JP2015536291A5 - - Google Patents
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- Publication number
- JP2015536291A5 JP2015536291A5 JP2015537192A JP2015537192A JP2015536291A5 JP 2015536291 A5 JP2015536291 A5 JP 2015536291A5 JP 2015537192 A JP2015537192 A JP 2015537192A JP 2015537192 A JP2015537192 A JP 2015537192A JP 2015536291 A5 JP2015536291 A5 JP 2015536291A5
- Authority
- JP
- Japan
- Prior art keywords
- zeolitic material
- range
- acid
- absorption band
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000000463 material Substances 0.000 claims description 36
- 238000000034 method Methods 0.000 claims description 29
- 238000010521 absorption reaction Methods 0.000 claims description 19
- 239000010457 zeolite Substances 0.000 claims description 13
- 238000002329 infrared spectrum Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 229910021536 Zeolite Inorganic materials 0.000 claims description 4
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims 9
- 239000007864 aqueous solution Substances 0.000 claims 8
- 239000000203 mixture Substances 0.000 claims 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims 3
- 150000007522 mineralic acids Chemical class 0.000 claims 3
- 150000007524 organic acids Chemical class 0.000 claims 3
- 150000003839 salts Chemical class 0.000 claims 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 2
- 229910052782 aluminium Inorganic materials 0.000 claims 2
- 229910052796 boron Inorganic materials 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- 239000013078 crystal Substances 0.000 claims 2
- 229910052733 gallium Inorganic materials 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- 229910052710 silicon Inorganic materials 0.000 claims 2
- 229910052718 tin Inorganic materials 0.000 claims 2
- 229910052719 titanium Inorganic materials 0.000 claims 2
- 229910052726 zirconium Inorganic materials 0.000 claims 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- 150000003863 ammonium salts Chemical group 0.000 claims 1
- 229910052732 germanium Inorganic materials 0.000 claims 1
- 239000011521 glass Substances 0.000 claims 1
- 229910052738 indium Inorganic materials 0.000 claims 1
- 229940098779 methanesulfonic acid Drugs 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 235000006408 oxalic acid Nutrition 0.000 claims 1
- 238000001308 synthesis method Methods 0.000 claims 1
- SCPYDCQAZCOKTP-UHFFFAOYSA-N silanol Chemical compound [SiH3]O SCPYDCQAZCOKTP-UHFFFAOYSA-N 0.000 description 6
- 238000010306 acid treatment Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 125000005372 silanol group Chemical group 0.000 description 2
- 229910008051 Si-OH Inorganic materials 0.000 description 1
- 229910006358 Si—OH Inorganic materials 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12189040.4 | 2012-10-18 | ||
| EP12189040 | 2012-10-18 | ||
| PCT/EP2013/071041 WO2014060260A1 (en) | 2012-10-18 | 2013-10-09 | Post-treatment of a zeolitic material |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015536291A JP2015536291A (ja) | 2015-12-21 |
| JP2015536291A5 true JP2015536291A5 (enExample) | 2016-12-01 |
| JP6367812B2 JP6367812B2 (ja) | 2018-08-01 |
Family
ID=47115431
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015537192A Active JP6367812B2 (ja) | 2012-10-18 | 2013-10-09 | ゼオライト材料の後処理 |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US10000387B2 (enExample) |
| EP (1) | EP2909144B1 (enExample) |
| JP (1) | JP6367812B2 (enExample) |
| KR (1) | KR102179936B1 (enExample) |
| CN (1) | CN104854031B (enExample) |
| BR (1) | BR112015008391B1 (enExample) |
| ES (1) | ES2697129T3 (enExample) |
| MX (1) | MX357216B (enExample) |
| MY (1) | MY181782A (enExample) |
| RU (1) | RU2637021C2 (enExample) |
| SG (2) | SG11201503017XA (enExample) |
| WO (1) | WO2014060260A1 (enExample) |
| ZA (1) | ZA201503392B (enExample) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016058541A1 (en) | 2014-10-15 | 2016-04-21 | Basf Se | Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom |
| US10556801B2 (en) | 2015-02-12 | 2020-02-11 | Basf Se | Process for the preparation of a dealuminated zeolitic material having the BEA framework structure |
| JP6879680B2 (ja) * | 2015-06-29 | 2021-06-02 | 日揮触媒化成株式会社 | 高シリカチャバザイト型ゼオライトの製造方法および高シリカチャバザイト型ゼオライト |
| CN108602056B (zh) * | 2015-12-09 | 2022-06-28 | 巴斯夫公司 | Cha型沸石材料和使用环烷基-和乙基三甲基铵化合物的组合制备它们的方法 |
| MX2018009534A (es) * | 2016-02-03 | 2018-09-06 | Basf Corp | Catalizador de chabazita cointercambiada con cobre y hierro. |
| KR102389627B1 (ko) * | 2016-03-30 | 2022-04-22 | 바스프 에스이 | 제올라이트 물질의 플래시 소성 방법 |
| US10953390B2 (en) | 2016-05-23 | 2021-03-23 | Tosoh Corporation | CHA-type zeolite and method for producing the same |
| KR102275364B1 (ko) * | 2016-06-07 | 2021-07-12 | 셰브런 유.에스.에이.인크. | 고농도-실리카 afx 프레임워크형 제올라이트 |
| EP3519354A1 (en) * | 2016-09-30 | 2019-08-07 | Johnson Matthey Public Limited Company | A novel zeolite synthesis with a fluoride source |
| CN110402246A (zh) | 2017-03-15 | 2019-11-01 | 巴斯夫欧洲公司 | 通过使羟基羧酸或酰胺与酸性BEA(H-β多晶型A)型沸石反应而制备环状二酯或环状二酰胺的方法 |
| CN108946755B (zh) * | 2017-05-22 | 2020-08-07 | 中国石油化工股份有限公司 | 无锗iwr沸石分子筛的合成方法 |
| MY190284A (en) * | 2017-10-11 | 2022-04-12 | Tosoh Corp | Metal-containing cha-type zeolite and method for producing the same |
| CN111601772A (zh) * | 2018-02-06 | 2020-08-28 | 巴斯夫欧洲公司 | 制备具有rth型骨架结构的沸石材料的方法 |
| FR3081347B1 (fr) * | 2018-05-24 | 2023-07-28 | Ifp Energies Now | Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote |
| US20220339611A1 (en) * | 2019-09-20 | 2022-10-27 | Basf Se | Synthesis and Use of a Zeolitic Material Having the ITH Framework Structure Type |
| CN111252781B (zh) * | 2020-02-05 | 2022-01-07 | 浙江大学 | 无有机模板剂晶种法合成高硅kfi沸石分子筛的方法 |
| JP7514467B2 (ja) * | 2020-05-12 | 2024-07-11 | 国立大学法人 東京大学 | ゼオライトの製造方法、ゼオライト、触媒、及び吸着剤 |
| WO2022195076A1 (en) | 2021-03-19 | 2022-09-22 | Basf Se | Process for the dealumination of zeolitic materials |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2445747A1 (fr) | 1979-01-05 | 1980-08-01 | Armines | Procede de fabrication de pieces en silicium nitrure |
| JP2826868B2 (ja) * | 1989-04-24 | 1998-11-18 | 鐘紡株式会社 | 安定化された合成ゼオライト及びその製造法 |
| US5443812A (en) * | 1989-04-24 | 1995-08-22 | Kanebo Ltd. | Stabilized synthetic zeolite and a process for the preparation thereof |
| CA2015277C (en) | 1989-04-24 | 2000-01-11 | Kazuhiko Nakajima | Stabilized synthetic zeolite and a process for the preparation thereof |
| JPH08690B2 (ja) * | 1989-08-18 | 1996-01-10 | 鐘紡株式会社 | 安定化された合成ゼオライト及びその製造法 |
| JP2808033B2 (ja) * | 1990-02-20 | 1998-10-08 | 鐘紡株式会社 | 合成ゼオライトをイオン交換すると共に安定化する方法 |
| JPH08689B2 (ja) * | 1989-07-24 | 1996-01-10 | 鐘紡株式会社 | 安定性のある合成ゼオライト及びその製造法 |
| JPH0596175A (ja) | 1991-10-03 | 1993-04-20 | Catalysts & Chem Ind Co Ltd | 変性結晶性アルミノシリケートゼオライトの製造方法 |
| TW270090B (enExample) | 1993-09-30 | 1996-02-11 | Sanyo Sekiyu Kagaku Kk | |
| US5508019A (en) | 1994-06-30 | 1996-04-16 | Arco Chemical Technology, L.P. | Dealumination of aluminosilicates |
| DE10061715A1 (de) * | 2000-12-12 | 2002-06-13 | Basf Ag | Verfahren zur Herstellung von Homo- und Copolymeren des Isobutens |
| US7011802B2 (en) | 2000-12-22 | 2006-03-14 | California Institute Of Technology | Synthesis of molecular sieves by hydrothermal treatment with acid |
| WO2004050548A2 (en) | 2002-11-27 | 2004-06-17 | Pq Holding, Inc. | High surface area zeolites and methods for preparation and use thereof |
| EP2025402A1 (en) | 2007-07-31 | 2009-02-18 | Total Petrochemicals Research Feluy | Phosphorus modified molecular sieves, their use in conversion of organics to olefins |
| EP2174713A1 (en) * | 2008-10-13 | 2010-04-14 | BP Chemicals Limited | Dealumination process |
| JP5508744B2 (ja) * | 2009-03-13 | 2014-06-04 | 出光興産株式会社 | ベータゼオライトの製造方法及び水素化分解触媒の製造方法 |
| EP2251314A1 (en) | 2009-05-14 | 2010-11-17 | BP Chemicals Limited | Carbonylation process |
| EP2694437B1 (en) | 2011-04-08 | 2020-10-21 | Basf Se | Process for producing acylation catalyst |
| JP6267211B2 (ja) | 2012-10-18 | 2018-01-24 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | 脱ホウ素化ｍｗｗゼオライトの後処理 |
| WO2014060259A1 (en) | 2012-10-18 | 2014-04-24 | Basf Se | Post-treatment of deboronated zeolite beta |
-
2013
- 2013-10-09 JP JP2015537192A patent/JP6367812B2/ja active Active
- 2013-10-09 SG SG11201503017XA patent/SG11201503017XA/en unknown
- 2013-10-09 BR BR112015008391-9A patent/BR112015008391B1/pt active IP Right Grant
- 2013-10-09 ES ES13774183T patent/ES2697129T3/es active Active
- 2013-10-09 RU RU2015118227A patent/RU2637021C2/ru active
- 2013-10-09 SG SG10201703183UA patent/SG10201703183UA/en unknown
- 2013-10-09 MY MYPI2015001013A patent/MY181782A/en unknown
- 2013-10-09 CN CN201380062829.8A patent/CN104854031B/zh active Active
- 2013-10-09 EP EP13774183.1A patent/EP2909144B1/en not_active Revoked
- 2013-10-09 KR KR1020157012944A patent/KR102179936B1/ko active Active
- 2013-10-09 WO PCT/EP2013/071041 patent/WO2014060260A1/en not_active Ceased
- 2013-10-09 US US14/436,180 patent/US10000387B2/en active Active
- 2013-10-09 MX MX2015004946A patent/MX357216B/es active IP Right Grant
-
2015
- 2015-05-15 ZA ZA2015/03392A patent/ZA201503392B/en unknown
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