JP2650144B2 - アジンの合成方法と、ヒドラジン製造への応用 - Google Patents
アジンの合成方法と、ヒドラジン製造への応用Info
- Publication number
- JP2650144B2 JP2650144B2 JP1345075A JP34507589A JP2650144B2 JP 2650144 B2 JP2650144 B2 JP 2650144B2 JP 1345075 A JP1345075 A JP 1345075A JP 34507589 A JP34507589 A JP 34507589A JP 2650144 B2 JP2650144 B2 JP 2650144B2
- Authority
- JP
- Japan
- Prior art keywords
- working fluid
- azine
- reaction
- compound
- distillation column
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
- C07C241/02—Preparation of hydrazines
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/16—Hydrazine; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/72—Hydrazones
- C07C251/88—Hydrazones having also the other nitrogen atom doubly-bound to a carbon atom, e.g. azines
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Plural Heterocyclic Compounds (AREA)
- Diaphragms For Electromechanical Transducers (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR896803 | 1989-05-24 | ||
| FR8906803A FR2647444B1 (enExample) | 1989-05-24 | 1989-05-24 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH02311448A JPH02311448A (ja) | 1990-12-27 |
| JP2650144B2 true JP2650144B2 (ja) | 1997-09-03 |
Family
ID=9381969
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1345075A Expired - Fee Related JP2650144B2 (ja) | 1989-05-24 | 1989-12-29 | アジンの合成方法と、ヒドラジン製造への応用 |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US6605265B1 (enExample) |
| EP (1) | EP0399866B1 (enExample) |
| JP (1) | JP2650144B2 (enExample) |
| KR (1) | KR940000059B1 (enExample) |
| AT (1) | ATE118760T1 (enExample) |
| AU (1) | AU625504B2 (enExample) |
| CA (1) | CA2017358C (enExample) |
| DE (1) | DE69017081T2 (enExample) |
| DK (1) | DK0399866T3 (enExample) |
| ES (1) | ES2068352T3 (enExample) |
| FI (1) | FI104167B (enExample) |
| FR (1) | FR2647444B1 (enExample) |
| GR (1) | GR3015800T3 (enExample) |
| IE (1) | IE70760B1 (enExample) |
| NO (1) | NO173091C (enExample) |
| PT (1) | PT94135B (enExample) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2062674T5 (es) * | 1990-11-23 | 2002-04-16 | Atofina | Procedimiento de sintesis de azinas. |
| FR2677648B1 (fr) * | 1991-06-12 | 1993-08-27 | Atochem | Procede pour reduire la teneur en co2 dans les reacteurs de synthese d'azines. |
| JP3962872B2 (ja) * | 1995-08-14 | 2007-08-22 | 三菱瓦斯化学株式会社 | ケタジンの合成方法 |
| FR2778659B1 (fr) * | 1998-05-14 | 2000-06-23 | Atochem Elf Sa | Procede de preparation d'hydrate d'hydrazine |
| FR2778660B1 (fr) * | 1998-05-14 | 2000-06-23 | Atochem Elf Sa | Procede de preparation d'hydrate d'hydrazine |
| FR2782717B1 (fr) | 1998-08-26 | 2000-09-29 | Atochem Elf Sa | Procede de fabrication d'hydrate d'hydrazine a partir d'azine de la methyl ethyl cetone |
| FR2784376B1 (fr) * | 1998-10-13 | 2000-12-08 | Atochem Elf Sa | Procede de preparation d'hydrazine |
| FR2787437B1 (fr) * | 1998-12-22 | 2001-02-09 | Atochem Elf Sa | Procede de fabrication d'hydrazine par hydrolyse d'une azine |
| FR2832142A1 (fr) * | 2001-11-09 | 2003-05-16 | Jean Pierre Schirmann | Procede ameliore de fabrication d'hydrate d'hydrazine |
| FR2959568A1 (fr) | 2010-04-28 | 2011-11-04 | Commissariat Energie Atomique | Procede et dispositif pour detecter et quantifier un analyte avec recyclage des reactifs |
| WO2018065997A1 (en) | 2016-10-03 | 2018-04-12 | Council Of Scientific & Industrial Research | An improved process for production of hydrazine hydrate |
| FR3096048B1 (fr) | 2019-05-16 | 2021-04-30 | Arkema France | Procede ameliore de preparation d'hydrate d'hydrazine avec recyclage oxime |
| FR3096049B1 (fr) | 2019-05-16 | 2021-12-17 | Arkema France | Procede ameliore de preparation d'hydrate d'hydrazine avec recyclage pyrazoline |
| FR3130815B1 (fr) | 2021-12-21 | 2025-02-28 | Arkema France | Procede de preparation d'hydrate d'hydrazine en presence d’un agent anti-mousse |
| FR3137086B1 (fr) | 2022-06-24 | 2025-05-23 | Arkema France | Procede de preparation d'hydrate d'hydrazine utilisant des reacteurs en cascade |
| CN115924864B (zh) * | 2022-12-23 | 2024-09-06 | 中国天辰工程有限公司 | 一种丁酮连氮水解制备水合肼的方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2120517A5 (enExample) * | 1971-01-07 | 1972-08-18 | Ugine Kuhlmann | |
| DE2326197A1 (de) * | 1973-05-23 | 1974-12-12 | Degussa | Verfahren zur herstellung von ketazinen |
| DE2344604A1 (de) * | 1973-09-05 | 1975-03-27 | Bayer Ag | Verfahren zur herstellung von azinen |
| FR2260569B1 (enExample) * | 1974-02-08 | 1978-06-16 | Ugine Kuhlmann | |
| DE2436335A1 (de) * | 1974-07-27 | 1976-02-05 | Bayer Ag | Verfahren zur aufbereitung von syntheseloesungen bei der hydrazinherstellung |
| US4013758A (en) * | 1975-08-07 | 1977-03-22 | Hans Osborg | Process for preparing hydrazines |
| FR2323635A1 (fr) * | 1975-09-10 | 1977-04-08 | Ugine Kuhlmann | Procede de preparation de solutions concentrees d'hydrate d'hydrazine |
| FR2324618A1 (fr) * | 1975-09-17 | 1977-04-15 | Ugine Kuhlmann | Nouveau procede de preparation d'azines |
| JPS58120507A (ja) * | 1982-01-14 | 1983-07-18 | Showa Denko Kk | ヒドラジンの連続的製造方法 |
| JPS60171205A (ja) * | 1984-02-17 | 1985-09-04 | Mitsubishi Gas Chem Co Inc | ヒドラジンハロゲン化水素酸塩の製法 |
| FR2571711A1 (fr) * | 1984-10-16 | 1986-04-18 | Atochem | Procede de fabrication d'hydrate d'hydrazine |
| US4888160A (en) * | 1985-12-20 | 1989-12-19 | J.M. Huber Corporation | Process for producing calcium carbonate and products thereof |
-
1989
- 1989-05-24 FR FR8906803A patent/FR2647444B1/fr not_active Expired - Lifetime
- 1989-12-29 JP JP1345075A patent/JP2650144B2/ja not_active Expired - Fee Related
-
1990
- 1990-05-09 DE DE69017081T patent/DE69017081T2/de not_active Expired - Fee Related
- 1990-05-09 AT AT90401224T patent/ATE118760T1/de not_active IP Right Cessation
- 1990-05-09 ES ES90401224T patent/ES2068352T3/es not_active Expired - Lifetime
- 1990-05-09 DK DK90401224.2T patent/DK0399866T3/da active
- 1990-05-09 EP EP90401224A patent/EP0399866B1/fr not_active Expired - Lifetime
- 1990-05-16 NO NO902187A patent/NO173091C/no not_active Application Discontinuation
- 1990-05-21 KR KR1019900007276A patent/KR940000059B1/ko not_active Expired - Fee Related
- 1990-05-23 FI FI902570A patent/FI104167B/fi not_active IP Right Cessation
- 1990-05-23 AU AU55766/90A patent/AU625504B2/en not_active Ceased
- 1990-05-23 PT PT94135A patent/PT94135B/pt not_active IP Right Cessation
- 1990-05-23 IE IE186590A patent/IE70760B1/en not_active IP Right Cessation
- 1990-05-23 CA CA002017358A patent/CA2017358C/fr not_active Expired - Fee Related
-
1994
- 1994-03-25 US US08/217,752 patent/US6605265B1/en not_active Expired - Fee Related
-
1995
- 1995-04-17 GR GR950400930T patent/GR3015800T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PT94135A (pt) | 1991-01-08 |
| CA2017358A1 (fr) | 1990-11-24 |
| DE69017081D1 (de) | 1995-03-30 |
| IE901865L (en) | 1990-11-24 |
| NO902187D0 (no) | 1990-05-16 |
| FI104167B1 (fi) | 1999-11-30 |
| FI902570A0 (fi) | 1990-05-23 |
| CA2017358C (fr) | 1996-09-03 |
| US6605265B1 (en) | 2003-08-12 |
| FI104167B (fi) | 1999-11-30 |
| EP0399866B1 (fr) | 1995-02-22 |
| ATE118760T1 (de) | 1995-03-15 |
| FR2647444B1 (enExample) | 1991-07-26 |
| ES2068352T3 (es) | 1995-04-16 |
| IE70760B1 (en) | 1996-12-30 |
| DK0399866T3 (da) | 1995-06-26 |
| NO173091C (no) | 1993-10-27 |
| PT94135B (pt) | 1997-01-31 |
| AU625504B2 (en) | 1992-07-16 |
| KR940000059B1 (ko) | 1994-01-05 |
| EP0399866A1 (fr) | 1990-11-28 |
| JPH02311448A (ja) | 1990-12-27 |
| KR900018007A (ko) | 1990-12-20 |
| GR3015800T3 (en) | 1995-07-31 |
| NO173091B (no) | 1993-07-19 |
| DE69017081T2 (de) | 1995-10-05 |
| NO902187L (no) | 1990-11-26 |
| FR2647444A1 (enExample) | 1990-11-30 |
| AU5576690A (en) | 1990-11-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH02311448A (ja) | アジンの合成方法と、ヒドラジン製造への応用 | |
| KR102704266B1 (ko) | 옥심 재순환을 갖는 하이드라진 수화물을 제조하는 개선된 방법 | |
| US5239119A (en) | Catalytic synthesis of azines from H2 O2 /NH3 /carbonyl compounds | |
| US4093656A (en) | Process for making azines | |
| US4256916A (en) | Oxidation of polyethylene glycols to dicarboxylic acids | |
| PL134893B1 (en) | Method of obtaining rhodium complexes of halogencarbonylobis/triorhanophosphoro/rhodium type | |
| JP4304446B2 (ja) | シュウ酸ジアルキルの製造法 | |
| JP2899883B2 (ja) | 蒸気状態におけるシュウ酸ジエステルの生成 | |
| US4827026A (en) | Method for producing 5-t-butylisophthalic acid | |
| JPS59205373A (ja) | 燐バナジウム触媒の再活性化、および、水存在下において正燐酸アルキルエステルで処理した無水マレイン酸触媒の製造方法 | |
| JP3535100B2 (ja) | アジンの加水分解によるヒドラジン製造方法 | |
| US3984451A (en) | Method for preparing hydrazo-bis-acetonitriles | |
| JP4131025B2 (ja) | ケタジン及び水加ヒドラジンの製造方法 | |
| JP4414091B2 (ja) | ヒドラジン水和物の調製方法 | |
| JP2002523478A (ja) | ヒドラジン水和物を製造するための方法 | |
| JP3528859B2 (ja) | ケタジンの合成法 | |
| JP3539433B2 (ja) | ケタジンの製造法 | |
| JP4131140B2 (ja) | ケタジン及び水加ヒドラジンの製造方法 | |
| FI117598B (fi) | Atsiinien synteesimenetelmä | |
| KR20250027267A (ko) | 캐스케이드 반응기를 이용한 아진의 제조 방법 | |
| CN113840800B (zh) | 采用吡唑啉再循环的制备肼水合物的经改善的方法 | |
| JP5614105B2 (ja) | ケタジン及び水加ヒドラジンの製造方法 | |
| JPS5822453B2 (ja) | ブチルアルデヒドの製造方法 | |
| KR830000207B1 (ko) | 케타진(ketazine)의 제조방법 | |
| JPH06183707A (ja) | アジ化ナトリウムの製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| LAPS | Cancellation because of no payment of annual fees |