CN102348640B - 硼酸锂系化合物的制备方法 - Google Patents

硼酸锂系化合物的制备方法 Download PDF

Info

Publication number
CN102348640B
CN102348640B CN201080011418.2A CN201080011418A CN102348640B CN 102348640 B CN102348640 B CN 102348640B CN 201080011418 A CN201080011418 A CN 201080011418A CN 102348640 B CN102348640 B CN 102348640B
Authority
CN
China
Prior art keywords
lithium
compound
based compound
lithium borate
carbonate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201080011418.2A
Other languages
English (en)
Chinese (zh)
Other versions
CN102348640A (zh
Inventor
小岛敏胜
境哲男
幸琢宽
小岛晶
丹羽淳一
村濑仁俊
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toyota Industries Corp
National Institute of Advanced Industrial Science and Technology AIST
Original Assignee
National Institute of Advanced Industrial Science and Technology AIST
Toyoda Automatic Loom Works Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by National Institute of Advanced Industrial Science and Technology AIST, Toyoda Automatic Loom Works Ltd filed Critical National Institute of Advanced Industrial Science and Technology AIST
Publication of CN102348640A publication Critical patent/CN102348640A/zh
Application granted granted Critical
Publication of CN102348640B publication Critical patent/CN102348640B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/10—Compounds containing boron and oxygen
    • C01B35/12—Borates
    • C01B35/128—Borates containing plural metal or metal and ammonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/10—Compounds containing boron and oxygen
    • C01B35/12—Borates
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139—Processes of manufacture
    • H01M4/1397—Processes of manufacture of electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
CN201080011418.2A 2009-03-09 2010-03-04 硼酸锂系化合物的制备方法 Expired - Fee Related CN102348640B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2009054842A JP5013622B2 (ja) 2009-03-09 2009-03-09 リチウムボレート系化合物の製造方法
JP2009-054842 2009-03-09
PCT/JP2010/054075 WO2010104137A1 (ja) 2009-03-09 2010-03-04 リチウムボレート系化合物の製造方法

Publications (2)

Publication Number Publication Date
CN102348640A CN102348640A (zh) 2012-02-08
CN102348640B true CN102348640B (zh) 2014-02-05

Family

ID=42728425

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080011418.2A Expired - Fee Related CN102348640B (zh) 2009-03-09 2010-03-04 硼酸锂系化合物的制备方法

Country Status (6)

Country Link
US (1) US20110315919A1 (enExample)
EP (1) EP2407426A1 (enExample)
JP (1) JP5013622B2 (enExample)
KR (1) KR101331916B1 (enExample)
CN (1) CN102348640B (enExample)
WO (1) WO2010104137A1 (enExample)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9172090B2 (en) * 2010-05-07 2015-10-27 Massachusetts Institute Of Technoloy Electrochemical device comprising lithium manganese borate compounds
JP5164287B2 (ja) * 2010-11-05 2013-03-21 株式会社豊田自動織機 リチウムシリケート系化合物およびその製造方法
JP5110664B2 (ja) * 2010-11-05 2012-12-26 株式会社豊田自動織機 リチウムボレート系化合物の製造方法
CN104795563A (zh) * 2014-01-18 2015-07-22 南京理工大学 一种柠檬酸法制备锂离子电池正极材料LiFeBO3/C的方法
CN103943857B (zh) * 2014-05-09 2016-02-03 湖南科技大学 一种锂离子电池LiMnBO3/KB复合正极材料及其制备方法
KR101637925B1 (ko) 2014-07-18 2016-07-08 한국과학기술연구원 리튬 망간 보레이트계 양극 활물질, 이를 포함하는 리튬 이온 이차전지 및 이의 제조방법
CN106654184A (zh) * 2015-10-29 2017-05-10 上海比亚迪有限公司 一种锂离子电池正极材料添加剂、正极材料、正极及电池
CN105789625B (zh) * 2016-04-25 2018-06-01 湖南科技大学 一种锂离子电池正极材料LiCoBO3的制备方法
CN107039643B (zh) * 2017-03-27 2019-05-24 上海应用技术大学 一种锂离子电池用正极材料及其制备方法
CN107946585B (zh) * 2017-12-26 2020-01-31 宁波职业技术学院 一种掺杂硼酸锰镁镁离子电池正极材料的制备方法
CN108910907A (zh) * 2018-07-20 2018-11-30 上海中锂实业有限公司 一种无水四硼酸锂的制备方法
CN109110774B (zh) * 2018-10-25 2022-02-01 河南省法恩莱特新能源科技有限公司 一种四氟硼酸锂的制备方法
CN110563339A (zh) * 2019-10-17 2019-12-13 维沃泰克仪器(扬州)有限公司 一种无水硼酸锂助熔剂的制备方法
KR102630488B1 (ko) * 2021-01-15 2024-01-29 울산대학교 산학협력단 할로겐 원소를 포함하는 전극 재료 및 이의 제조 방법
CN115924931B (zh) * 2023-01-06 2024-07-30 中国科学院新疆理化技术研究所 一种化合物硼酸锂钠及制备方法和用途
CN119503825A (zh) * 2024-11-14 2025-02-25 孝感楚能新能源创新科技有限公司 一种硼酸钛铁锂正极材料及其制备方法和应用

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004207051A (ja) * 2002-12-25 2004-07-22 Junko Shigehara 正極材料、それを利用したリチウム二次電池及びリチウムイオン二次電池
JP2005112711A (ja) * 2003-12-24 2005-04-28 Mitsui Mining & Smelting Co Ltd リチウム−マンガン系複合酸化物及びリチウム二次電池
JP2005183088A (ja) * 2003-12-17 2005-07-07 Nichia Chem Ind Ltd 非水電解質二次電池用正極活物質および非水電解質二次電池
CN101176226A (zh) * 2005-05-17 2008-05-07 Agc清美化学股份有限公司 锂二次电池正极用的含锂复合氧化物的制造方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10241682A (ja) * 1997-02-25 1998-09-11 Mitsubishi Cable Ind Ltd リチウム二次電池用の正極活物質およびその製造方法
JP2001048545A (ja) * 1999-08-09 2001-02-20 Mitsubishi Chemicals Corp リチウムマンガン複合酸化物の製造方法及びこれを用いた二次電池
JP2001064020A (ja) * 1999-08-30 2001-03-13 Mitsui Mining & Smelting Co Ltd マンガン酸リチウムの製造方法
JP4691228B2 (ja) * 1999-11-02 2011-06-01 Ａｇｃセイミケミカル株式会社 非水リチウム二次電池用リチウム−マンガン複合酸化物の製造法
KR20010056566A (ko) * 1999-12-15 2001-07-04 성재갑 리튬전지용 리튬 망간 복합산화물 분말의 제조방법

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004207051A (ja) * 2002-12-25 2004-07-22 Junko Shigehara 正極材料、それを利用したリチウム二次電池及びリチウムイオン二次電池
JP2005183088A (ja) * 2003-12-17 2005-07-07 Nichia Chem Ind Ltd 非水電解質二次電池用正極活物質および非水電解質二次電池
JP2005112711A (ja) * 2003-12-24 2005-04-28 Mitsui Mining & Smelting Co Ltd リチウム−マンガン系複合酸化物及びリチウム二次電池
CN101176226A (zh) * 2005-05-17 2008-05-07 Agc清美化学股份有限公司 锂二次电池正极用的含锂复合氧化物的制造方法

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
JP特开2004207051A 2004.07.22
JP特开2005112711A 2005.04.28
JP特开2005183088A 2005.07.07

Also Published As

Publication number Publication date
JP5013622B2 (ja) 2012-08-29
JP2010208876A (ja) 2010-09-24
KR20110118806A (ko) 2011-11-01
KR101331916B1 (ko) 2013-11-21
CN102348640A (zh) 2012-02-08
WO2010104137A1 (ja) 2010-09-16
US20110315919A1 (en) 2011-12-29
EP2407426A1 (en) 2012-01-18

Similar Documents

Publication Publication Date Title
CN102348640B (zh) 硼酸锂系化合物的制备方法
CN102300811B (zh) 硅酸锂系化合物的制造方法
US9643846B2 (en) Recycling method of olivine-based cathode material for lithium secondary battery, cathode material fabricated therefrom, and cathode and lithium secondary battery including the same
JP5116177B2 (ja) リチウムシリケート系化合物の製造方法
JP6176510B2 (ja) シリコン材料及び二次電池の負極
WO2015182116A1 (ja) ナノシリコン材料とその製造方法及び二次電池の負極
WO2014129096A1 (ja) リチウムイオン二次電池及びその製造方法
TWI465390B (zh) 鋰蓄電池用正極活性物質之製造方法
Zhao et al. Environmentally benign and scalable synthesis of LiFePO4 nanoplates with high capacity and excellent rate cycling performance for lithium ion batteries
JP5110664B2 (ja) リチウムボレート系化合物の製造方法
KR101821880B1 (ko) 글루코스를 이용한 다공성 게르마늄-카본 복합체 제조방법
JP5608856B2 (ja) リチウムイオン二次電池用正極活物質とその製造方法及びリチウムイオン二次電池用正極とリチウムイオン二次電池
JP5686378B2 (ja) 水素含有リチウムシリケート系化合物及びその製造方法、並びに非水電解質二次電池用正極活物質、非水電解質二次電池用正極、非水電解質二次電池及び車両
WO2014155408A1 (ja) 水素含有リチウムシリケート系化合物及びその製造方法、並びに非水電解質二次電池用正極活物質、非水電解質二次電池用正極、及び非水電解質二次電池
Hu et al. Synthesis and electrochemical performance of Li2Mg0. 15Mn0. 4Co0. 45SiO4/C cathode material for lithium ion batteries
Grag et al. Carbon-coated LiFePO4–carbon nanotube electrodes for high-rate Li-ion battery
WO2019053983A1 (ja) Ａｌ含有シリコン材料を含む負極活物質

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140205

Termination date: 20150304

EXPY Termination of patent right or utility model