JP3621928B2 - カーボンナノ微粒子の製造方法,カーボンナノ微粒子の製造装置 - Google Patents

カーボンナノ微粒子の製造方法,カーボンナノ微粒子の製造装置 Download PDF

Info

Publication number
JP3621928B2
JP3621928B2 JP2002103825A JP2002103825A JP3621928B2 JP 3621928 B2 JP3621928 B2 JP 3621928B2 JP 2002103825 A JP2002103825 A JP 2002103825A JP 2002103825 A JP2002103825 A JP 2002103825A JP 3621928 B2 JP3621928 B2 JP 3621928B2
Authority
JP
Japan
Prior art keywords
electrode
carbon
arc
gas
arc discharge
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2002103825A
Other languages
English (en)
Japanese (ja)
Other versions
JP2003300713A (ja
JP2003300713A5 (enExample
Inventor
浩史 滝川
光邦 池田
茂生 伊藤
智徳 田原
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tokai Carbon Co Ltd
Futaba Corp
Original Assignee
Tokai Carbon Co Ltd
Futaba Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tokai Carbon Co Ltd, Futaba Corp filed Critical Tokai Carbon Co Ltd
Priority to JP2002103825A priority Critical patent/JP3621928B2/ja
Priority to TW092107357A priority patent/TWI271381B/zh
Priority to KR1020030021329A priority patent/KR100840500B1/ko
Priority to US10/407,666 priority patent/US6989083B2/en
Priority to CNB031429092A priority patent/CN100503430C/zh
Publication of JP2003300713A publication Critical patent/JP2003300713A/ja
Publication of JP2003300713A5 publication Critical patent/JP2003300713A5/ja
Application granted granted Critical
Publication of JP3621928B2 publication Critical patent/JP3621928B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/087—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • B01J19/088—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/16—Preparation
    • C01B32/162—Preparation characterised by catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/0015—Controlling the temperature by thermal insulation means
    • B01J2219/00155—Controlling the temperature by thermal insulation means using insulating materials or refractories
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0803—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • B01J2219/0805—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges
    • B01J2219/0807—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges involving electrodes
    • B01J2219/0809—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges involving electrodes employing two or more electrodes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0803—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • B01J2219/0805—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges
    • B01J2219/0807—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges involving electrodes
    • B01J2219/0822—The electrode being consumed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0803—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • B01J2219/0805—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges
    • B01J2219/0807—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges involving electrodes
    • B01J2219/0824—Details relating to the shape of the electrodes
    • B01J2219/0835—Details relating to the shape of the electrodes substantially flat
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0803—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • B01J2219/0805—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges
    • B01J2219/0807—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges involving electrodes
    • B01J2219/0837—Details relating to the material of the electrodes
    • B01J2219/0839—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0871—Heating or cooling of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0873—Materials to be treated
    • B01J2219/0881—Two or more materials
    • B01J2219/0886—Gas-solid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0873—Materials to be treated
    • B01J2219/0892—Materials to be treated involving catalytically active material
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/34—Length
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/36—Diameter

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Composite Materials (AREA)
  • Toxicology (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Carbon And Carbon Compounds (AREA)
JP2002103825A 2002-04-05 2002-04-05 カーボンナノ微粒子の製造方法,カーボンナノ微粒子の製造装置 Expired - Fee Related JP3621928B2 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
JP2002103825A JP3621928B2 (ja) 2002-04-05 2002-04-05 カーボンナノ微粒子の製造方法,カーボンナノ微粒子の製造装置
TW092107357A TWI271381B (en) 2002-04-05 2003-04-01 Method for preparing carbon nano-fine particle, apparatus for preparing the same, and mono layer carbon nanotube
KR1020030021329A KR100840500B1 (ko) 2002-04-05 2003-04-04 카본나노 미립자의 제조방법, 카본나노 미립자의 제조장치및 단층 카본나노튜브
US10/407,666 US6989083B2 (en) 2002-04-05 2003-04-04 Method for preparing carbon nano-fine particle, apparatus for preparing the same and mono-layer carbon nanotube
CNB031429092A CN100503430C (zh) 2002-04-05 2003-04-05 制备碳纳米细颗粒的方法和装置及单层碳纳米管

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2002103825A JP3621928B2 (ja) 2002-04-05 2002-04-05 カーボンナノ微粒子の製造方法,カーボンナノ微粒子の製造装置

Publications (3)

Publication Number Publication Date
JP2003300713A JP2003300713A (ja) 2003-10-21
JP2003300713A5 JP2003300713A5 (enExample) 2004-09-02
JP3621928B2 true JP3621928B2 (ja) 2005-02-23

Family

ID=28672259

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2002103825A Expired - Fee Related JP3621928B2 (ja) 2002-04-05 2002-04-05 カーボンナノ微粒子の製造方法,カーボンナノ微粒子の製造装置

Country Status (5)

Country Link
US (1) US6989083B2 (enExample)
JP (1) JP3621928B2 (enExample)
KR (1) KR100840500B1 (enExample)
CN (1) CN100503430C (enExample)
TW (1) TWI271381B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103101902A (zh) * 2013-01-28 2013-05-15 深圳青铜剑电力电子科技有限公司 一种纳米材料的制备设备

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3826108B2 (ja) * 2002-04-24 2006-09-27 キヤノン株式会社 成膜装置及び成膜方法
TWI251580B (en) * 2002-08-02 2006-03-21 Ind Tech Res Inst Preparation of magnetic metal filled carbon nanocapsules
JPWO2004069743A1 (ja) * 2003-02-10 2006-05-25 日本電気株式会社 ナノカーボンの製造装置およびナノカーボンの製造方法
JPWO2004103902A1 (ja) * 2003-05-20 2006-07-20 日本電気株式会社 カーボンナノホーン製造装置およびカーボンナノホーンの製造方法
WO2005061382A1 (en) * 2003-12-24 2005-07-07 Nanometrix Inc. Continuous production of carbon nanotubes
JP4012516B2 (ja) * 2004-03-30 2007-11-21 浩史 滝川 カーボンナノバルーン構造体の製造方法
FR2872826B1 (fr) * 2004-07-07 2006-09-15 Commissariat Energie Atomique Croissance a basse temperature de nanotubes de carbone orientes
KR100707199B1 (ko) * 2005-07-12 2007-04-13 삼성전자주식회사 H2o 플라즈마를 이용한 단일벽 탄소나노튜브의 저온성장방법
CN100482582C (zh) * 2005-08-05 2009-04-29 鸿富锦精密工业(深圳)有限公司 碳纳米管制备方法及装置
JP5330035B2 (ja) * 2008-03-21 2013-10-30 国立大学法人東北大学 カーボンナノチューブおよびその製造方法
US8211100B2 (en) * 2009-01-12 2012-07-03 Tyco Healthcare Group Lp Energy delivery algorithm for medical devices based on maintaining a fixed position on a tissue electrical conductivity v. temperature curve
KR20140038411A (ko) * 2011-04-15 2014-03-28 가부시키가이샤 간쿄우 에네루기 나노 기쥬츠 겡큐쇼 카본 나노 재료 제조 장치 및 그 이용
RU2476620C1 (ru) * 2011-09-12 2013-02-27 Федеральное государственное унитарное предприятие "Научно-исследовательский институт физических проблем им. Ф.В. Лукина" Устройство и способ получения наночастиц
JP6414404B2 (ja) * 2014-07-18 2018-10-31 日新電機株式会社 陰極部材及びこれを用いたプラズマ装置
CN104609390A (zh) * 2015-01-20 2015-05-13 北京清大际光科技发展有限公司 一种电弧法制备碳纳米角的方法
US10813257B2 (en) * 2016-09-05 2020-10-20 Nec Corporation Electromagnetic wave absorbing material
CN108383105A (zh) * 2018-04-28 2018-08-10 青岛科技大学 一种滚筒式电弧法分散碳纳米管的装置
JP2020191164A (ja) * 2019-05-20 2020-11-26 東芝ライテック株式会社 ヒータ
CN112744805B (zh) * 2021-01-21 2022-07-26 宁波埃氪新材料科技有限公司 一种电极喷射装置、碳纳米管反应器及碳纳米管制备方法
KR102768387B1 (ko) * 2021-12-07 2025-02-19 한국생산기술연구원 연속식 송연 탄소입자 제조장치, 및 그 제조방법

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4234812B2 (ja) 1998-07-25 2009-03-04 独立行政法人科学技術振興機構 単層カーボンナノホーン構造体とその製造方法
JP3606232B2 (ja) * 2001-06-01 2005-01-05 富士ゼロックス株式会社 炭素構造体の製造装置および製造方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103101902A (zh) * 2013-01-28 2013-05-15 深圳青铜剑电力电子科技有限公司 一种纳米材料的制备设备

Also Published As

Publication number Publication date
US6989083B2 (en) 2006-01-24
TW200400919A (en) 2004-01-16
KR20030079801A (ko) 2003-10-10
KR100840500B1 (ko) 2008-06-23
JP2003300713A (ja) 2003-10-21
TWI271381B (en) 2007-01-21
CN100503430C (zh) 2009-06-24
US20030188963A1 (en) 2003-10-09
CN1456497A (zh) 2003-11-19

Similar Documents

Publication Publication Date Title
KR100840500B1 (ko) 카본나노 미립자의 제조방법, 카본나노 미립자의 제조장치및 단층 카본나노튜브
JP3825336B2 (ja) ナノカーボンの製造方法及びナノカーボンの製造装置
JP3754417B2 (ja) 二重壁炭素ナノチューブ並びにその製造および使用方法
US6887451B2 (en) Process for preparing carbon nanotubes
JP3986711B2 (ja) 単層カーボンナノチューブの製造方法
US7364709B2 (en) Manufacturing apparatus and method for carbon nanotube
KR100562975B1 (ko) 나노튜브의 제조방법 및 이 방법을 이용하여 제조된나노튜브, 나노튜브의 제조장치, 나노튜브의 패턴화 방법및 이 방법을 이용하여 패턴화된 나노튜브 기재 및 이패턴화된 나노튜브 기재를 이용한 전자방출원
Zeng et al. Synthesis and application of carbon nanotubes
JP2000277003A (ja) 電子放出源の製造方法及び電子放出源
CN101370734A (zh) 用富勒烯官能化的碳纳米管
JP2003300713A5 (enExample)
JP2002263496A (ja) 触媒組成物、その製造方法及びカーボンナノファイバーの製造方法
JP5647827B2 (ja) カーボンナノ材料及びその利用
JP4572319B2 (ja) カーボンナノホーンの製造方法及び製造装置
JP2003277029A (ja) カーボンナノチューブ及びその製造方法
JP3885719B2 (ja) グラフェンシート筒の先端部の一部又は全部が破れているカーボンナノチューブの製造方法及び製造装置
Yin et al. Postgrowth processing of carbon nanotube arrays-enabling new functionalities and applications
JP3602092B2 (ja) ナノカーボンの製造方法、ナノカーボンの製造装置、ナノカーボンのパターン化方法
JP4339870B2 (ja) ナノカーボンの製造方法及びナノカーボンの製造装置
JP2005263523A (ja) メソサイズ微粒子およびその製造方法
JP3861857B2 (ja) カーボンナノチューブテープの製造方法
JP4615900B2 (ja) カーボンナノチューブ、カーボンナノワイヤおよびカーボンナノオニオンの製造方法
Dimitrov et al. Production, purification, characterization, and application of CNTs
Thapa Electron Field Emission and Electrochemical Lithiation Properties of Vertically Aligned Carbon Nanotube Arrays Grown Directly on Metal Substrates
JP3915119B2 (ja) カーボンナノチューブを含むテープ状物質の回収方法

Legal Events

Date Code Title Description
A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20040817

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20041014

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20041116

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20041119

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20071126

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20081126

Year of fee payment: 4

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20081126

Year of fee payment: 4

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20091126

Year of fee payment: 5

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20101126

Year of fee payment: 6

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20111126

Year of fee payment: 7

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20111126

Year of fee payment: 7

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121126

Year of fee payment: 8

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121126

Year of fee payment: 8

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20131126

Year of fee payment: 9

LAPS Cancellation because of no payment of annual fees