JP4970700B2 - （メタ）アクリル酸のｔ−Ｃ４〜Ｃ８−アルキルエステルの製造方法 - Google Patents

（メタ）アクリル酸のｔ−Ｃ４〜Ｃ８−アルキルエステルの製造方法 Download PDF

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JP4970700B2
JP4970700B2 JP2002516243A JP2002516243A JP4970700B2 JP 4970700 B2 JP4970700 B2 JP 4970700B2 JP 2002516243 A JP2002516243 A JP 2002516243A JP 2002516243 A JP2002516243 A JP 2002516243A JP 4970700 B2 JP4970700 B2 JP 4970700B2
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meth
acrylate
alkyl
evaporator
acrylic acid
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Japanese (ja)
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JP2004505102A (ja
Inventor
クロカー ループレヒト
ネストラー ゲルハルト
シュミット ヴェルナー
シュム ヴィンフリート
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/04—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/06—Evaporators with vertical tubes
    • B01D1/065—Evaporators with vertical tubes by film evaporating
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/09—Plural feed

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2002516243A 2000-07-28 2001-07-27 （メタ）アクリル酸のｔ−Ｃ４〜Ｃ８−アルキルエステルの製造方法 Expired - Lifetime JP4970700B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10036958A DE10036958A1 (de) 2000-07-28 2000-07-28 Verfahren zur Herstellung von tert.-C4-C8-Alkylestern der (Meth)acrylsäure
DE10036958.8 2000-07-28
PCT/EP2001/008713 WO2002010110A2 (de) 2000-07-28 2001-07-27 Verfahren zur herstellung von tert.-c4-c8-alkylestern der (meth)acrylsäure und darin verwandter fallfilmverdampfer

Publications (2)

Publication Number Publication Date
JP2004505102A JP2004505102A (ja) 2004-02-19
JP4970700B2 true JP4970700B2 (ja) 2012-07-11

Family

ID=7650632

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2002516243A Expired - Lifetime JP4970700B2 (ja) 2000-07-28 2001-07-27 （メタ）アクリル酸のｔ−Ｃ４〜Ｃ８−アルキルエステルの製造方法

Country Status (6)

Country Link
US (1) US6998026B2 (de)
EP (1) EP1305276B1 (de)
JP (1) JP4970700B2 (de)
AU (1) AU2001291689A1 (de)
DE (2) DE10036958A1 (de)
WO (1) WO2002010110A2 (de)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4278058B2 (ja) 2004-11-29 2009-06-10 ボッシュ株式会社 作動液リザーバおよび液圧制御ユニット
DE102006062258A1 (de) * 2006-12-22 2008-06-26 Basf Se Verfahren zum Übertragen von Wärme auf ein wenigstens ein (Meth)acrylmonomeres enthaltendes flüssiges Gemsich
EP2017255A1 (de) 2007-07-19 2009-01-21 Basf Se Verfahren zur Herstellung von teritären Alkylestern der (Meth)Acrylsäure mit mindestens 4 Kohlenstoffatomen im Alkylrest
DE102015205752A1 (de) 2015-03-31 2016-10-20 Basf Se Herstellung von tert-Butylestern aliphatischer Carbonsäuren
JP6890591B2 (ja) 2015-12-15 2021-06-18 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ エチレン性不飽和カルボン酸のｔｅｒｔ−ブチルエステルの製造
DE202016006882U1 (de) 2016-11-10 2016-11-23 Basf Se Verfilmbare Dispersionen mit tert-Butyl(meth)acrylat
FR3060000B1 (fr) * 2016-12-08 2020-05-01 Arkema France Procede pour eviter le depot de polymeres dans un procede de purification d'acide (meth)acrylique.
US10906862B2 (en) * 2016-12-21 2021-02-02 Basf Se Process for isolating pure butyl acrylate from crude butyl acrylate by distillation, where butyl is n-butyl or isobutyl
KR102519200B1 (ko) * 2016-12-21 2023-04-06 바스프 에스이 조질 t-부틸 (메트)아크릴레이트로부터 증류에 의해 순수 t-부틸 (메트)아크릴레이트를 단리하는 방법
WO2024126176A1 (de) 2022-12-15 2024-06-20 Basf Se Verfahren zur kontinuierlichen herstellung von tert.-butyl(meth)acrylat

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US3172905A (en) * 1965-03-09 Catalytic preparation of esters from tertiary olefins and carboxylic acids
US995776A (en) * 1910-07-18 1911-06-20 Joseph E Dunn Evaporating and concentrating apparatus.
US1028792A (en) * 1910-12-28 1912-06-04 Sanborn Evaporator Company Evaporating apparatus.
CH225352A (de) * 1941-05-18 1943-01-31 Rosenblads Patenter Ab Röhrenverdampfer für Berieselungsbetrieb mit Einrichtung zur Verteilung der Flüssigkeit.
US2392255A (en) * 1943-10-20 1946-01-01 John J Mcandrews Evaporator
BE590370A (de) * 1959-04-29 1900-01-01
DE1128428B (de) 1959-08-08 1962-04-26 Hoechst Ag Verfahren zur Herstellung von Carbonsaeure-tertiaer-alkylestern und zur Abtrennung und bzw. oder Gewinnung von tertiaeren Olefinen aus diese enthaltenden Kohlenwasserstoffgemischen
DE1135897B (de) 1959-12-28 1962-09-06 Basf Ag Verfahren zur Herstellung von Tertiaer-butylestern der Acrylsaeure oder von in ª‡-Stellung durch Chlor oder Alkylreste substituierter Acrylsaeure
US3087962A (en) * 1960-01-21 1963-04-30 Rohm & Haas Process of making esters of acrylic and methacrylic acids
US3082246A (en) * 1960-02-17 1963-03-19 Texaco Inc Preparation of tertiary esters
US3031495A (en) * 1960-05-13 1962-04-24 Sinclair Refining Co Preparation of tertiary alkyl formate and acetate
DE1249857B (de) * 1961-03-29 1967-09-14 Badische Anilin &. Soda-Fabnk Aktiengesellschaft, Ludwigshaf en/Rhem Verfahren zur kontinuierlichen gewinnung von carbonsäureestern tertiärer alkohole.
US3088969A (en) * 1961-04-21 1963-05-07 Standard Oil Co Manufacture of t-butyl esters of unsaturated acids
US3620283A (en) * 1969-02-04 1971-11-16 Artisan Ind Falling film evaporator stripper
JPS4924898B1 (de) 1970-12-26 1974-06-26
DE2121123C3 (de) * 1971-04-29 1980-06-12 Basf Ag, 6700 Ludwigshafen Verfahren zum Abtrennen von Wasser aus wäßrigen Lösungen von Acrylsäure durch azeotrope Destillation
DE2212816C3 (de) * 1972-03-16 1974-12-12 Wiegand Karlsruhe Gmbh, 7505 Ettlingen Vorrichtung zur gleichmäßigen Verteilung einzudampfender Flüssigkeit in einem Fallstromverdampfer
US4094734A (en) * 1973-10-15 1978-06-13 Henderson Industrial Corporation Evaporator and treatment of viscous brines
CH586567A5 (de) * 1974-10-09 1977-04-15 Luwa Ag
DE2931553A1 (de) 1979-08-03 1981-02-26 Basf Ag Verfahren zur stabilisierung monomerer acrylsaeureester gegen vorzeitige polymerisation
JPS5772939A (en) * 1980-10-24 1982-05-07 Celanese Corp Improved manufacture of ethyl acrylate
DE3105399A1 (de) 1981-02-14 1982-10-21 EC Erdölchemie GmbH, 5000 Köln Verfahren zur herstellung von carbonsaeureestern
JPS60130546A (ja) 1983-12-20 1985-07-12 Mitsubishi Petrochem Co Ltd １，２−不飽和カルボン酸の精製方法
JPH07116103B2 (ja) 1986-11-27 1995-12-13 三菱レイヨン株式会社 メタクリル酸ｔ−ブチルの製造法
DE3709652A1 (de) * 1987-03-24 1988-10-06 Thermo Consulting Heidelberg Vorrichtung zum verdampfen von fluessigkeiten bzw. absorbieren oder entgasen von zwei- oder mehrstoff-loesungen in innenrohr-fallfilm-bauweise
US5246541A (en) * 1991-05-14 1993-09-21 A. Ahlstrom Corporation Evaporator for liquid solutions
FI93427B (fi) * 1993-04-01 1994-12-30 Tampella Power Oy Putoavan kalvon periaatteella toimiva haihdutin
FI101644B (fi) * 1994-02-25 1998-07-31 Ahlstrom Machinery Oy Lämmönsiirtoelementti ja menetelmä sen valmistamiseksi
DE19602640A1 (de) * 1996-01-25 1997-07-31 Basf Ag Verfahren und Verdampfer zur Verdampfung oxidationsempfindlicher Verbindungen
JP2001131116A (ja) * 1999-11-08 2001-05-15 Nippon Shokubai Co Ltd 易重合性物質含有液の蒸留方法
DE19957458A1 (de) * 1999-11-29 2001-05-31 Bayer Ag Strangverdampfer

Also Published As

Publication number Publication date
DE10036958A1 (de) 2002-02-07
DE50102341D1 (de) 2004-06-24
WO2002010110A3 (de) 2002-09-19
EP1305276B1 (de) 2004-05-19
US6998026B2 (en) 2006-02-14
JP2004505102A (ja) 2004-02-19
AU2001291689A1 (en) 2002-02-13
WO2002010110A2 (de) 2002-02-07
EP1305276A2 (de) 2003-05-02
US20030127315A1 (en) 2003-07-10

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