JP2020090683A - 改善された硬化速度を有する安定した熱重合性ビニル、アミノ、またはオリゴマーフェノキシベンゾキシシクロブテンモノマーを製造する方法 - Google Patents
改善された硬化速度を有する安定した熱重合性ビニル、アミノ、またはオリゴマーフェノキシベンゾキシシクロブテンモノマーを製造する方法 Download PDFInfo
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- C08F32/00—Homopolymers and copolymers of cyclic compounds having no unsaturated aliphatic radicals in a side chain, and having one or more carbon-to-carbon double bonds in a carbocyclic ring system
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- C08G81/024—Block or graft polymers containing sequences of polymers of C08C or C08F and of polymers of C08G
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
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- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4846—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample
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Abstract
Description
Mは、C1〜C6アルキル置換または非置換芳香族ラジカル基、あるいはC1〜C6アルキル置換または非置換二価のヘテロ芳香族ラジカル基から選択される二価の芳香族基である。
L1は共有結合であり、そして、
R1〜R6は、それぞれに独立して水素、重水素、ハロゲン、ヒドロキシル、C1〜C6アルコキシ基、C1〜C6アルコキシ基、C1〜C6アルキル置換炭化水素基、ヘテロ原子含有炭素水素基、C1〜C6アルキル置換ヘテロ炭化水素基、シアノ基またはヒドロキシル基から選ばれた一価の基から選択され、あるいは好ましくは各R1、R2及びR3は水素、またはより好ましくは各R1〜R6は水素である。
BCB:ベンゾシクロブテン;
DMF:ジメチルホルムアミド;
THF:テトラヒドロフラン;及び、
V601:ジアゾラジカル開始剤、ジメチル2,2´−アゾビス(2−メチルプロピオネート(CAS番号2589−57−3、和光化学、日本)。
Claims (4)
- 以下の構造を有するモノマー:
Mは、C1〜C6アルキル置換または非置換芳香族ラジカル基、あるいはC1〜C6アルキル置換または非置換二価のヘテロ芳香族ラジカル基から選択される二価の芳香族基であり、
L1は共有結合であり、並びに、
R1〜R6は、それぞれに独立して水素、重水素、ハロゲン、ヒドロキシル、C1〜C6アルコキシ基、C1〜C6アルコキシ基、C1〜C6アルキル置換炭化水素基、ヘテロ原子含有炭素水素基、C1〜C6アルキル置換ヘテロ炭化水素基、シアノ基またはヒドロキシル基から選ばれる一価の基から選択される。 - R1、R2及びR3のそれぞれが水素である、請求項2に記載のモノマー。
- R1〜R6のそれぞれが水素である、請求項2に記載のモノマー。
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US15/828,972 | 2017-12-01 | ||
US15/828,972 US10513568B2 (en) | 2017-12-01 | 2017-12-01 | Methods of making stable and thermally polymerizable vinyl, amino or oligomeric phenoxy benzocyclobutene monomers with improved curing kinetics |
JP2018208511A JP6706658B2 (ja) | 2017-12-01 | 2018-11-06 | 改善された硬化速度を有する安定した熱重合性ビニル、アミノ、またはオリゴマーフェノキシベンゾキシシクロブテンモノマーを製造する方法 |
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JP2020021555A Active JP6920488B2 (ja) | 2017-12-01 | 2020-02-12 | 改善された硬化速度を有する安定した熱重合性ビニル、アミノ、またはオリゴマーフェノキシベンゾキシシクロブテンモノマーを製造する方法 |
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EP (2) | EP3492444B1 (ja) |
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KR (1) | KR102275979B1 (ja) |
CN (1) | CN109867590B (ja) |
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TWI803738B (zh) | 2019-03-11 | 2023-06-01 | 美商羅門哈斯電子材料有限公司 | 製造印刷線路板的方法 |
US10815179B1 (en) * | 2019-09-04 | 2020-10-27 | Eastman Chemical Company | Aromatic dicarbinols |
US11603422B2 (en) * | 2019-12-30 | 2023-03-14 | Rohm And Haas Electronic Materials Llc | Polymeric resin for dielectric applications |
US11920023B2 (en) | 2022-04-28 | 2024-03-05 | Rohm And Haas Electronic Materials Llc. | Composite materials for dielectric applications |
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US20200087429A1 (en) | 2020-03-19 |
EP3492444A1 (en) | 2019-06-05 |
TWI803733B (zh) | 2023-06-01 |
EP3492444B1 (en) | 2020-07-08 |
EP3708559A1 (en) | 2020-09-16 |
TWI690508B (zh) | 2020-04-11 |
TW202024007A (zh) | 2020-07-01 |
JP6920488B2 (ja) | 2021-08-18 |
US10513568B2 (en) | 2019-12-24 |
US20190169327A1 (en) | 2019-06-06 |
KR102275979B1 (ko) | 2021-07-12 |
CN109867590A (zh) | 2019-06-11 |
TW201925152A (zh) | 2019-07-01 |
JP2019099802A (ja) | 2019-06-24 |
JP6706658B2 (ja) | 2020-06-10 |
CN109867590B (zh) | 2022-06-21 |
KR20190065126A (ko) | 2019-06-11 |
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