JP2016539893A5 - - Google Patents
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- Publication number
- JP2016539893A5 JP2016539893A5 JP2016525917A JP2016525917A JP2016539893A5 JP 2016539893 A5 JP2016539893 A5 JP 2016539893A5 JP 2016525917 A JP2016525917 A JP 2016525917A JP 2016525917 A JP2016525917 A JP 2016525917A JP 2016539893 A5 JP2016539893 A5 JP 2016539893A5
- Authority
- JP
- Japan
- Prior art keywords
- slurry
- aging
- range
- sapo
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002808 molecular sieve Substances 0.000 claims description 17
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 17
- 239000002245 particle Substances 0.000 claims description 16
- 239000003054 catalyst Substances 0.000 claims description 9
- 239000013078 crystal Substances 0.000 claims description 5
- 241000269350 Anura Species 0.000 claims description 4
- 239000002002 slurry Substances 0.000 claims 39
- 238000000034 method Methods 0.000 claims 28
- 230000032683 aging Effects 0.000 claims 23
- 239000000203 mixture Substances 0.000 claims 17
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 16
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 12
- 239000003795 chemical substances by application Substances 0.000 claims 11
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 8
- 229910052782 aluminium Inorganic materials 0.000 claims 8
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 7
- 229910052710 silicon Inorganic materials 0.000 claims 7
- 239000010703 silicon Substances 0.000 claims 7
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 6
- 229910052698 phosphorus Inorganic materials 0.000 claims 6
- 239000011574 phosphorus Substances 0.000 claims 6
- 150000001336 alkenes Chemical class 0.000 claims 5
- 238000002425 crystallisation Methods 0.000 claims 5
- 230000008025 crystallization Effects 0.000 claims 5
- 230000001939 inductive effect Effects 0.000 claims 5
- 150000003973 alkyl amines Chemical class 0.000 claims 3
- 238000010438 heat treatment Methods 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 claims 2
- 239000002243 precursor Substances 0.000 claims 2
- 150000003856 quaternary ammonium compounds Chemical class 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- 230000002194 synthesizing effect Effects 0.000 claims 1
- 229940073455 tetraethylammonium hydroxide Drugs 0.000 claims 1
- LRGJRHZIDJQFCL-UHFFFAOYSA-M tetraethylazanium;hydroxide Chemical group [OH-].CC[N+](CC)(CC)CC LRGJRHZIDJQFCL-UHFFFAOYSA-M 0.000 claims 1
- 239000011159 matrix material Substances 0.000 description 3
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361895087P | 2013-10-24 | 2013-10-24 | |
| US61/895,087 | 2013-10-24 | ||
| PCT/US2014/061925 WO2015061544A1 (en) | 2013-10-24 | 2014-10-23 | Method for synthesizing silicoaluminophosphate-34 molecular sieves |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2016539893A JP2016539893A (ja) | 2016-12-22 |
| JP2016539893A5 true JP2016539893A5 (OSRAM) | 2019-03-14 |
| JP6649882B2 JP6649882B2 (ja) | 2020-02-19 |
Family
ID=52993546
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016525917A Expired - Fee Related JP6649882B2 (ja) | 2013-10-24 | 2014-10-23 | シリコアルミノリン酸塩−３４モレキュラーシーブの合成方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US9889440B2 (OSRAM) |
| EP (1) | EP3060339A4 (OSRAM) |
| JP (1) | JP6649882B2 (OSRAM) |
| KR (1) | KR20160077109A (OSRAM) |
| CN (1) | CN105682795B (OSRAM) |
| CA (1) | CA2928547C (OSRAM) |
| MX (1) | MX2016004737A (OSRAM) |
| RU (1) | RU2700590C2 (OSRAM) |
| WO (1) | WO2015061544A1 (OSRAM) |
| ZA (1) | ZA201602075B (OSRAM) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6723223B2 (ja) * | 2014-08-22 | 2020-07-15 | ダブリュー・アール・グレース・アンド・カンパニー−コーンＷ Ｒ Ｇｒａｃｅ ＆ Ｃｏ−Ｃｏｎｎ | モノイソプロパノールアミンを用いたシリコアルミノホスフェート−３４モレキュラーシーブの合成方法 |
| GB2537206A (en) * | 2015-01-29 | 2016-10-12 | Johnson Matthey Plc | Direct incorporation of iron complexes into SAPO-34 (CHA) type materials |
| CN106241831B (zh) * | 2016-07-26 | 2018-08-07 | 南开大学 | Cha结构与afi结构交叉生长的硅磷酸铝分子筛及其合成 |
| FR3063995A1 (fr) * | 2017-03-17 | 2018-09-21 | Arkema France | Procede de synthese multi-reacteur de cristaux de zeolithe a granulometrie controlee |
| CN111099625B (zh) * | 2018-10-25 | 2021-10-01 | 中国石油化工股份有限公司 | 分子筛scm-24、其合成方法及其用途 |
| KR102224614B1 (ko) * | 2018-12-31 | 2021-03-05 | 포항공과대학교 산학협력단 | 무기 금속 성분을 포함하는 cha형 sapo 및 그 제조 방법 |
| CN112624150B (zh) * | 2019-09-24 | 2022-09-06 | 中国石油化工股份有限公司 | Sapo-34分子筛的合成方法、合成的分子筛及其用途 |
| CN112824322B (zh) * | 2019-11-21 | 2022-11-08 | 国家能源投资集团有限责任公司 | 小粒径sapo-34分子筛以及制备方法与应用 |
| CN113753915B (zh) * | 2020-06-01 | 2023-04-07 | 中国石油化工股份有限公司 | 小晶粒sapo-34分子筛的制法、制备的分子筛和用途 |
| CN115849399B (zh) * | 2021-09-26 | 2024-08-30 | 中国石油化工股份有限公司 | 一种sapo-5分子筛及其制备方法和应用 |
| US20240207831A1 (en) * | 2022-12-08 | 2024-06-27 | California Institute Of Technology | Molecular Sieve CIT-16P, Its Synthesis, Transformation and Use |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4310440A (en) | 1980-07-07 | 1982-01-12 | Union Carbide Corporation | Crystalline metallophosphate compositions |
| US4440871A (en) * | 1982-07-26 | 1984-04-03 | Union Carbide Corporation | Crystalline silicoaluminophosphates |
| US4677243A (en) | 1982-10-04 | 1987-06-30 | Union Carbide Corporation | Production of light olefins from aliphatic hetero compounds |
| US4499327A (en) | 1982-10-04 | 1985-02-12 | Union Carbide Corporation | Production of light olefins |
| NO304108B1 (no) * | 1996-10-09 | 1998-10-26 | Polymers Holding As | En mikroporos silikoaluminofosfat-sammensetning, katalytisk materiale som omfatter denne sammensetningen og fremgangsmate for fremstilling derav, og bruken av disse for a fremstille olefiner fra metanol |
| ID28170A (id) * | 1998-07-29 | 2001-05-10 | Exxon Chemical Patents Inc | Proses untuk pembuatan ayakan molekul |
| JP4168214B2 (ja) | 1998-10-15 | 2008-10-22 | 三菱瓦斯化学株式会社 | メチルアミン製造触媒及び該触媒の製造方法 |
| US6521562B1 (en) | 2000-09-28 | 2003-02-18 | Exxonmobil Chemical Patents, Inc. | Preparation of molecular sieve catalysts micro-filtration |
| US6696032B2 (en) * | 2001-11-29 | 2004-02-24 | Exxonmobil Chemical Patents Inc. | Process for manufacturing a silicoaluminophosphate molecular sieve |
| US6660682B2 (en) | 2001-11-30 | 2003-12-09 | Exxon Mobil Chemical Patents Inc. | Method of synthesizing molecular sieves |
| US6685905B2 (en) | 2001-12-21 | 2004-02-03 | Exxonmobil Chemical Patents Inc. | Silicoaluminophosphate molecular sieves |
| US6680278B2 (en) * | 2002-06-12 | 2004-01-20 | Exxonmobil Chemical Patents, Inc. | Synthesis of silicoaluminophosphates |
| US6767858B1 (en) * | 2003-02-20 | 2004-07-27 | Exxonmobil Chemical Patents Inc. | Synthesis of alumino- and silicoalumino-phosphates of CHA framework type |
| US7241713B2 (en) * | 2003-10-02 | 2007-07-10 | Exxonmobil Chemical Patents Inc. | Molecular sieve catalyst composition, its making and use in conversion processes |
| US7622624B2 (en) * | 2004-04-05 | 2009-11-24 | Exxonmobil Chemical Patents Inc. | Crystalline intergrowth material, its synthesis and its use in the conversion of oxygenates to olefins |
| US7708976B2 (en) * | 2004-10-01 | 2010-05-04 | Exxonmobil Chemical Patents Inc. | Aluminophosphate molecular sieve, its synthesis and use |
| US7090814B2 (en) * | 2004-11-10 | 2006-08-15 | Exxonmobil Chemical Patents Inc. | Method of synthesizing silicoaluminophosphate molecular sieves |
| US7528201B2 (en) * | 2004-12-22 | 2009-05-05 | Exxonmobil Chemical Patents Inc. | Synthesis of silicoaluminophosphate molecular sieves |
| CN101208149B (zh) * | 2005-06-27 | 2010-11-03 | 埃克森美孚化学专利公司 | 制备硅铝磷酸盐分子筛的方法 |
| US7112316B1 (en) * | 2005-08-08 | 2006-09-26 | Uop Llc | Process for preparing molecular sieves via continuous addition of nutrients |
| EP2021126B1 (en) * | 2006-04-25 | 2019-09-11 | ExxonMobil Chemical Patents Inc. | Method of synthesizing aluminophosphate and silicoaluminophosphate molecular sieves |
| US20070276174A1 (en) * | 2006-05-26 | 2007-11-29 | Martens Luc R M | Synthesis of molecular sieves and their use in the conversion of oxygenates to olefins |
| US20090196812A1 (en) * | 2008-01-31 | 2009-08-06 | Basf Catalysts Llc | Catalysts, Systems and Methods Utilizing Non-Zeolitic Metal-Containing Molecular Sieves Having the CHA Crystal Structure |
| US8313727B2 (en) * | 2008-07-25 | 2012-11-20 | Exxonmobil Chemical Patents Inc. | Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins |
| US20100029998A1 (en) * | 2008-07-29 | 2010-02-04 | Chevron U.S.A. Inc. | Synthesis of a Crystalline Silicoaluminophosphate |
| US20100087610A1 (en) * | 2008-10-06 | 2010-04-08 | Vaughn Stephen N | Method Of Preparing And Using A Molecular Sieve |
| KR101193973B1 (ko) | 2009-10-22 | 2012-10-24 | 현대엔지니어링 주식회사 | 고강도를 갖는 ｓａｐｏ-34 미소구형체 촉매, 이의 제조방법 및 이를 이용한 경질올레핀의 제조방법 |
| CN102336412B (zh) * | 2011-06-24 | 2013-03-27 | 神华集团有限责任公司 | 一种sapo-34分子筛的制备方法 |
| CN102838131B (zh) * | 2012-09-17 | 2015-02-18 | 神华集团有限责任公司 | Sapo-34分子筛及其制备方法 |
-
2014
- 2014-10-23 RU RU2016119886A patent/RU2700590C2/ru active
- 2014-10-23 CA CA2928547A patent/CA2928547C/en active Active
- 2014-10-23 KR KR1020167013319A patent/KR20160077109A/ko not_active Ceased
- 2014-10-23 WO PCT/US2014/061925 patent/WO2015061544A1/en not_active Ceased
- 2014-10-23 MX MX2016004737A patent/MX2016004737A/es unknown
- 2014-10-23 EP EP14855571.7A patent/EP3060339A4/en not_active Withdrawn
- 2014-10-23 CN CN201480058171.8A patent/CN105682795B/zh active Active
- 2014-10-23 US US15/031,609 patent/US9889440B2/en active Active
- 2014-10-23 JP JP2016525917A patent/JP6649882B2/ja not_active Expired - Fee Related
-
2016
- 2016-03-29 ZA ZA2016/02075A patent/ZA201602075B/en unknown
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