JP2016540038A - アミドイミン配位子を含む金属複合体 - Google Patents
アミドイミン配位子を含む金属複合体 Download PDFInfo
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- JP2016540038A JP2016540038A JP2016552193A JP2016552193A JP2016540038A JP 2016540038 A JP2016540038 A JP 2016540038A JP 2016552193 A JP2016552193 A JP 2016552193A JP 2016552193 A JP2016552193 A JP 2016552193A JP 2016540038 A JP2016540038 A JP 2016540038A
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- C07C251/04—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups having carbon atoms of imino groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C251/06—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups having carbon atoms of imino groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of a saturated carbon skeleton
- C07C251/08—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups having carbon atoms of imino groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of a saturated carbon skeleton being acyclic
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- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
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- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
- C23C16/45523—Pulsed gas flow or change of composition over time
- C23C16/45525—Atomic layer deposition [ALD]
- C23C16/45527—Atomic layer deposition [ALD] characterized by the ALD cycle, e.g. different flows or temperatures during half-reactions, unusual pulsing sequence, use of precursor mixtures or auxiliary reactants or activations
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- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
- C23C16/45523—Pulsed gas flow or change of composition over time
- C23C16/45525—Atomic layer deposition [ALD]
- C23C16/45527—Atomic layer deposition [ALD] characterized by the ALD cycle, e.g. different flows or temperatures during half-reactions, unusual pulsing sequence, use of precursor mixtures or auxiliary reactants or activations
- C23C16/45536—Use of plasma, radiation or electromagnetic fields
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- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
- C23C16/45523—Pulsed gas flow or change of composition over time
- C23C16/45525—Atomic layer deposition [ALD]
- C23C16/45553—Atomic layer deposition [ALD] characterized by the use of precursors specially adapted for ALD
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- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having at least one potential-jump barrier or surface barrier, e.g. PN junction, depletion layer or carrier concentration layer
- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having at least one potential-jump barrier or surface barrier, e.g. PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic System or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/28—Manufacture of electrodes on semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/268
- H01L21/283—Deposition of conductive or insulating materials for electrodes conducting electric current
- H01L21/285—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation
- H01L21/28506—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers
- H01L21/28512—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers on semiconductor bodies comprising elements of Group IV of the Periodic System
- H01L21/28556—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers on semiconductor bodies comprising elements of Group IV of the Periodic System by chemical means, e.g. CVD, LPCVD, PECVD, laser CVD
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- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
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- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having at least one potential-jump barrier or surface barrier, e.g. PN junction, depletion layer or carrier concentration layer
- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having at least one potential-jump barrier or surface barrier, e.g. PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic System or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/28—Manufacture of electrodes on semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/268
- H01L21/283—Deposition of conductive or insulating materials for electrodes conducting electric current
- H01L21/285—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation
- H01L21/28506—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers
- H01L21/28512—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers on semiconductor bodies comprising elements of Group IV of the Periodic System
- H01L21/28568—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation of conductive layers on semiconductor bodies comprising elements of Group IV of the Periodic System the conductive layers comprising transition metals
Abstract
Description
a.基板温度:50〜600℃
b.蒸発器温度(金属前駆物質の温度):0〜200℃
c.反応炉圧力:0〜100Torr
d.アルゴンまたは窒素キャリアガスの流速:0〜500sccm
e.酸素流速:0〜500sccm
f.水素流速:0〜500sccm
g.反応時間:所望の膜厚に応じて変わる。
a.基板温度:0〜400℃
b.蒸発器温度(金属前駆物質の温度):0〜200℃
c.反応炉圧力:0〜100Torr
d.アルゴンまたは窒素キャリアガスの流速:0〜500sccm
e.反応気体流速:0〜500sccm
f.パルスシークエンス(金属複合体/パージ/反応気体/パージ):チャンバーサイズに応じて変わる
g.反応回数:所望の膜厚に応じて変わる。
初めに、原子層蒸着チャンバーに基板を置いた。基板表面に、マンガン前駆物質、例えば、マンガン複合体1〜5のうちの一つ、を接触させた。その後、過剰の未反応マンガン前駆物質を、反応チャンバーからパージした。その後、水素ガスをチャンバー中の基板表面に流した。基板表面に結合しているマンガン前駆物質は、還元され、主にマンガン金属からなるマンガン被膜が生成された。その後、過剰のマンガン前駆物質を、チャンバーからパージした。所望の膜厚に到達するまで、本プロセスを繰り返した。
初めに、原子層蒸着チャンバーに基板を置いた。基板表面に、マンガン前駆物質、例えば、マンガン複合体1〜5のうちの一つ、を接触させた。その後、過剰の未反応マンガン前駆物質を、反応チャンバーからパージした。その後、アンモニアガスをチャンバー中の基板表面に流した。基板表面に結合しているマンガン前駆物質は、アンモニアガスと反応し、窒化マンガンからなる被膜が生成された。その後、過剰のマンガン前駆物質を、チャンバーからパージした。所望の膜厚に到達するまで、本プロセスを繰り返した。
Claims (69)
- 式中、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される、請求項1に記載の金属複合体。
- 式中、R1、R2、R2’およびR3は、C1〜C4のアルキル、またはC6〜C10のアリールを含む群から独立に選択される、請求項1または2に記載の金属複合体。
- 式中、R1、R2、R2’およびR3は、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択される、上記請求項の何れか1項に記載の金属複合体。
- 式中、R2およびR2’は、各々、メチルである、上記請求項の何れか1項に記載の金属複合体。
- 式中、Lは、単座、または二座の配位子を少なくとも一つ含む、上記請求項の何れか1項に記載の金属複合体。
- 式中、Lは、アミドイミン配位子、ジアザブタジエン配位子、アミジネート配位子、またはアリール配位子を含む、上記請求項の何れか1項に記載の金属複合体。
- 式中、Lは、η3−アリール配位子を含む、上記請求項の何れか1項に記載の金属複合体。
- 式中、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される、請求項9に記載の金属複合体。
- 式中、R1、R2、R2’、R3、R4、R5、R6およびR6’は、C1〜C4のアルキル、またはC6〜C10のアリールを含む群から独立に選択される、請求項9または10に記載の金属複合体。
- 式中、R1、R2、R2’、R3、R4、R5、R6およびR6’は、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択される、請求項9〜11の何れか1項に記載の金属複合体。
- 式中、R2、R2’、R6およびR6’は、各々、メチルである、請求項9〜12の何れか1項に記載の金属複合体。
- 式中、金属複合体は、ホモレプティック金属複合体である、請求項9〜13の何れか1項に記載の金属複合体。
- 式中、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される、請求項15に記載の金属複合体。
- 式中、R1、R2、R2’およびR3は、C1〜C4のアルキル、またはC6〜C10のアリールを含む群から独立に選択され;また、R7、R8、R9およびR10は、水素、C1〜C4アルキル、またはC6〜C10アリールを含む群から独立に選択される、請求項15または16に記載の金属複合体。
- 式中、R1、R2、R2’およびR3は、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択され;また、R7、R8、R9およびR10は、水素、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択される、請求項15〜17の何れか1項に記載の金属複合体。
- 式中、R2およびR2’は、各々、メチルである、請求項15〜18の何れか1項に記載の金属複合体。
- 式中、R8およびR9は、各々、水素である、請求項15〜19の何れか1項に記載の金属複合体。
- 式中、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される、請求項21に記載の金属複合体。
- 式中、R1、R2、R2’、R3、R11、R12およびR13は、水素、C1〜C4アルキル、またはC6〜C10アリールを含む群から独立に選択される、請求項21または22に記載の金属複合体。
- 式中、R1、R2、R2’、R3、R11、R12およびR13は、水素、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択される、請求項21〜23の何れか1項に記載の金属複合体。
- 式中、R2およびR2’は、各々、メチルである、請求項21〜24の何れか1項に記載の金属複合体。
- 式中、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される、請求項26に記載の金属複合体。
- 式中、R1、R2、R2’およびR3は、C1〜C4アルキル、またはC6〜C10アリールを含む群から独立に選択され;また、
R14、R14’、R15、R16およびR16’は、水素、C1〜C4アルキル、C6〜C10アリール、またはトリ(C1〜C4アルキル)シリルを含む群から独立に選択される、請求項26または27の何れか1項に記載の金属複合体。 - 式中、R1、R2、R2’およびR3は、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択され;また、
R14、R14’、R15、R16およびR16’は、水素、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、フェニル、またはトリメチルシリルから独立に選択される、請求項26〜28の何れか1項に記載の金属複合体。 - 式中、R2およびR2’は、各々、メチルである、請求項26〜29の何れか1項に記載の金属複合体。
- 上記請求項の何れか1項に記載の溶媒和物。
- 溶媒和物は、エーテル溶媒和物、アミン溶媒和物、または芳香族炭化水素溶媒和物である、請求項30に記載の溶媒和物。
- 請求項33に記載の方法であり、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される方法。
- 請求項33または34に記載の方法であり、R1、R2、R2’およびR3は、水素、C1〜C4アルキル、またはC6〜C10アリールを含む群から独立に選択される方法。
- 請求項33〜35の何れか1項に記載の方法であり、R1、R2、R2’およびR3は、水素、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択される方法。
- 請求項33〜36の何れか1項に記載の方法であり、R2およびR2’は、各々、メチルである方法。
- 請求項33〜37の何れか1項に記載の方法であり、Lは、単座、または二座の配位子を少なくとも一つ含む方法。
- 請求項33〜38の何れか1項に記載の方法であり、Lは、アミドイミン配位子、ジアザブタジエン配位子、アミジネート配位子、またはアリール配位子を含む方法。
- 請求項33〜39の何れか1項に記載の方法であり、Lは、η3−アリール配位子を含む方法。
- 請求項41に記載の方法であり、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される方法。
- 請求項41または42に記載の方法であり、R1、R2、R2’、R3、R4、R5、R6およびR6’は、水素、C1〜C4アルキル、またはC6〜C10アリールを含む群から独立に選択される方法。
- 請求項41〜43の何れか1項に記載の方法であり、R1、R2、R2’、R3、R4、R5、R6およびR6’は、水素、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択される方法。
- 請求項41〜44の何れか1項に記載の方法であり、R2、R2’、R6およびR6’は、各々、メチルである方法。
- 請求項41〜45の何れか1項に記載の方法であり、金属複合体は、ホモレプティック金属複合体である方法。
- 請求項47に記載の方法であり、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される方法。
- 請求項47または48に記載の方法であり、R1、R2、R2’、R3、R7、R8、R9およびR10は、水素、C1〜C4アルキル、またはC6〜C10アリールを含む群から独立に選択される方法。
- 請求項47〜49の何れか1項に記載の方法であり、R1、R2、R2’、R3、R7、R8、R9およびR10は、水素、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択される方法。
- 請求項47〜50の何れか1項に記載の方法であり、R2およびR2’は、各々、メチルである方法。
- 請求項47〜51の何れか1項に記載の方法であり、R8およびR9は、各々、水素である方法。
- 気相蒸着プロセスによって金属含有被膜を形成する方法であり、請求項21〜25の何れか1項に記載の構造を示す少なくとも一つの金属複合体を気化することを含む方法。
- 請求項54に記載の方法であり、Mは、マンガン、コバルト、ニッケル、または銅を含む群から選択される方法。
- 請求項54または55に記載の方法であり、R1、R2、R2’およびR3は、水素、C1〜C4アルキル、またはC6〜C10アリールを含む群から独立に選択され;また、
R14、R14’、R15、R16およびR16’は、水素、C1〜C4アルキル、C6〜C10アリール、またはトリ(C1〜C4アルキル)シリルを含む群から独立に選択される方法。 - 請求項54〜56の何れか1項に記載の方法であり、R1、R2、R2’およびR3は、水素、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、またはフェニルを含む群から独立に選択され;また、
R14、R14’、R15、R16およびR16’は、水素、メチル、エチル、プロピル、イソプロピル、ブチル、sec−ブチル、tert−ブチル、フェニル、またはトリメチルシリルを含む群から独立に選択される方法。 - 請求項54〜57の何れか1項に記載の方法であり、R2およびR2’は、各々、メチルである方法。
- 請求項33〜58の何れか1項に記載の方法であり、気相蒸着プロセスは化学気相蒸着である方法。
- 請求項59に記載の方法であり、化学気相蒸着はパルス化学気相蒸着、または連続フロー化学気相蒸着である方法。
- 請求項59に記載の方法であり、化学気相蒸着は液体注入化学気相蒸着である方法。
- 請求項33〜58の何れか1項に記載の方法であり、気相蒸着プロセスは原子層蒸着である方法。
- 請求項62に記載の方法であり、原子層蒸着は液体注入原子層蒸着、またはプラズマ強化原子層蒸着である方法。
- 請求項33〜63の何れか1項に記載の方法であり、少なくとも一つの金属複合体は、酸化金属被膜の形成のため、酸素供給源のパルスに代わるパルスにおける基板へと供給される方法。
- 請求項64に記載の方法であり、酸素供給源がH2O、空気、O2、またはオゾンを含む群から選択される方法。
- 請求項33〜65の何れか1項に記載の方法であり、水素、水素プラズマ、酸素、空気、水、アンモニア、ヒドラジン、ボラン、シラン、オゾン、またはこれらの組み合わせを含む群から選択される少なくとも一つの共反応剤の気化をさらに含む方法。
- 請求項33〜65の何れか1項に記載の方法であり、共反応剤であるヒドラジンの気化をさらに含む方法。
- 請求項67の方法であり、ヒドラジンが、ヒドラジン(N2H4)、またはN,N−ジメチルヒドラジンである方法。
- 請求項33〜68の何れか1項に記載の方法であり、DRAM応用、またはCMOS応用に用いられる方法。
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US20160273106A1 (en) | 2016-09-22 |
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