式会社豊田自動織機 リチウムボレート系化合物の製造方法
CN104795563A (zh) * 2014-01-18 2015-07-22 南京理工大学 一种柠檬酸法制备锂离子电池正极材料LiFeBO3/C的方法
CN103943857B (zh) * 2014-05-09 2016-02-03 湖南科技大学 一种锂离子电池LiMnBO3/KB复合正极材料及其制备方法
KR101637925B1 (ko) 2014-07-18 2016-07-08 한국과학기술연구원 리튬 망간 보레이트계 양극 활물질, 이를 포함하는 리튬 이온 이차전지 및 이의 제조방법
CN106654184A (zh) * 2015-10-29 2017-05-10 上海比亚迪有限公司 一种锂离子电池正极材料添加剂、正极材料、正极及电池
CN105789625B (zh) * 2016-04-25 2018-06-01 湖南科技大学 一种锂离子电池正极材料LiCoBO3的制备方法
CN107946585B (zh) * 2017-12-26 2020-01-31 宁波职业技术学院 一种掺杂硼酸锰镁镁离子电池正极材料的制备方法
CN108910907A (zh) * 2018-07-20 2018-11-30 上海中锂实业有限公司 一种无水四硼酸锂的制备方法
CN109110774B (zh) * 2018-10-25 2022-02-01 河南省法恩莱特新能源科技有限公司 一种四氟硼酸锂的制备方法
CN110563339A (zh) * 2019-10-17 2019-12-13 维沃泰克仪器(扬州)有限公司 一种无水硼酸锂助熔剂的制备方法
KR102630488B1 (ko) * 2021-01-15 2024-01-29 울산대학교 산학협력단 할로겐 원소를 포함하는 전극 재료 및 이의 제조 방법
CN115924931B (zh) * 2023-01-06 2024-07-30 中国科学院新疆理化技术研究所 一种化合物硼酸锂钠及制备方法和用途
CN119503825A (zh) * 2024-11-14 2025-02-25 孝感楚能新能源创新科技有限公司 一种硼酸钛铁锂正极材料及其制备方法和应用

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10241682A (ja) * 1997-02-25 1998-09-11 Mitsubishi Cable Ind Ltd リチウム二次電池用の正極活物質およびその製造方法
JP2001048545A (ja) * 1999-08-09 2001-02-20 Mitsubishi Chemicals Corp リチウムマンガン複合酸化物の製造方法及びこれを用いた二次電池
JP2001064020A (ja) * 1999-08-30 2001-03-13 Mitsui Mining & Smelting Co Ltd マンガン酸リチウムの製造方法
JP4691228B2 (ja) * 1999-11-02 2011-06-01 Ａｇｃセイミケミカル株式会社 非水リチウム二次電池用リチウム−マンガン複合酸化物の製造法
KR20010056566A (ko) * 1999-12-15 2001-07-04 성재갑 리튬전지용 리튬 망간 복합산화물 분말의 제조방법
JP2004207051A (ja) * 2002-12-25 2004-07-22 Junko Shigehara 正極材料、それを利用したリチウム二次電池及びリチウムイオン二次電池
JP2005183088A (ja) * 2003-12-17 2005-07-07 Nichia Chem Ind Ltd 非水電解質二次電池用正極活物質および非水電解質二次電池
JP3763537B2 (ja) * 2003-12-24 2006-04-05 三井金属鉱業株式会社 リチウム−マンガン系複合酸化物及びリチウム二次電池
JP5132308B2 (ja) * 2005-05-17 2013-01-30 Ａｇｃセイミケミカル株式会社 リチウム二次電池正極用のリチウム含有複合酸化物の製造方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107039643A (zh) * 2017-03-27 2017-08-11 上海应用技术大学 一种锂离子电池用正极材料及其制备方法
CN107039643B (zh) * 2017-03-27 2019-05-24 上海应用技术大学 一种锂离子电池用正极材料及其制备方法

Also Published As

Publication number Publication date
CN102348640B (zh) 2014-02-05
JP2010208876A (ja) 2010-09-24
KR20110118806A (ko) 2011-11-01
KR101331916B1 (ko) 2013-11-21
CN102348640A (zh) 2012-02-08
WO2010104137A1 (ja) 2010-09-16
US20110315919A1 (en) 2011-12-29
EP2407426A1 (en) 2012-01-18

Similar Documents

Publication Publication Date Title
JP5013622B2 (ja) リチウムボレート系化合物の製造方法
JP5298286B2 (ja) リチウムシリケート系化合物の製造方法
US12170361B2 (en) Batteries with anodes of carbon-coated macro-porous silicon
JP5116177B2 (ja) リチウムシリケート系化合物の製造方法
JP5252064B2 (ja) リチウムシリケート系化合物及びその製造方法
JP5164287B2 (ja) リチウムシリケート系化合物およびその製造方法
JP2011213587A (ja) リン酸マンガン鉄リチウム粒子粉末の製造方法、リン酸マンガン鉄リチウム粒子粉末、及び該粒子粉末を用いた非水電解質二次電池
JPWO2017183653A1 (ja) 正極用材料
KR101352793B1 (ko) 이차전지용 양극재료 및 이의 제조방법
TWI465390B (zh) 鋰蓄電池用正極活性物質之製造方法
JP5110664B2 (ja) リチウムボレート系化合物の製造方法
JP2012023006A (ja) リチウム二次電池用陽極材料及びその製造方法並びにその材料を含むリチウム二次電池
JP2010238603A (ja) フッ化リン酸鉄リチウム固溶体正極活物質粉末、及び製造方法、並びにリチウムイオン二次電池
JP5608856B2 (ja) リチウムイオン二次電池用正極活物質とその製造方法及びリチウムイオン二次電池用正極とリチウムイオン二次電池
KR101821880B1 (ko) 글루코스를 이용한 다공성 게르마늄-카본 복합체 제조방법
JP5686378B2 (ja) 水素含有リチウムシリケート系化合物及びその製造方法、並びに非水電解質二次電池用正極活物質、非水電解質二次電池用正極、非水電解質二次電池及び車両
WO2014155408A1 (ja) 水素含有リチウムシリケート系化合物及びその製造方法、並びに非水電解質二次電池用正極活物質、非水電解質二次電池用正極、及び非水電解質二次電池

Legal Events

Date Code Title Description
A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20111017

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20111014

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20111102

A871 Explanation of circumstances concerning accelerated examination

Free format text: JAPANESE INTERMEDIATE CODE: A871

Effective date: 20120423

TRDD Decision of grant or rejection written
A975 Report on accelerated examination

Free format text: JAPANESE INTERMEDIATE CODE: A971005

Effective date: 20120515

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20120522

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20120604

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20150615

Year of fee payment: 3

R150 Certificate of patent or registration of utility model

Ref document number: 5013622

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S533 Written request for registration of change of name

Free format text: JAPANESE INTERMEDIATE CODE: R313533

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313117

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees