JP5006030B2 - 粉末冶金スパッタリングターゲット及びその製造方法 - Google Patents
粉末冶金スパッタリングターゲット及びその製造方法 Download PDFInfo
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- JP5006030B2 JP5006030B2 JP2006500812A JP2006500812A JP5006030B2 JP 5006030 B2 JP5006030 B2 JP 5006030B2 JP 2006500812 A JP2006500812 A JP 2006500812A JP 2006500812 A JP2006500812 A JP 2006500812A JP 5006030 B2 JP5006030 B2 JP 5006030B2
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- Prior art keywords
- metal
- tantalum
- powder
- ppm
- metal powder
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- Expired - Fee Related
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- 238000005477 sputtering target Methods 0.000 title claims description 45
- 238000004663 powder metallurgy Methods 0.000 title description 16
- 238000004519 manufacturing process Methods 0.000 title description 7
- 229910052751 metal Inorganic materials 0.000 claims description 121
- 239000002184 metal Substances 0.000 claims description 121
- 239000000843 powder Substances 0.000 claims description 88
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 78
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims description 43
- 229910052757 nitrogen Inorganic materials 0.000 claims description 37
- 229910052715 tantalum Inorganic materials 0.000 claims description 37
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 35
- 239000001301 oxygen Substances 0.000 claims description 35
- 229910052760 oxygen Inorganic materials 0.000 claims description 35
- 239000002245 particle Substances 0.000 claims description 16
- 229910052758 niobium Inorganic materials 0.000 claims description 14
- 239000010955 niobium Substances 0.000 claims description 14
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims description 14
- 150000004767 nitrides Chemical class 0.000 claims description 6
- 229910001257 Nb alloy Inorganic materials 0.000 claims description 2
- 229910001362 Ta alloys Inorganic materials 0.000 claims description 2
- 238000000034 method Methods 0.000 description 32
- 239000000463 material Substances 0.000 description 23
- 238000005245 sintering Methods 0.000 description 17
- 238000009694 cold isostatic pressing Methods 0.000 description 15
- 239000000956 alloy Substances 0.000 description 12
- 229910045601 alloy Inorganic materials 0.000 description 12
- 238000005538 encapsulation Methods 0.000 description 12
- 230000000930 thermomechanical effect Effects 0.000 description 12
- 239000007769 metal material Substances 0.000 description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 8
- 230000004888 barrier function Effects 0.000 description 8
- 239000010408 film Substances 0.000 description 8
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 7
- 229910052802 copper Inorganic materials 0.000 description 7
- 239000010949 copper Substances 0.000 description 7
- 238000009792 diffusion process Methods 0.000 description 7
- 238000001125 extrusion Methods 0.000 description 7
- 238000005242 forging Methods 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- 239000011261 inert gas Substances 0.000 description 6
- 238000005121 nitriding Methods 0.000 description 6
- 238000004544 sputter deposition Methods 0.000 description 6
- MZLGASXMSKOWSE-UHFFFAOYSA-N tantalum nitride Chemical compound [Ta]#N MZLGASXMSKOWSE-UHFFFAOYSA-N 0.000 description 6
- 229910052782 aluminium Inorganic materials 0.000 description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
- 229910001873 dinitrogen Inorganic materials 0.000 description 5
- 238000001513 hot isostatic pressing Methods 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 4
- 239000003990 capacitor Substances 0.000 description 4
- 238000002386 leaching Methods 0.000 description 4
- 239000000155 melt Substances 0.000 description 4
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 4
- 239000004065 semiconductor Substances 0.000 description 4
- 239000013077 target material Substances 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 238000007596 consolidation process Methods 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000006392 deoxygenation reaction Methods 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 238000000465 moulding Methods 0.000 description 3
- 238000005546 reactive sputtering Methods 0.000 description 3
- 238000005096 rolling process Methods 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 239000010936 titanium Substances 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- -1 VIB metals Chemical class 0.000 description 2
- 230000009102 absorption Effects 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 2
- 150000001342 alkaline earth metals Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000010941 cobalt Substances 0.000 description 2
- 229910017052 cobalt Inorganic materials 0.000 description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 238000005272 metallurgy Methods 0.000 description 2
- BPUBBGLMJRNUCC-UHFFFAOYSA-N oxygen(2-);tantalum(5+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Ta+5].[Ta+5] BPUBBGLMJRNUCC-UHFFFAOYSA-N 0.000 description 2
- 238000001953 recrystallisation Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 238000005482 strain hardening Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910001936 tantalum oxide Inorganic materials 0.000 description 2
- 239000010409 thin film Substances 0.000 description 2
- ZMZDMBWJUHKJPS-UHFFFAOYSA-N thiocyanic acid Chemical compound SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 description 2
- 229910052727 yttrium Inorganic materials 0.000 description 2
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910000881 Cu alloy Inorganic materials 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 101000652359 Homo sapiens Spermatogenesis-associated protein 2 Proteins 0.000 description 1
- 101000642464 Homo sapiens Spermatogenesis-associated protein 2-like protein Proteins 0.000 description 1
- 102100030254 Spermatogenesis-associated protein 2 Human genes 0.000 description 1
- 229910004164 TaMo Inorganic materials 0.000 description 1
- 229910004168 TaNb Inorganic materials 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- CFJRGWXELQQLSA-UHFFFAOYSA-N azanylidyneniobium Chemical compound [Nb]#N CFJRGWXELQQLSA-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000003635 deoxygenating effect Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000010891 electric arc Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000007888 film coating Substances 0.000 description 1
- 238000009501 film coating Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000001755 magnetron sputter deposition Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- NFFIWVVINABMKP-UHFFFAOYSA-N methylidynetantalum Chemical compound [Ta]#C NFFIWVVINABMKP-UHFFFAOYSA-N 0.000 description 1
- 238000004377 microelectronic Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000009103 reabsorption Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000005549 size reduction Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000009718 spray deposition Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 229910003468 tantalcarbide Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/004—Details
- H01G9/04—Electrodes or formation of dielectric layers thereon
- H01G9/048—Electrodes or formation of dielectric layers thereon characterised by their structure
- H01G9/052—Sintered electrodes
- H01G9/0525—Powder therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/14—Treatment of metallic powder
- B22F1/145—Chemical treatment, e.g. passivation or decarburisation
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/3407—Cathode assembly for sputtering apparatus, e.g. Target
- C23C14/3414—Metallurgical or chemical aspects of target preparation, e.g. casting, powder metallurgy
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C8/00—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C8/02—Pretreatment of the material to be coated
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C8/00—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C8/80—After-treatment
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/34—Gas-filled discharge tubes operating with cathodic sputtering
- H01J37/3411—Constructional aspects of the reactor
- H01J37/3414—Targets
- H01J37/3426—Material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12014—All metal or with adjacent metals having metal particles
- Y10T428/12028—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, etc.]
- Y10T428/12049—Nonmetal component
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12014—All metal or with adjacent metals having metal particles
- Y10T428/12028—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, etc.]
- Y10T428/12063—Nonparticulate metal component
- Y10T428/12104—Particles discontinuous
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Power Engineering (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Analytical Chemistry (AREA)
- Microelectronics & Electronic Packaging (AREA)
- General Chemical & Material Sciences (AREA)
- Powder Metallurgy (AREA)
- Physical Vapour Deposition (AREA)
- Electrodes Of Semiconductors (AREA)
Description
1. 冷間等方加圧、焼結、封入、熱間等方加圧、及び熱機械処理;
2. 冷間等方加圧、焼結、熱間等方加圧、及び熱機械処理;
3. 冷間等方加圧、封入、熱間等方加圧、及び熱機械処理;
4. 冷間等方加圧、封入、及び熱間等方加圧;
5. 封入、及び熱間等方加圧;
6. 冷間等方加圧、焼結、封入、押出し、及び熱機械処理;
7. 冷間等方加圧、焼結、押出し、及び熱機械処理;
8. 冷間等方加圧、焼結、及び押出し;
9. 冷間等方加圧、封入、押出し、及び熱機械処理;
10.冷間等方加圧、封入、及び押出し;
11.封入、及び押出し;
12.機械プレス成形、焼結、及び押出し;
13.冷間等方加圧、焼結、封入、鍛造、及び熱機械処理;
14.冷間等方加圧、封入、鍛造、及び熱機械処理;
15.冷間等方加圧、封入、及び鍛造;
16.冷間等方加圧、焼結、及び鍛造;
17.冷間等方加圧、焼結、及び圧延;
18.封入、及び鍛造;
19.封入、及び圧延;
20.冷間等方加圧、焼結、及び熱機械処理;
21.噴霧堆積;
22.機械プレス成形、及び焼結;並びに
23.機械プレス成形、焼結、再圧縮、及び再焼結。
Claims (3)
- 圧密された表面窒化金属粉末スパッタターゲットとバッキングプレートを含み、該金属粉末が、タンタル、ニオブ、タンタルの合金、又はニオブの合金であり、該金属粉末が、100ppm以下の酸素含有量と、40ppm〜10,000ppmの窒素含有量とを有し、かつ前記スパッタターゲットが、124.1〜275.8MPa(18,000〜40,000psi)の降伏強さと、20%以上の破断点伸びと、100μm以下の平均粒度とを有する、スパッタリングターゲットアセンブリ。
- 前記スパッタターゲットが、前記金属の表面上又は厚さ全体に及ぶ(111)の均一な一次組織を有する、請求項1に記載のスパッタリングターゲットアセンブリ。
- 前記スパッタターゲットが、前記金属の表面上又は厚さ全体に及ぶ(100)の均一な一次組織を有するか又は(100):(111)の均一な混合された組織を有する、請求項1に記載のスパッタリングターゲットアセンブリ。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US43846503P | 2003-01-07 | 2003-01-07 | |
US60/438,465 | 2003-01-07 | ||
PCT/US2004/000270 WO2004064114A2 (en) | 2003-01-07 | 2004-01-07 | Powder metallurgy sputtering targets and methods of producing same |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2006517612A JP2006517612A (ja) | 2006-07-27 |
JP2006517612A5 JP2006517612A5 (ja) | 2007-03-01 |
JP5006030B2 true JP5006030B2 (ja) | 2012-08-22 |
Family
ID=32713330
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2006500812A Expired - Fee Related JP5006030B2 (ja) | 2003-01-07 | 2004-01-07 | 粉末冶金スパッタリングターゲット及びその製造方法 |
Country Status (5)
Country | Link |
---|---|
US (3) | US7067197B2 (ja) |
EP (1) | EP1585844B1 (ja) |
JP (1) | JP5006030B2 (ja) |
TW (1) | TWI341337B (ja) |
WO (1) | WO2004064114A2 (ja) |
Families Citing this family (71)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20030002043A1 (en) * | 2001-04-10 | 2003-01-02 | Kla-Tencor Corporation | Periodic patterns and technique to control misalignment |
US7067849B2 (en) | 2001-07-17 | 2006-06-27 | Lg Electronics Inc. | Diode having high brightness and method thereof |
US7993773B2 (en) | 2002-08-09 | 2011-08-09 | Infinite Power Solutions, Inc. | Electrochemical apparatus with barrier layer protected substrate |
US8445130B2 (en) | 2002-08-09 | 2013-05-21 | Infinite Power Solutions, Inc. | Hybrid thin-film battery |
US8236443B2 (en) | 2002-08-09 | 2012-08-07 | Infinite Power Solutions, Inc. | Metal film encapsulation |
US8431264B2 (en) | 2002-08-09 | 2013-04-30 | Infinite Power Solutions, Inc. | Hybrid thin-film battery |
US8404376B2 (en) | 2002-08-09 | 2013-03-26 | Infinite Power Solutions, Inc. | Metal film encapsulation |
US8021778B2 (en) | 2002-08-09 | 2011-09-20 | Infinite Power Solutions, Inc. | Electrochemical apparatus with barrier layer protected substrate |
US20070264564A1 (en) | 2006-03-16 | 2007-11-15 | Infinite Power Solutions, Inc. | Thin film battery on an integrated circuit or circuit board and method thereof |
US8394522B2 (en) | 2002-08-09 | 2013-03-12 | Infinite Power Solutions, Inc. | Robust metal film encapsulation |
TWI341337B (en) * | 2003-01-07 | 2011-05-01 | Cabot Corp | Powder metallurgy sputtering targets and methods of producing same |
US8728285B2 (en) | 2003-05-23 | 2014-05-20 | Demaray, Llc | Transparent conductive oxides |
WO2005071135A2 (en) * | 2004-01-08 | 2005-08-04 | Cabot Corporation | Tantalum and other metals with (110) orientation |
WO2006055513A2 (en) * | 2004-11-18 | 2006-05-26 | Honeywell International Inc. | Methods of forming three-dimensional pvd targets |
US7959769B2 (en) | 2004-12-08 | 2011-06-14 | Infinite Power Solutions, Inc. | Deposition of LiCoO2 |
KR101021536B1 (ko) | 2004-12-08 | 2011-03-16 | 섬모픽스, 인코포레이티드 | LiCoO2의 증착 |
JP4936511B2 (ja) * | 2005-03-31 | 2012-05-23 | 富士フイルム株式会社 | 駆動装置、撮影装置及び携帯電話 |
CN100439559C (zh) * | 2005-04-08 | 2008-12-03 | 光洋应用材料科技股份有限公司 | 钽基化合物的陶瓷溅镀靶材及其应用方法和制备方法 |
EP1880035B1 (en) * | 2005-05-05 | 2021-01-20 | Höganäs Germany GmbH | Method for coating a substrate surface and coated product |
AU2006243448B2 (en) * | 2005-05-05 | 2011-09-01 | H.C. Starck Inc. | Coating process for manufacture or reprocessing of sputter targets and X-ray anodes |
US7708868B2 (en) * | 2005-07-08 | 2010-05-04 | Tosoh Smd, Inc. | Variable thickness plate for forming variable wall thickness physical vapor deposition target |
JP5114812B2 (ja) | 2006-03-07 | 2013-01-09 | キャボット コーポレイション | 変形させた金属部材の製造方法 |
US20070251819A1 (en) * | 2006-05-01 | 2007-11-01 | Kardokus Janine K | Hollow cathode magnetron sputtering targets and methods of forming hollow cathode magnetron sputtering targets |
US8062708B2 (en) | 2006-09-29 | 2011-11-22 | Infinite Power Solutions, Inc. | Masking of and material constraint for depositing battery layers on flexible substrates |
US20080078268A1 (en) | 2006-10-03 | 2008-04-03 | H.C. Starck Inc. | Process for preparing metal powders having low oxygen content, powders so-produced and uses thereof |
US8197781B2 (en) | 2006-11-07 | 2012-06-12 | Infinite Power Solutions, Inc. | Sputtering target of Li3PO4 and method for producing same |
DK2104753T3 (da) * | 2006-11-07 | 2014-09-29 | Starck H C Gmbh | Fremgangsmåde til belægning af et substrat og et belagt produkt |
US7776166B2 (en) * | 2006-12-05 | 2010-08-17 | Praxair Technology, Inc. | Texture and grain size controlled hollow cathode magnetron targets and method of manufacture |
US20080145688A1 (en) | 2006-12-13 | 2008-06-19 | H.C. Starck Inc. | Method of joining tantalum clade steel structures |
US20080210555A1 (en) * | 2007-03-01 | 2008-09-04 | Heraeus Inc. | High density ceramic and cermet sputtering targets by microwave sintering |
US20080233420A1 (en) * | 2007-03-23 | 2008-09-25 | Mccracken Colin G | Production of high-purity tantalum flake powder |
US20080229880A1 (en) * | 2007-03-23 | 2008-09-25 | Reading Alloys, Inc. | Production of high-purity tantalum flake powder |
US8197894B2 (en) | 2007-05-04 | 2012-06-12 | H.C. Starck Gmbh | Methods of forming sputtering targets |
JP5389802B2 (ja) * | 2007-08-06 | 2014-01-15 | エイチ.シー. スターク インコーポレイテッド | 組織の均一性が改善された高融点金属プレート |
US8250895B2 (en) * | 2007-08-06 | 2012-08-28 | H.C. Starck Inc. | Methods and apparatus for controlling texture of plates and sheets by tilt rolling |
US8702919B2 (en) * | 2007-08-13 | 2014-04-22 | Honeywell International Inc. | Target designs and related methods for coupled target assemblies, methods of production and uses thereof |
TWI441937B (zh) | 2007-12-21 | 2014-06-21 | Infinite Power Solutions Inc | 形成用於電解質薄膜之濺鍍靶材的方法 |
US8268488B2 (en) | 2007-12-21 | 2012-09-18 | Infinite Power Solutions, Inc. | Thin film electrolyte for thin film batteries |
KR101606183B1 (ko) | 2008-01-11 | 2016-03-25 | 사푸라스트 리써치 엘엘씨 | 박막 배터리 및 기타 소자를 위한 박막 캡슐화 |
DE102008005781A1 (de) * | 2008-01-23 | 2009-07-30 | Tradium Gmbh | Phlegmatisierte Metallpulver oder Legierungspulver und Verfahren bzw. Reaktionsgefäß zu deren Herstellung |
ES2302663B2 (es) * | 2008-02-28 | 2009-02-16 | Universidad Politecnica De Madrid | Procedimiento para la obtencion de peliculas de materiales semiconductores incorporando una banda intermedia. |
EP2266183B1 (en) | 2008-04-02 | 2018-12-12 | Sapurast Research LLC | Passive over/under voltage control and protection for energy storage devices associated with energy harvesting |
JP5172465B2 (ja) * | 2008-05-20 | 2013-03-27 | 三菱電機株式会社 | 放電表面処理用電極の製造方法および放電表面処理用電極 |
EP2319101B1 (en) | 2008-08-11 | 2015-11-04 | Sapurast Research LLC | Energy device with integral collector surface for electromagnetic energy harvesting and method thereof |
US8246903B2 (en) | 2008-09-09 | 2012-08-21 | H.C. Starck Inc. | Dynamic dehydriding of refractory metal powders |
KR101613671B1 (ko) | 2008-09-12 | 2016-04-19 | 사푸라스트 리써치 엘엘씨 | 전자기 에너지에 의해 데이터 통신을 하는 통합 도전성 표면을 가진 에너지 장치 및 그 통신 방법 |
US8043655B2 (en) * | 2008-10-06 | 2011-10-25 | H.C. Starck, Inc. | Low-energy method of manufacturing bulk metallic structures with submicron grain sizes |
US8508193B2 (en) | 2008-10-08 | 2013-08-13 | Infinite Power Solutions, Inc. | Environmentally-powered wireless sensor module |
EP2474056B1 (en) | 2009-09-01 | 2016-05-04 | Sapurast Research LLC | Printed circuit board with integrated thin film battery |
WO2011156392A1 (en) | 2010-06-07 | 2011-12-15 | Infinite Power Solutions, Inc. | Rechargeable, high-density electrochemical device |
EP2604719B1 (en) * | 2010-08-09 | 2020-11-11 | JX Nippon Mining & Metals Corporation | Tantalum spattering target |
JP5912559B2 (ja) | 2011-03-30 | 2016-04-27 | 田中貴金属工業株式会社 | FePt−C系スパッタリングターゲットの製造方法 |
JP5758204B2 (ja) | 2011-06-07 | 2015-08-05 | 日本発條株式会社 | チタン合金部材およびその製造方法 |
US8734896B2 (en) | 2011-09-29 | 2014-05-27 | H.C. Starck Inc. | Methods of manufacturing high-strength large-area sputtering targets |
TWI515316B (zh) | 2012-01-13 | 2016-01-01 | Tanaka Precious Metal Ind | FePt sputtering target and its manufacturing method |
CN103084567B (zh) * | 2012-11-25 | 2015-06-24 | 安徽普源分离机械制造有限公司 | 一种膜片阀阀杆的粉末冶金制备方法 |
EP3129176A1 (en) * | 2014-04-11 | 2017-02-15 | H.C. Starck Inc. | High purity refractory metal sputtering targets which have a uniform random texture manufactured by hot isostatic pressing high purity refractory metal powders |
CN107532287B (zh) * | 2015-05-22 | 2019-11-05 | 捷客斯金属株式会社 | 钽溅射靶及其制造方法 |
EP3339469A4 (en) * | 2016-03-25 | 2019-03-27 | JX Nippon Mining & Metals Corporation | TI-TA ALLOY SPUTTER TARGET AND MANUFACTURING METHOD THEREFOR |
CN106111993B (zh) * | 2016-07-28 | 2018-05-04 | 西北有色金属研究院 | 一种粉末冶金法制备铌合金板材的方法 |
WO2018197612A1 (en) | 2017-04-27 | 2018-11-01 | Basf Se | Preparation of powders of nitrided inorganic materials |
GB201803142D0 (en) | 2018-02-27 | 2018-04-11 | Rolls Royce Plc | A method of manufacturing an austenitc iron alloy |
KR102389784B1 (ko) | 2018-03-05 | 2022-04-22 | 글로벌 어드밴스드 메탈스 유에스에이, 아이엔씨. | 구형 분말을 함유하는 애노드 및 커패시터 |
EP3746240A2 (en) | 2018-03-05 | 2020-12-09 | Global Advanced Metals USA, Inc. | Spherical tantalum powder, products containing the same, and methods of making the same |
US20190271068A1 (en) * | 2018-03-05 | 2019-09-05 | Global Advanced Metals Usa, Inc. | Powder Metallurgy Sputtering Targets And Methods Of Producing Same |
RU2680082C1 (ru) * | 2018-05-31 | 2019-02-15 | Федеральное государственное бюджетное учреждение науки Федеральный исследовательский центр "Кольский научный центр Российской академии наук" (ФИЦ КНЦ РАН) | Способ изготовления анода конденсатора на основе вентильного металла |
US11289276B2 (en) | 2018-10-30 | 2022-03-29 | Global Advanced Metals Japan K.K. | Porous metal foil and capacitor anodes made therefrom and methods of making same |
EP3951004A4 (en) * | 2019-03-26 | 2022-12-14 | JX Nippon Mining & Metals Corporation | NIOBIUM SPRAYINGTARGET |
US11725270B2 (en) | 2020-01-30 | 2023-08-15 | Taiwan Semiconductor Manufacturing Co., Ltd. | PVD target design and semiconductor devices formed using the same |
CN111621753B (zh) * | 2020-07-29 | 2020-11-17 | 江苏集萃先进金属材料研究所有限公司 | 靶材坯料及其制作方法 |
CN113981390A (zh) * | 2021-10-29 | 2022-01-28 | 宁波江丰半导体科技有限公司 | 一种高纯低氧钽靶材的制备方法 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5242481A (en) * | 1989-06-26 | 1993-09-07 | Cabot Corporation | Method of making powders and products of tantalum and niobium |
ES2020131A6 (es) * | 1989-06-26 | 1991-07-16 | Cabot Corp | Procedimiento para la produccion de polvos de tantalo, niobio y sus aleaciones. |
DE69223479T2 (de) * | 1991-09-27 | 1998-04-02 | Hitachi Metals Ltd | Target zum reaktiven Sputtern sowie Verfahren zur Bildung eines Films unter Verwendung des Targets |
US5415829A (en) * | 1992-12-28 | 1995-05-16 | Nikko Kyodo Co., Ltd. | Sputtering target |
EP0665302B1 (en) | 1994-01-26 | 2000-05-03 | H.C. Starck, INC. | Nitriding tantalum powder |
US5863398A (en) | 1996-10-11 | 1999-01-26 | Johnson Matthey Electonics, Inc. | Hot pressed and sintered sputtering target assemblies and method for making same |
JP4012287B2 (ja) * | 1997-08-27 | 2007-11-21 | 株式会社ブリヂストン | スパッタリングターゲット盤 |
US6348113B1 (en) | 1998-11-25 | 2002-02-19 | Cabot Corporation | High purity tantalum, products containing the same, and methods of making the same |
JP5053471B2 (ja) | 1999-05-11 | 2012-10-17 | 株式会社東芝 | 配線膜の製造方法と電子部品の製造方法 |
JP2001020065A (ja) * | 1999-07-07 | 2001-01-23 | Hitachi Metals Ltd | スパッタリング用ターゲット及びその製造方法ならびに高融点金属粉末材料 |
US6261337B1 (en) * | 1999-08-19 | 2001-07-17 | Prabhat Kumar | Low oxygen refractory metal powder for powder metallurgy |
US6521173B2 (en) * | 1999-08-19 | 2003-02-18 | H.C. Starck, Inc. | Low oxygen refractory metal powder for powder metallurgy |
US6342133B2 (en) * | 2000-03-14 | 2002-01-29 | Novellus Systems, Inc. | PVD deposition of titanium and titanium nitride layers in the same chamber without use of a collimator or a shutter |
DE60136351D1 (de) | 2000-05-22 | 2008-12-11 | Cabot Corp | Hochreines niobmetall und erzeugnisse daraus und verfahren zu dessen herstellung |
US6887356B2 (en) * | 2000-11-27 | 2005-05-03 | Cabot Corporation | Hollow cathode target and methods of making same |
TWI341337B (en) * | 2003-01-07 | 2011-05-01 | Cabot Corp | Powder metallurgy sputtering targets and methods of producing same |
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2004
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- 2004-01-06 US US10/752,270 patent/US7067197B2/en not_active Expired - Lifetime
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TW200502435A (en) | 2005-01-16 |
US20060201583A1 (en) | 2006-09-14 |
US7601296B2 (en) | 2009-10-13 |
EP1585844A2 (en) | 2005-10-19 |
EP1585844B1 (en) | 2016-08-24 |
US20090324439A1 (en) | 2009-12-31 |
WO2004064114A3 (en) | 2005-01-20 |
JP2006517612A (ja) | 2006-07-27 |
US8168118B2 (en) | 2012-05-01 |
US7067197B2 (en) | 2006-06-27 |
WO2004064114A2 (en) | 2004-07-29 |
US20040141870A1 (en) | 2004-07-22 |
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