JP2928189B2 - 多孔性複合酸化物の製造方法 - Google Patents
多孔性複合酸化物の製造方法Info
- Publication number
- JP2928189B2 JP2928189B2 JP9063635A JP6363597A JP2928189B2 JP 2928189 B2 JP2928189 B2 JP 2928189B2 JP 9063635 A JP9063635 A JP 9063635A JP 6363597 A JP6363597 A JP 6363597A JP 2928189 B2 JP2928189 B2 JP 2928189B2
- Authority
- JP
- Japan
- Prior art keywords
- oxide source
- porous composite
- psi
- solution
- silicon oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000002131 composite material Substances 0.000 title claims description 12
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 22
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 16
- 229910052814 silicon oxide Inorganic materials 0.000 claims description 14
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 12
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 239000004115 Sodium Silicate Substances 0.000 claims description 4
- 150000004645 aluminates Chemical class 0.000 claims description 4
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 229910001388 sodium aluminate Inorganic materials 0.000 claims description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 4
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 4
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 3
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 2
- 239000011259 mixed solution Substances 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 239000010703 silicon Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 230000003647 oxidation Effects 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- 239000011148 porous material Substances 0.000 description 41
- 229910000323 aluminium silicate Inorganic materials 0.000 description 15
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 14
- 239000003054 catalyst Substances 0.000 description 9
- 238000009826 distribution Methods 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 239000000843 powder Substances 0.000 description 6
- 239000000376 reactant Substances 0.000 description 4
- 238000006555 catalytic reaction Methods 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000009827 uniform distribution Methods 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000000908 ammonium hydroxide Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000002407 reforming Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Chemical compound [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/12—Silica and alumina
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/03—Precipitation; Co-precipitation
- B01J37/036—Precipitation; Co-precipitation to form a gel or a cogel
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/14—Pore volume
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/16—Pore diameter
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Catalysts (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1019960029309A KR100195111B1 (ko) | 1996-07-19 | 1996-07-19 | 다공성 복합 산화물의 제조방법 |
KR199629309 | 1996-07-19 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH1036111A JPH1036111A (ja) | 1998-02-10 |
JP2928189B2 true JP2928189B2 (ja) | 1999-08-03 |
Family
ID=19466849
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP9063635A Expired - Fee Related JP2928189B2 (ja) | 1996-07-19 | 1997-03-17 | 多孔性複合酸化物の製造方法 |
Country Status (6)
Country | Link |
---|---|
JP (1) | JP2928189B2 (it) |
KR (1) | KR100195111B1 (it) |
CN (1) | CN1074303C (it) |
BR (1) | BR9701084A (it) |
GB (1) | GB2315430B (it) |
IT (1) | IT1289954B1 (it) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TWI279848B (en) | 2004-11-04 | 2007-04-21 | Ind Tech Res Inst | Structure and method for forming a heat-prevented layer on plastic substrate |
CN101388414B (zh) * | 2004-11-05 | 2011-01-26 | 财团法人工业技术研究院 | 塑料基板上的阻热结构 |
KR100761452B1 (ko) * | 2006-11-06 | 2007-10-04 | 한양대학교 산학협력단 | 화학적 합성에 의한 미립자 시멘트의 제조방법 및 이를이용한 콘크리트 제조방법 |
KR101142398B1 (ko) * | 2009-08-17 | 2012-05-08 | (주)한천자원 | 석탄계 분탄을 이용한 성형탄 제조방법 |
CN103055891A (zh) * | 2012-12-03 | 2013-04-24 | 天津大学 | 非晶合金条带上采用恒电压脱合金法制备掺杂Pd的纳米多孔二氧化钛薄膜的方法 |
CN114763543A (zh) | 2021-01-15 | 2022-07-19 | 百瑞全球有限公司 | 膜状固定化细胞、多肽、寡肽或蛋白质及其制备方法 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1413874A (en) * | 1973-01-10 | 1975-11-12 | Atlantic Richfield Co | Process for hydrotreating high nitrogen feedstocks and a catalyst for use therein |
US3974099A (en) * | 1975-04-08 | 1976-08-10 | W. R. Grace & Co. | High activity amorphous silica-alumina catalyst |
US4181532A (en) * | 1975-10-22 | 1980-01-01 | United Kingdom Atomic Energy Authority | Production of colloidal dispersions |
US4559321A (en) * | 1985-01-28 | 1985-12-17 | Shell Oil Company | Process for producing wide pore catalyst supports |
IT1219692B (it) * | 1988-05-06 | 1990-05-24 | Eniricerche Spa | Gel di silice e allumina cataliticamente attivo e procedimento per la sua preparazione |
JPH0655276B2 (ja) * | 1990-02-28 | 1994-07-27 | 富田製薬株式会社 | アンモニウムイオン選択性吸着剤の製造法 |
GB2276486A (en) * | 1993-02-25 | 1994-09-28 | Ronald William Bennett | Combined clamp/tuning means for a guitar string |
BE1007148A3 (fr) * | 1993-05-17 | 1995-04-11 | Solvay | Support pour catalyseurs, procede pour la fabrication d'un gel precurseur d'un support pour catalyseurs, procede de preparation d'un support pour catalyseurs, catalyseur pour la polymerisation d'olefines et procede pour la polymerisation d'olefines au moyen de ce catalyseur. |
IT1265320B1 (it) * | 1993-12-22 | 1996-10-31 | Eniricerche Spa | Procedimento per la preparazione di silico-allumine amorfe cataliticamente attive |
US5436681A (en) * | 1994-04-12 | 1995-07-25 | Michaels; Brian A. | Apparatus and method for screening individuals for ametropic conditions |
BE1008640A7 (fr) * | 1994-09-14 | 1996-07-02 | Messadek Jallal | Methodes de preparations de xerogels silice-alumine. |
ATE167641T1 (de) * | 1994-09-22 | 1998-07-15 | Hoffmann La Roche | Heterogenen katalysatoren |
-
1996
- 1996-07-19 KR KR1019960029309A patent/KR100195111B1/ko not_active IP Right Cessation
-
1997
- 1997-01-27 GB GB9701614A patent/GB2315430B/en not_active Expired - Fee Related
- 1997-02-21 IT IT97MI000382A patent/IT1289954B1/it active IP Right Grant
- 1997-02-26 BR BR9701084A patent/BR9701084A/pt not_active IP Right Cessation
- 1997-02-28 CN CN97103418A patent/CN1074303C/zh not_active Expired - Fee Related
- 1997-03-17 JP JP9063635A patent/JP2928189B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
GB2315430B (en) | 1999-04-07 |
BR9701084A (pt) | 1998-12-15 |
ITMI970382A1 (it) | 1998-08-21 |
CN1074303C (zh) | 2001-11-07 |
GB2315430A (en) | 1998-02-04 |
KR980009114A (ko) | 1998-04-30 |
CN1171295A (zh) | 1998-01-28 |
IT1289954B1 (it) | 1998-10-19 |
GB9701614D0 (en) | 1997-03-19 |
JPH1036111A (ja) | 1998-02-10 |
KR100195111B1 (ko) | 1999-06-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 19990413 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
LAPS | Cancellation because of no payment of annual fees |