KR101331916B1 - 리튬 보레이트계 화합물의 제조 방법, 리튬 이온 2차 전지용 정극 활물질, 리튬 이온 2차 전지용 정극 및 리튬 이온 2차 전지 - Google Patents

리튬 보레이트계 화합물의 제조 방법, 리튬 이온 2차 전지용 정극 활물질, 리튬 이온 2차 전지용 정극 및 리튬 이온 2차 전지 Download PDF

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KR101331916B1
KR101331916B1 KR1020117020913A KR20117020913A KR101331916B1 KR 101331916 B1 KR101331916 B1 KR 101331916B1 KR 1020117020913 A KR1020117020913 A KR 1020117020913A KR 20117020913 A KR20117020913 A KR 20117020913A KR 101331916 B1 KR101331916 B1 KR 101331916B1
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compound
lithium
carbonate
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lithium borate
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KR20110118806A (ko
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토시카츠 고지마
테츠오 사카이
타쿠히로 미유키
아키라 고지마
준이치 니와
히토토시 무라세
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가부시키가이샤 도요다 지도숏키
도꾸리츠교우세이호우진 산교기쥬츠소우고겐큐쇼
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/10—Compounds containing boron and oxygen
    • C01B35/12—Borates
    • C01B35/128—Borates containing plural metal or metal and ammonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
    • C01B35/10—Compounds containing boron and oxygen
    • C01B35/12—Borates
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139—Processes of manufacture
    • H01M4/1397—Processes of manufacture of electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nanotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Composite Materials (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
KR1020117020913A 2009-03-09 2010-03-04 리튬 보레이트계 화합물의 제조 방법, 리튬 이온 2차 전지용 정극 활물질, 리튬 이온 2차 전지용 정극 및 리튬 이온 2차 전지 Expired - Fee Related KR101331916B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2009054842A JP5013622B2 (ja) 2009-03-09 2009-03-09 リチウムボレート系化合物の製造方法
JPJP-P-2009-054842 2009-03-09
PCT/JP2010/054075 WO2010104137A1 (ja) 2009-03-09 2010-03-04 リチウムボレート系化合物の製造方法

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KR20110118806A KR20110118806A (ko) 2011-11-01
KR101331916B1 true KR101331916B1 (ko) 2013-11-21

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Country Link
US (1) US20110315919A1 (enExample)
EP (1) EP2407426A1 (enExample)
JP (1) JP5013622B2 (enExample)
KR (1) KR101331916B1 (enExample)
CN (1) CN102348640B (enExample)
WO (1) WO2010104137A1 (enExample)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011140327A2 (en) * 2010-05-07 2011-11-10 Massachusetts Institute Of Technology Lithium manganese borate compounds
JP5110664B2 (ja) * 2010-11-05 2012-12-26 株式会社豊田自動織機 リチウムボレート系化合物の製造方法
JP5164287B2 (ja) * 2010-11-05 2013-03-21 株式会社豊田自動織機 リチウムシリケート系化合物およびその製造方法
CN104795563A (zh) * 2014-01-18 2015-07-22 南京理工大学 一种柠檬酸法制备锂离子电池正极材料LiFeBO3/C的方法
CN103943857B (zh) * 2014-05-09 2016-02-03 湖南科技大学 一种锂离子电池LiMnBO3/KB复合正极材料及其制备方法
KR101637925B1 (ko) 2014-07-18 2016-07-08 한국과학기술연구원 리튬 망간 보레이트계 양극 활물질, 이를 포함하는 리튬 이온 이차전지 및 이의 제조방법
CN106654184A (zh) * 2015-10-29 2017-05-10 上海比亚迪有限公司 一种锂离子电池正极材料添加剂、正极材料、正极及电池
CN105789625B (zh) * 2016-04-25 2018-06-01 湖南科技大学 一种锂离子电池正极材料LiCoBO3的制备方法
CN107039643B (zh) * 2017-03-27 2019-05-24 上海应用技术大学 一种锂离子电池用正极材料及其制备方法
CN107946585B (zh) * 2017-12-26 2020-01-31 宁波职业技术学院 一种掺杂硼酸锰镁镁离子电池正极材料的制备方法
CN108910907A (zh) * 2018-07-20 2018-11-30 上海中锂实业有限公司 一种无水四硼酸锂的制备方法
CN109110774B (zh) * 2018-10-25 2022-02-01 河南省法恩莱特新能源科技有限公司 一种四氟硼酸锂的制备方法
CN110563339A (zh) * 2019-10-17 2019-12-13 维沃泰克仪器(扬州)有限公司 一种无水硼酸锂助熔剂的制备方法
KR102630488B1 (ko) * 2021-01-15 2024-01-29 울산대학교 산학협력단 할로겐 원소를 포함하는 전극 재료 및 이의 제조 방법
CN115924931B (zh) * 2023-01-06 2024-07-30 中国科学院新疆理化技术研究所 一种化合物硼酸锂钠及制备方法和用途
CN117069119B (zh) * 2023-06-29 2025-12-16 甘肃睿思科新材料有限公司 一种使用电池级碳酸锂在液相中制备高纯高密度四硼酸锂粉体的方法
CN119503825A (zh) * 2024-11-14 2025-02-25 孝感楚能新能源创新科技有限公司 一种硼酸钛铁锂正极材料及其制备方法和应用

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KR20010056566A (ko) * 1999-12-15 2001-07-04 성재갑 리튬전지용 리튬 망간 복합산화물 분말의 제조방법
JP2004207051A (ja) * 2002-12-25 2004-07-22 Junko Shigehara 正極材料、それを利用したリチウム二次電池及びリチウムイオン二次電池
JP2005112711A (ja) * 2003-12-24 2005-04-28 Mitsui Mining & Smelting Co Ltd リチウム−マンガン系複合酸化物及びリチウム二次電池
JP2005183088A (ja) * 2003-12-17 2005-07-07 Nichia Chem Ind Ltd 非水電解質二次電池用正極活物質および非水電解質二次電池

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JPH10241682A (ja) * 1997-02-25 1998-09-11 Mitsubishi Cable Ind Ltd リチウム二次電池用の正極活物質およびその製造方法
JP2001048545A (ja) * 1999-08-09 2001-02-20 Mitsubishi Chemicals Corp リチウムマンガン複合酸化物の製造方法及びこれを用いた二次電池
JP2001064020A (ja) * 1999-08-30 2001-03-13 Mitsui Mining & Smelting Co Ltd マンガン酸リチウムの製造方法
JP4691228B2 (ja) * 1999-11-02 2011-06-01 Ａｇｃセイミケミカル株式会社 非水リチウム二次電池用リチウム−マンガン複合酸化物の製造法
WO2006123711A1 (ja) * 2005-05-17 2006-11-23 Agc Seimi Chemical Co., Ltd. リチウム二次電池正極用のリチウム含有複合酸化物の製造方法

Patent Citations (4)

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Publication number Priority date Publication date Assignee Title
KR20010056566A (ko) * 1999-12-15 2001-07-04 성재갑 리튬전지용 리튬 망간 복합산화물 분말의 제조방법
JP2004207051A (ja) * 2002-12-25 2004-07-22 Junko Shigehara 正極材料、それを利用したリチウム二次電池及びリチウムイオン二次電池
JP2005183088A (ja) * 2003-12-17 2005-07-07 Nichia Chem Ind Ltd 非水電解質二次電池用正極活物質および非水電解質二次電池
JP2005112711A (ja) * 2003-12-24 2005-04-28 Mitsui Mining & Smelting Co Ltd リチウム−マンガン系複合酸化物及びリチウム二次電池

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JP2010208876A (ja) 2010-09-24
CN102348640B (zh) 2014-02-05
WO2010104137A1 (ja) 2010-09-16
JP5013622B2 (ja) 2012-08-29
EP2407426A1 (en) 2012-01-18
US20110315919A1 (en) 2011-12-29
KR20110118806A (ko) 2011-11-01
CN102348640A (zh) 2012-02-08

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