JP2016128909A - 感光性樹脂組成物、これを用いた色変換パネル及び表示装置 - Google Patents
感光性樹脂組成物、これを用いた色変換パネル及び表示装置 Download PDFInfo
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- JP2016128909A JP2016128909A JP2016002337A JP2016002337A JP2016128909A JP 2016128909 A JP2016128909 A JP 2016128909A JP 2016002337 A JP2016002337 A JP 2016002337A JP 2016002337 A JP2016002337 A JP 2016002337A JP 2016128909 A JP2016128909 A JP 2016128909A
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- Prior art keywords
- resin composition
- photosensitive resin
- color conversion
- phosphate
- disposed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 109
- 239000011342 resin composition Substances 0.000 title claims abstract description 85
- 150000001875 compounds Chemical class 0.000 claims abstract description 77
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 44
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 41
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000003999 initiator Substances 0.000 claims abstract description 15
- 229910052698 phosphorus Inorganic materials 0.000 claims abstract description 14
- 239000011574 phosphorus Substances 0.000 claims abstract description 14
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002904 solvent Substances 0.000 claims abstract description 7
- 239000004973 liquid crystal related substance Substances 0.000 claims description 70
- -1 stearyl (3,5-ditertiarybutyl-4-hydroxyphenyl) propionate Chemical compound 0.000 claims description 66
- 239000000758 substrate Substances 0.000 claims description 61
- 239000002096 quantum dot Substances 0.000 claims description 35
- 239000007983 Tris buffer Substances 0.000 claims description 29
- 239000010409 thin film Substances 0.000 claims description 23
- 229910052712 strontium Inorganic materials 0.000 claims description 19
- 230000005540 biological transmission Effects 0.000 claims description 17
- 229910052791 calcium Inorganic materials 0.000 claims description 15
- 229910019142 PO4 Inorganic materials 0.000 claims description 12
- 229910052788 barium Inorganic materials 0.000 claims description 12
- 239000002270 dispersing agent Substances 0.000 claims description 12
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 12
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 12
- 239000010452 phosphate Substances 0.000 claims description 12
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims description 10
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 claims description 10
- 229910003564 SiAlON Inorganic materials 0.000 claims description 9
- 229910004613 CdTe Inorganic materials 0.000 claims description 7
- 229910007709 ZnTe Inorganic materials 0.000 claims description 7
- UHYPYGJEEGLRJD-UHFFFAOYSA-N cadmium(2+);selenium(2-) Chemical compound [Se-2].[Cd+2] UHYPYGJEEGLRJD-UHFFFAOYSA-N 0.000 claims description 7
- SBIBMFFZSBJNJF-UHFFFAOYSA-N selenium;zinc Chemical compound [Se]=[Zn] SBIBMFFZSBJNJF-UHFFFAOYSA-N 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 7
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims description 6
- 150000001412 amines Chemical class 0.000 claims description 6
- FQUNFJULCYSSOP-UHFFFAOYSA-N bisoctrizole Chemical compound N1=C2C=CC=CC2=NN1C1=CC(C(C)(C)CC(C)(C)C)=CC(CC=2C(=C(C=C(C=2)C(C)(C)CC(C)(C)C)N2N=C3C=CC=CC3=N2)O)=C1O FQUNFJULCYSSOP-UHFFFAOYSA-N 0.000 claims description 6
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 6
- 229910021480 group 4 element Inorganic materials 0.000 claims description 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 6
- 229910052749 magnesium Inorganic materials 0.000 claims description 6
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 6
- 150000002989 phenols Chemical class 0.000 claims description 6
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 6
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 5
- 229910004283 SiO 4 Inorganic materials 0.000 claims description 5
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 5
- 150000004645 aluminates Chemical class 0.000 claims description 5
- 239000002223 garnet Substances 0.000 claims description 5
- 150000003463 sulfur Chemical class 0.000 claims description 5
- 229910052717 sulfur Inorganic materials 0.000 claims description 5
- YBNMDCCMCLUHBL-UHFFFAOYSA-N (2,5-dioxopyrrolidin-1-yl) 4-pyren-1-ylbutanoate Chemical compound C=1C=C(C2=C34)C=CC3=CC=CC4=CC=C2C=1CCCC(=O)ON1C(=O)CCC1=O YBNMDCCMCLUHBL-UHFFFAOYSA-N 0.000 claims description 4
- 229910002601 GaN Inorganic materials 0.000 claims description 4
- 229910005540 GaP Inorganic materials 0.000 claims description 4
- 229910001218 Gallium arsenide Inorganic materials 0.000 claims description 4
- 229910004262 HgTe Inorganic materials 0.000 claims description 4
- 229910002665 PbTe Inorganic materials 0.000 claims description 4
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 4
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 4
- 229940117969 neopentyl glycol Drugs 0.000 claims description 4
- 229920005862 polyol Polymers 0.000 claims description 4
- 150000003077 polyols Chemical class 0.000 claims description 4
- OCGWQDWYSQAFTO-UHFFFAOYSA-N tellanylidenelead Chemical compound [Pb]=[Te] OCGWQDWYSQAFTO-UHFFFAOYSA-N 0.000 claims description 4
- UWIPPHXVRZCFHT-UHFFFAOYSA-N (2-butylphenyl) dihydrogen phosphate Chemical compound CCCCC1=CC=CC=C1OP(O)(O)=O UWIPPHXVRZCFHT-UHFFFAOYSA-N 0.000 claims description 3
- URBFWIOUKUBOAS-UHFFFAOYSA-N 1,1-bis(2,4-ditert-butylphenyl)-2,2-bis(hydroxymethyl)propane-1,3-diol phosphono dihydrogen phosphate Chemical compound OP(O)(=O)OP(=O)(O)O.C(C)(C)(C)C1=C(C=CC(=C1)C(C)(C)C)C(O)(C(CO)(CO)CO)C1=C(C=C(C=C1)C(C)(C)C)C(C)(C)C URBFWIOUKUBOAS-UHFFFAOYSA-N 0.000 claims description 3
- TYCLKLCKLGCVEZ-UHFFFAOYSA-N 1,1-bis(2,6-ditert-butyl-4-methylphenyl)-2,2-bis(hydroxymethyl)propane-1,3-diol phosphono dihydrogen phosphate Chemical compound OP(O)(=O)OP(=O)(O)O.C(C)(C)(C)C1=C(C(=CC(=C1)C)C(C)(C)C)C(O)(C(CO)(CO)CO)C1=C(C=C(C=C1C(C)(C)C)C)C(C)(C)C TYCLKLCKLGCVEZ-UHFFFAOYSA-N 0.000 claims description 3
- YTDOAJNXRUZBRM-UHFFFAOYSA-N 1,3,7,9-tetratert-butyl-11-octoxy-5h-benzo[d][1,3,2]benzodioxaphosphocine 11-oxide Chemical compound C1C2=CC(C(C)(C)C)=CC(C(C)(C)C)=C2OP(OCCCCCCCC)(=O)OC2=C1C=C(C(C)(C)C)C=C2C(C)(C)C YTDOAJNXRUZBRM-UHFFFAOYSA-N 0.000 claims description 3
- RMSGQZDGSZOJMU-UHFFFAOYSA-N 1-butyl-2-phenylbenzene Chemical group CCCCC1=CC=CC=C1C1=CC=CC=C1 RMSGQZDGSZOJMU-UHFFFAOYSA-N 0.000 claims description 3
- QBEVRWIMOMSOBC-UHFFFAOYSA-N 10,10-diphenyldecyl dihydrogen phosphate Chemical compound C=1C=CC=CC=1C(CCCCCCCCCOP(O)(=O)O)C1=CC=CC=C1 QBEVRWIMOMSOBC-UHFFFAOYSA-N 0.000 claims description 3
- BSYJHYLAMMJNRC-UHFFFAOYSA-N 2,4,4-trimethylpentan-2-ol Chemical compound CC(C)(C)CC(C)(C)O BSYJHYLAMMJNRC-UHFFFAOYSA-N 0.000 claims description 3
- DXCHWXWXYPEZKM-UHFFFAOYSA-N 2,4-ditert-butyl-6-[1-(3,5-ditert-butyl-2-hydroxyphenyl)ethyl]phenol Chemical compound C=1C(C(C)(C)C)=CC(C(C)(C)C)=C(O)C=1C(C)C1=CC(C(C)(C)C)=CC(C(C)(C)C)=C1O DXCHWXWXYPEZKM-UHFFFAOYSA-N 0.000 claims description 3
- FLSKKFALEYBSJE-UHFFFAOYSA-N 2,6-ditert-butyl-4-[1-(3,5-ditert-butyl-4-hydroxyphenyl)butyl]phenol Chemical compound C=1C(C(C)(C)C)=C(O)C(C(C)(C)C)=CC=1C(CCC)C1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 FLSKKFALEYBSJE-UHFFFAOYSA-N 0.000 claims description 3
- JMCKNCBUBGMWAY-UHFFFAOYSA-N 2,6-ditert-butyl-4-[[4-(3,5-ditert-butyl-4-hydroxyphenoxy)-6-octylsulfanyl-1,3,5-triazin-2-yl]oxy]phenol Chemical compound N=1C(OC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=NC(SCCCCCCCC)=NC=1OC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 JMCKNCBUBGMWAY-UHFFFAOYSA-N 0.000 claims description 3
- HXIQYSLFEXIOAV-UHFFFAOYSA-N 2-tert-butyl-4-(5-tert-butyl-4-hydroxy-2-methylphenyl)sulfanyl-5-methylphenol Chemical compound CC1=CC(O)=C(C(C)(C)C)C=C1SC1=CC(C(C)(C)C)=C(O)C=C1C HXIQYSLFEXIOAV-UHFFFAOYSA-N 0.000 claims description 3
- PFANXOISJYKQRP-UHFFFAOYSA-N 2-tert-butyl-4-[1-(5-tert-butyl-4-hydroxy-2-methylphenyl)butyl]-5-methylphenol Chemical compound C=1C(C(C)(C)C)=C(O)C=C(C)C=1C(CCC)C1=CC(C(C)(C)C)=C(O)C=C1C PFANXOISJYKQRP-UHFFFAOYSA-N 0.000 claims description 3
- JJHKARPEMHIIQC-UHFFFAOYSA-N 4-octadecoxy-2,6-diphenylphenol Chemical compound C=1C(OCCCCCCCCCCCCCCCCCC)=CC(C=2C=CC=CC=2)=C(O)C=1C1=CC=CC=C1 JJHKARPEMHIIQC-UHFFFAOYSA-N 0.000 claims description 3
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 3
- 102100032047 Alsin Human genes 0.000 claims description 3
- 101710187109 Alsin Proteins 0.000 claims description 3
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 claims description 3
- NKXTXHZPUXGCBK-UHFFFAOYSA-N C(CCC)C(C(O)O)(C)CC.C1(=CC=CC=C1)O Chemical compound C(CCC)C(C(O)O)(C)CC.C1(=CC=CC=C1)O NKXTXHZPUXGCBK-UHFFFAOYSA-N 0.000 claims description 3
- ZAVSTKBSHFACFV-UHFFFAOYSA-N CCCC(C1=CC(=C(C=C1C)O)C(C)(C)C)C2=CC(=C(C=C2C)OP(=O)(O)OP(=O)(O)O)C(C)(C)C Chemical compound CCCC(C1=CC(=C(C=C1C)O)C(C)(C)C)C2=CC(=C(C=C2C)OP(=O)(O)OP(=O)(O)O)C(C)(C)C ZAVSTKBSHFACFV-UHFFFAOYSA-N 0.000 claims description 3
- JYFHYPJRHGVZDY-UHFFFAOYSA-N Dibutyl phosphate Chemical compound CCCCOP(O)(=O)OCCCC JYFHYPJRHGVZDY-UHFFFAOYSA-N 0.000 claims description 3
- 229910000673 Indium arsenide Inorganic materials 0.000 claims description 3
- 229910017639 MgSi Inorganic materials 0.000 claims description 3
- QOCCCTYZUWSWDU-UHFFFAOYSA-N OP(O)(=O)OP(=O)(O)O.C(CCCCCCCC)C1=C(C=CC=C1)C(O)(C(CO)(CO)CO)C1=C(C=CC=C1)CCCCCCCCC Chemical compound OP(O)(=O)OP(=O)(O)O.C(CCCCCCCC)C1=C(C=CC=C1)C(O)(C(CO)(CO)CO)C1=C(C=CC=C1)CCCCCCCCC QOCCCTYZUWSWDU-UHFFFAOYSA-N 0.000 claims description 3
- RZUHBLGLDSYPOM-UHFFFAOYSA-N OP(O)(=O)OP(=O)(O)O.C(CCCCCCCCCCCCCCCCC)C(O)(C(CO)(CO)CO)CCCCCCCCCCCCCCCCCC Chemical compound OP(O)(=O)OP(=O)(O)O.C(CCCCCCCCCCCCCCCCC)C(O)(C(CO)(CO)CO)CCCCCCCCCCCCCCCCCC RZUHBLGLDSYPOM-UHFFFAOYSA-N 0.000 claims description 3
- 229910004122 SrSi Inorganic materials 0.000 claims description 3
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 3
- GTVWRXDRKAHEAD-UHFFFAOYSA-N Tris(2-ethylhexyl) phosphate Chemical compound CCCCC(CC)COP(=O)(OCC(CC)CCCC)OCC(CC)CCCC GTVWRXDRKAHEAD-UHFFFAOYSA-N 0.000 claims description 3
- VYGRRCKMMADGBB-UHFFFAOYSA-N [3-hydroxy-2,2-bis(hydroxymethyl)propyl] phosphono hydrogen phosphate Chemical compound OCC(CO)(CO)COP(O)(=O)OP(O)(O)=O VYGRRCKMMADGBB-UHFFFAOYSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- 235000010290 biphenyl Nutrition 0.000 claims description 3
- 239000004305 biphenyl Substances 0.000 claims description 3
- 125000006267 biphenyl group Chemical group 0.000 claims description 3
- JTNKWPDPEXRFOV-UHFFFAOYSA-N bis(8-methylnonyl) phenyl phosphate Chemical compound CC(C)CCCCCCCOP(=O)(OCCCCCCCC(C)C)OC1=CC=CC=C1 JTNKWPDPEXRFOV-UHFFFAOYSA-N 0.000 claims description 3
- JWXSMZJIYUUXSV-UHFFFAOYSA-N bis[2-tert-butyl-6-[(3-tert-butyl-2-hydroxy-5-methylphenyl)methyl]-4-methylphenyl] benzene-1,4-dicarboxylate Chemical compound CC(C)(C)C1=CC(C)=CC(CC=2C(=C(C=C(C)C=2)C(C)(C)C)OC(=O)C=2C=CC(=CC=2)C(=O)OC=2C(=CC(C)=CC=2CC=2C(=C(C=C(C)C=2)C(C)(C)C)O)C(C)(C)C)=C1O JWXSMZJIYUUXSV-UHFFFAOYSA-N 0.000 claims description 3
- 229910052794 bromium Inorganic materials 0.000 claims description 3
- 239000001273 butane Substances 0.000 claims description 3
- 229910052801 chlorine Inorganic materials 0.000 claims description 3
- 239000011258 core-shell material Substances 0.000 claims description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 3
- JTXUVYOABGUBMX-UHFFFAOYSA-N didodecyl hydrogen phosphate Chemical compound CCCCCCCCCCCCOP(O)(=O)OCCCCCCCCCCCC JTXUVYOABGUBMX-UHFFFAOYSA-N 0.000 claims description 3
- 229910052731 fluorine Inorganic materials 0.000 claims description 3
- 229910052949 galena Inorganic materials 0.000 claims description 3
- RPQDHPTXJYYUPQ-UHFFFAOYSA-N indium arsenide Chemical compound [In]#[As] RPQDHPTXJYYUPQ-UHFFFAOYSA-N 0.000 claims description 3
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 3
- 150000004767 nitrides Chemical class 0.000 claims description 3
- 229910052757 nitrogen Inorganic materials 0.000 claims description 3
- CYCBIVGDSMISKD-UHFFFAOYSA-N o-tridecyl 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanethioate Chemical compound CCCCCCCCCCCCCOC(=S)CCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 CYCBIVGDSMISKD-UHFFFAOYSA-N 0.000 claims description 3
- YAFOVCNAQTZDQB-UHFFFAOYSA-N octyl diphenyl phosphate Chemical compound C=1C=CC=CC=1OP(=O)(OCCCCCCCC)OC1=CC=CC=C1 YAFOVCNAQTZDQB-UHFFFAOYSA-N 0.000 claims description 3
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 claims description 3
- 239000002530 phenolic antioxidant Substances 0.000 claims description 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 3
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 claims description 3
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- 229910052950 sphalerite Inorganic materials 0.000 claims description 3
- 229960001295 tocopherol Drugs 0.000 claims description 3
- 229930003799 tocopherol Natural products 0.000 claims description 3
- 235000010384 tocopherol Nutrition 0.000 claims description 3
- 239000011732 tocopherol Substances 0.000 claims description 3
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 claims description 3
- GAJQCIFYLSXSEZ-UHFFFAOYSA-L tridecyl phosphate Chemical compound CCCCCCCCCCCCCOP([O-])([O-])=O GAJQCIFYLSXSEZ-UHFFFAOYSA-L 0.000 claims description 3
- OHRVKCZTBPSUIK-UHFFFAOYSA-N tridodecyl phosphate Chemical compound CCCCCCCCCCCCOP(=O)(OCCCCCCCCCCCC)OCCCCCCCCCCCC OHRVKCZTBPSUIK-UHFFFAOYSA-N 0.000 claims description 3
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 claims description 3
- AZSKHRTUXHLAHS-UHFFFAOYSA-N tris(2,4-di-tert-butylphenyl) phosphate Chemical compound CC(C)(C)C1=CC(C(C)(C)C)=CC=C1OP(=O)(OC=1C(=CC(=CC=1)C(C)(C)C)C(C)(C)C)OC1=CC=C(C(C)(C)C)C=C1C(C)(C)C AZSKHRTUXHLAHS-UHFFFAOYSA-N 0.000 claims description 3
- ABZKABVFEBSHLR-UHFFFAOYSA-N tris(2,5-ditert-butylphenyl) phosphate Chemical compound CC(C)(C)C1=CC=C(C(C)(C)C)C(OP(=O)(OC=2C(=CC=C(C=2)C(C)(C)C)C(C)(C)C)OC=2C(=CC=C(C=2)C(C)(C)C)C(C)(C)C)=C1 ABZKABVFEBSHLR-UHFFFAOYSA-N 0.000 claims description 3
- OOZBTDPWFHJVEK-UHFFFAOYSA-N tris(2-nonylphenyl) phosphate Chemical compound CCCCCCCCCC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)CCCCCCCCC)OC1=CC=CC=C1CCCCCCCCC OOZBTDPWFHJVEK-UHFFFAOYSA-N 0.000 claims description 3
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- 229910052984 zinc sulfide Inorganic materials 0.000 claims description 3
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 3
- VSAWBBYYMBQKIK-UHFFFAOYSA-N 4-[[3,5-bis[(3,5-ditert-butyl-4-hydroxyphenyl)methyl]-2,4,6-trimethylphenyl]methyl]-2,6-ditert-butylphenol Chemical compound CC1=C(CC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)C(C)=C(CC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)C(C)=C1CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 VSAWBBYYMBQKIK-UHFFFAOYSA-N 0.000 claims description 2
- FDXLFVQXSBEQEH-UHFFFAOYSA-N CCCCCCCCCCCCCCCCCCOP(=O)OCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 Chemical compound CCCCCCCCCCCCCCCCCCOP(=O)OCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 FDXLFVQXSBEQEH-UHFFFAOYSA-N 0.000 claims description 2
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 2
- CGRTZESQZZGAAU-UHFFFAOYSA-N [2-[3-[1-[3-(3-tert-butyl-4-hydroxy-5-methylphenyl)propanoyloxy]-2-methylpropan-2-yl]-2,4,8,10-tetraoxaspiro[5.5]undecan-9-yl]-2-methylpropyl] 3-(3-tert-butyl-4-hydroxy-5-methylphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C)=CC(CCC(=O)OCC(C)(C)C2OCC3(CO2)COC(OC3)C(C)(C)COC(=O)CCC=2C=C(C(O)=C(C)C=2)C(C)(C)C)=C1 CGRTZESQZZGAAU-UHFFFAOYSA-N 0.000 claims description 2
- IORUEKDKNHHQAL-UHFFFAOYSA-N [2-tert-butyl-6-[(3-tert-butyl-2-hydroxy-5-methylphenyl)methyl]-4-methylphenyl] prop-2-enoate Chemical compound CC(C)(C)C1=CC(C)=CC(CC=2C(=C(C=C(C)C=2)C(C)(C)C)OC(=O)C=C)=C1O IORUEKDKNHHQAL-UHFFFAOYSA-N 0.000 claims description 2
- 239000011593 sulfur Substances 0.000 claims description 2
- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 238000000149 argon plasma sintering Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 16
- 150000003464 sulfur compounds Chemical class 0.000 abstract description 5
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Abstract
【解決手段】 本発明による感光性樹脂組成物は、ナノ蛍光体と、光重合開始剤と、光重合化合物と、抗酸化剤及び溶媒を含み、前記抗酸化剤は、フェノール系、リン系及び硫黄系の化合物から選ばれる1種以上を含む。
【選択図】 図1A
Description
[反応式1]
R・ + O2 → ROO・
[反応式2]
ROO・ + ジ−t−ブチルフェノールのヒドロキシ基 → ROOH
第1及び第2の半導体層154a、154bは、それぞれ第1及び第2のゲート電極124a、124bの上に配設される。
140 ゲート絶縁膜
173 ソース電極
175 ドレイン電極
180a 第1の保護膜
180b 第2の保護膜
230 カラーフィルター
10 表示パネル
12、22 偏光板
30 色変換パネル
310 第1の基板
131 維持電極線
11 第1の配向膜
21 第2配向膜
110 下部基板
121 ゲート線
191 画素電極
220 遮光層
390 キャッピング層
270 共通電極
305 微細空間
307FP 液晶注入部
307 入口部
31 液晶分子
10 表示パネル
30 色変換パネル
372 遮光部材
340B 透過層
210 上部基板
470 有機発光部材
340R、340G 色変換層
Claims (29)
- ナノ蛍光体と、光重合開始剤と、光重合化合物と、抗酸化剤及び溶媒を含み、
前記抗酸化剤は、フェノール系、リン系及び硫黄系の化合物から選ばれる1種以上を含む感光性樹脂組成物。 - 前記ナノ蛍光体は、量子点及び無機蛍光体のうちの少なくとも一方を含む請求項1に記載の感光性樹脂組成物。
- 前記フェノール系抗酸化剤は、2,6−ジターシャリブチル−p−クレゾール、2,6−ジフェニル−4−オクタデシルオキシフェノール、ステアリル(3,5−ジターシャリブチル−4−ヒドロキシフェニル)プロピオナート、ジステアリル(3,5−ジターシャリブチル−4−ヒドロキシベンジル)ホスホナート、トリデシル・3,5−ジターシャリブチル−4−ヒドロキシベンジルチオアセタート、チオジエチレンビス[(3,5−ジターシャリブチル−4−ヒドロキシフェニル)プロピオナート]、4,4'−チオビス(6−ターシャリブチル−m−クレゾール)、2−オクチルチオ−4,6−ジ(3,5−ジターシャリブチル−4−ヒドロキシフェノキシ)−s−トリアジン、2,2'−メチレンビス(4−メチル−6−ターシャリブチルフェノール)、ビス[3,3−ビス(4−ヒドロキシ−3−ターシャリブチルフェニル)酪酸]グリコールエステル、4,4'−ブチリデンビス(2,6−ジターシャリブチルフェノール)、4,4'−ブチリデンビス(6−ターシャリブチル−3−メチルフェノール)、2,2'−エチリデンビス(4,6−ジターシャリブチルフェノール)、1,1,3−トリス(2−メチル−4−ヒドロキシ−5−ターシャリブチルフェニル)ブタン、ビス[2−ターシャリブチル−4−メチル−6−(2−ヒドロキシ−3−ターシャリブチル−5−メチルベンジル)フェニル]テレフタラート、1,3,5−トリス(2,6−ジメチル−3−ヒドロキシ−4−ターシャリブチルベンジル)イソシアヌラート、1,3,5−トリス(3,5−ジターシャリブチル−4−ヒドロキシベンジル)イソシアヌラート、1,3,5−トリス(3,5−ジターシャリブチル−4−ヒドロキシベンジル)−2,4,6−トリメチルベンゼン、1,3,5−トリス[(3,5−ジターシャリブチル−4−ヒドロキシフェニル)プロピオニルオキシエチル]イソシアヌラート、テトラキス[メチレン−3−(3',5'−ジターシャリブチル−4'−ヒドロキシフェニル)プロピオナート]メタン、2−ターシャリブチル−4−メチル−6−(2−アクリロイルオキシ−3−ターシャリブチル−5−メチルベンジル)フェノール、3,9−ビス[2−(3−ターシャリブチル−4−ヒドロキシ−5−メチルヒドロシンナモイルオキシ)−1,1−ジメチルエチル]−2,4,8,10−テトラオキサスピロ[5.5]ウンデカン、トリエチレングリコールビス[β−(3−ターシャリブチル−4−ヒドロキシ−5−メチルフェニル)プロピオナート]及びトコフェノールのうちの少なくとも一種を含む請求項2に記載の感光性樹脂組成物。
- 前記リン系抗酸化剤は、トリフェニルホスファート、トリス(2,4−ジターシャリブチルフェニル)ホスファート、トリス(2,5−ジターシャリブチルフェニル)ホスファート、トリス(ノニルフェニル)ホスファート、トリス(ジノニルフェニル)ホスファート、トリス(モノ、ジ混合ノニルフェニル)ホスファート、ジフェニルアシッドホスファート、2,2'−メチレンビス(4,6−ジターシャリブチルフェニル)オクチルホスファート、ジフェニルデシルホスファート、ジフェニルオクチルホスファート、ジ(ノニルフェニル)ペンタエリスリトールジホスファート、フェニルジイソデシルホスファート、トリブチルホスファート、トリス(2−エチルヘキシル)ホスファート、トリデシルホスファート、トリラウリルホスファート、ジブチルアシッドホスファート、ジラウリルアシッドホスファート、トリラウリルトリチオホスファート、ビス(ネオペンチルグリコール)・1,4−シクロヘキサンジメチルジホスファート、ビス(2,4−ジターシャリブチルフェニル)ペンタエリスリトールジホスファート、ビス(2,5−ジターシャリブチルフェニル)ペンタエリスリトールジホスファート、ビス(2,6−ジターシャリブチル−4−メチルフェニル)ペンタエリスリトールジホスファート、ビス(2,4−ジクミルフェニル)ペンタエリスリトールジホスファート、ジステアリルペンタエリスリトールジホスファート、テトラ(C12−15混合アルキル)−4,4'−イソプロピリデンジフェニルホスファート、ビス[2,2'−メチレンビス(4,6−ジアミルフェニル)]・イソプロピリデンジフェニルホスファート、テトラトリデシル(4,4'−ブチリデンビス(2−ターシャリブチル−5−メチルフェノール)ジホスファート、ヘキサ(トリデシル)・1,1,3−トリス(2−メチル−5−ターシャリブチル−4−ヒドロキシフェニル)ブタン・トリホスファート、テトラキス(2,4−ジターシャリブチルフェニル)ビフェニレンジホスファナート、トリス(2−[2,4,7,9−テトラキスターシャリブチルジベンゾ[d,f][1,3,2]ジオキサホスフェピン−6−イル)オキシ]エチル)アミン、9,10−ジヒドロ−9−オキサ−10−ホスファフェナントレン−10−オキシド、トリス(2−[(2,4,8,10−テトラキスターシャリブチルジベンゾ[d,f][1,3,2]ジオキサホスフェピン−6−イル)オキシ]エチル)アミン及び2−(1,1−ジメチルエチル)−6−メチル−4−[3−[[2,4,8,10−テトラキス(1,1−ジメチルエチル)ジベンゾ[d,f][1,3,2]ジオキサホスフェピン−6−イル]オキシ]プロピル]フェノール2−ブチル−2−エチルプロパンジオ−ル・2,4,6−トリターシャリブチルフェノールモノホスファートのうちの少なくとも一種を含む請求項2に記載の感光性樹脂組成物。
- 前記硫黄系抗酸化剤は、ジアルキルチオジプロピオナート及びポリオールのβ−アルキルメルカプトプロピオン酸エステルのうちの少なくとも一種を含む請求項2に記載の感光性樹脂組成物。
- 前記抗酸化剤は、前記感光性樹脂組成物の固形分の総重量に対して1〜5重量%の含量を有する請求項2に記載の感光性樹脂組成物。
- 前記量子点は、II−VI族化合物、III−V族化合物、III−VI族化合物、IV−VI族化合物、II−III−V族化合物、II−III−VI族化合物、IV族元素及びIV族化合物から選ばれるいずれか1種以上を含み、
前記量子点は、コア及び前記コアを覆うシェルを有するコア−シェル構造である、請求項2に記載の感光性樹脂組成物。 - 前記コアは、CdSe、CdS、ZnS、ZnSe、CdTe、CdSeTe、CdZnS、PbSe、AgInZnS、ZnTe、CdSeS、PbS、PbTe、HgS、HgSe、HgTe、GaN、GaP、GaAs、InP、InZnP、InGaP、InGaN、InAs及びZnOから選ばれる少なくとも一種の化合物を含み、
前記シェルは、CdSe、ZnSe、ZnS、ZnTe、CdTe、PbS、SrSe、CdO、CdS、ZnO、InP、InS、GaP、GaN、GaO、InZnP、InGaP、InGaN、InZnSCdSe及びHgSeから選ばれる少なくとも一種の化合物を含む請求項7に記載の感光性樹脂組成物。 - 前記無機蛍光体は、ガーネット系、シリケート系、硫化物系、酸窒化物系、硝酸塩系及びアルミナート系から選ばれる1種以上を含む請求項2に記載の感光性樹脂組成物。
- 前記無機蛍光体は、Y3Al5O12:Ce3+(YAG:Ce)、Tb3Al5O12:Ce3+(TAG:Ce)、(Sr,Ba,Ca)2SiO4:Eu2+、(Sr,Ba,Ca,Mg,Zn)2Si(OD)4:Eu2+ D=F,Cl,S,N,Br、Ba2MgSi2O7:Eu2+、Ba2SiO4:Eu2+、Ca3(Sc,Mg)2Si3O12:Ce3+、(Ca,Sr)S:Eu2+、(Sr,Ca)Ga2S4:Eu2+、SrSi2O2N2:Eu2+、SiAlON:Ce3+、β−SiAlON:Eu2+、Ca−α−SiAlON:Eu2+、Ba3Si6O12N2:Eu2+、CaAlSiN3:Eu2+、(Sr,Ca)AlSiN3:Eu2+、Sr2Si5N8:Eu2+、(Sr,Ba)Al2O4:Eu2+、(Mg,Sr)Al2O4:Eu2+及びBaMg2Al16O27:Eu2+から選ばれる少なくとも一種を含む請求項9に記載の感光性樹脂組成物。
- 分散剤を更に含む請求項2に記載の感光性樹脂組成物。
- 光散乱体を更に含む請求項11に記載の感光性樹脂組成物。
- 前記光散乱体は、TiO2、Al2O3及びSiO2から選ばれる少なくとも一種を含む請求項12に記載の感光性樹脂組成物。
- 下部基板と、
前記下部基板の上に配設される薄膜トランジスターと、
前記薄膜トランジスターと接続される画素電極と、
前記下部基板と向かい合う上部基板と、
前記下部基板及び前記上部基板の間に配設されるカラーフィルターと、
を備え、
前記カラーフィルターは、ナノ蛍光体及び抗酸化剤を含み、
前記抗酸化剤は、フェノール系、リン系及び硫黄系化合物から選ばれる1種以上を含む感光性樹脂組成物を含む表示装置。 - 前記ナノ蛍光体は、量子点及び無機蛍光体のうちの少なくとも一方を含む請求項14に記載の表示装置。
- 前記抗酸化剤は、前記感光性樹脂組成物の固形分の総重量に対して1〜5重量%の含量を有する請求項15に記載の表示装置。
- 前記量子点は、II−VI族化合物、III−V族化合物、III−VI族化合物、IV−VI族化合物、II−III−V族化合物、II−III−VI族化合物、IV族元素及びIV族化合物から選ばれる1種以上を含み、
前記量子点は、コア及び前記コアを覆うシェルを有するコア−シェル構造である請求項15に記載の表示装置。 - 前記無機蛍光体は、ガーネット系、シリケート系、硫化物系、酸窒化物系、窒化物系及びアルミナート系から選ばれるいずれか一種以上を含む請求項15に記載の表示装置。
- 前記感光性樹脂組成物は、分散剤を更に含む請求項15に記載の表示装置。
- 前記感光性樹脂組成物は、光散乱体を更に含む請求項19に記載の表示装置。
- 第1の基板と、
前記第1の基板の上に配設される複数の色変換層及び透過層と、
前記複数の色変換層のうち隣り合う色変換層の間及び前記複数の色変換層のうちの一つと前記透過層との間に配設される遮光部材と、
を備え、
前記色変換層は、ナノ蛍光体及び抗酸化剤を含み、
前記抗酸化剤は、フェノール系、リン系及び硫黄系化合物から選ばれる1種以上を含む色変換パネル。 - 前記ナノ蛍光体は、量子点及び無機蛍光体のうちの少なくとも一方を含む請求項21に記載の色変換パネル。
- 前記抗酸化剤は、前記感光性樹脂組成物の固形分の総重量に対して1〜5重量%の含量を有する請求項22に記載の色変換パネル。
- 前記感光性樹脂組成物は、分散剤及び光散乱体のうちの少なくとも一方を更に含む請求項22に記載の色変換パネル。
- 表示パネルと、
前記表示パネルの上に配設される色変換パネルと、
を備え、
前記色変換パネルは、
第1の基板と、
前記表示パネルに面する前記第1の基板の一方の面に配設される複数の色変換層及び透過層と、
前記複数の色変換層のうち隣り合う色変換層の間及び前記複数の色変換層のうちの一つと前記透過層との間に配設される遮光部材と、
を備え、
前記色変換層は、ナノ蛍光体及び抗酸化剤を含み、
前記抗酸化剤は、フェノール系、リン系及び硫黄系化合物から選ばれる1種以上を含む表示装置。 - 前記表示パネルは、
下部基板と、
前記下部基板の上に配設される薄膜トランジスターと、
前記薄膜トランジスターと接続される画素電極と、
を備える請求項25に記載の表示装置。 - 前記下部基板から離れて向かい合う上部基板と、
前記下部基板及び前記上部基板の間に配設される液晶層と、
を更に備える請求項26に記載の表示装置。 - 前記画素電極と向かい合うルーフ層と、
前記画素電極と前記ループ層との間の複数の微細空間に配設される液晶層と、
を更に備える請求項26に記載の表示装置。 - 前記画素電極の上に配設される有機発光部材と、
前記有機発光部材の上に配設される共通電極と、
を更に備える請求項26に記載の表示装置。
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KR1020150167387A KR102660293B1 (ko) | 2015-01-09 | 2015-11-27 | 감광성 수지 조성물, 이를 이용한 색변환 패널 및 표시 장치 |
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