KR102179936B1 - 제올라이트 물질의 후처리 - Google Patents

제올라이트 물질의 후처리 Download PDF

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KR102179936B1
KR102179936B1 KR1020157012944A KR20157012944A KR102179936B1 KR 102179936 B1 KR102179936 B1 KR 102179936B1 KR 1020157012944 A KR1020157012944 A KR 1020157012944A KR 20157012944 A KR20157012944 A KR 20157012944A KR 102179936 B1 KR102179936 B1 KR 102179936B1
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zeolite material
zeolite
range
acid
treatment
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KR20150074085A (ko
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슈테판 마우러
파루크 외즈키림
안드레이-니콜라 파르불레스쿠
제프 양
울리히 뮐러
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바스프 에스이
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B01J35/1014—
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/38—Base treatment

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
KR1020157012944A 2012-10-18 2013-10-09 제올라이트 물질의 후처리 Active KR102179936B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12189040.4 2012-10-18
EP12189040 2012-10-18
PCT/EP2013/071041 WO2014060260A1 (en) 2012-10-18 2013-10-09 Post-treatment of a zeolitic material

Publications (2)

Publication Number Publication Date
KR20150074085A KR20150074085A (ko) 2015-07-01
KR102179936B1 true KR102179936B1 (ko) 2020-11-17

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KR1020157012944A Active KR102179936B1 (ko) 2012-10-18 2013-10-09 제올라이트 물질의 후처리

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Country Link
US (1) US10000387B2 (enExample)
EP (1) EP2909144B1 (enExample)
JP (1) JP6367812B2 (enExample)
KR (1) KR102179936B1 (enExample)
CN (1) CN104854031B (enExample)
BR (1) BR112015008391B1 (enExample)
ES (1) ES2697129T3 (enExample)
MX (1) MX357216B (enExample)
MY (1) MY181782A (enExample)
RU (1) RU2637021C2 (enExample)
SG (2) SG11201503017XA (enExample)
WO (1) WO2014060260A1 (enExample)
ZA (1) ZA201503392B (enExample)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016058541A1 (en) 2014-10-15 2016-04-21 Basf Se Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom
US10556801B2 (en) 2015-02-12 2020-02-11 Basf Se Process for the preparation of a dealuminated zeolitic material having the BEA framework structure
JP6879680B2 (ja) * 2015-06-29 2021-06-02 日揮触媒化成株式会社 高シリカチャバザイト型ゼオライトの製造方法および高シリカチャバザイト型ゼオライト
CN108602056B (zh) * 2015-12-09 2022-06-28 巴斯夫公司 Cha型沸石材料和使用环烷基-和乙基三甲基铵化合物的组合制备它们的方法
MX2018009534A (es) * 2016-02-03 2018-09-06 Basf Corp Catalizador de chabazita cointercambiada con cobre y hierro.
KR102389627B1 (ko) * 2016-03-30 2022-04-22 바스프 에스이 제올라이트 물질의 플래시 소성 방법
US10953390B2 (en) 2016-05-23 2021-03-23 Tosoh Corporation CHA-type zeolite and method for producing the same
KR102275364B1 (ko) * 2016-06-07 2021-07-12 셰브런 유.에스.에이.인크. 고농도-실리카 afx 프레임워크형 제올라이트
EP3519354A1 (en) * 2016-09-30 2019-08-07 Johnson Matthey Public Limited Company A novel zeolite synthesis with a fluoride source
CN110402246A (zh) 2017-03-15 2019-11-01 巴斯夫欧洲公司 通过使羟基羧酸或酰胺与酸性BEA(H-β多晶型A)型沸石反应而制备环状二酯或环状二酰胺的方法
CN108946755B (zh) * 2017-05-22 2020-08-07 中国石油化工股份有限公司 无锗iwr沸石分子筛的合成方法
MY190284A (en) * 2017-10-11 2022-04-12 Tosoh Corp Metal-containing cha-type zeolite and method for producing the same
CN111601772A (zh) * 2018-02-06 2020-08-28 巴斯夫欧洲公司 制备具有rth型骨架结构的沸石材料的方法
FR3081347B1 (fr) * 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
US20220339611A1 (en) * 2019-09-20 2022-10-27 Basf Se Synthesis and Use of a Zeolitic Material Having the ITH Framework Structure Type
CN111252781B (zh) * 2020-02-05 2022-01-07 浙江大学 无有机模板剂晶种法合成高硅kfi沸石分子筛的方法
JP7514467B2 (ja) * 2020-05-12 2024-07-11 国立大学法人 東京大学 ゼオライトの製造方法、ゼオライト、触媒、及び吸着剤
WO2022195076A1 (en) 2021-03-19 2022-09-22 Basf Se Process for the dealumination of zeolitic materials

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JP2010215434A (ja) 2009-03-13 2010-09-30 Idemitsu Kosan Co Ltd ベータゼオライトの製造方法及び水素化分解触媒の製造方法

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Also Published As

Publication number Publication date
EP2909144B1 (en) 2018-08-15
MX2015004946A (es) 2016-02-22
SG10201703183UA (en) 2017-06-29
CN104854031B (zh) 2018-04-06
US20150284255A1 (en) 2015-10-08
BR112015008391B1 (pt) 2022-03-29
RU2637021C2 (ru) 2017-11-29
SG11201503017XA (en) 2015-05-28
US10000387B2 (en) 2018-06-19
ZA201503392B (en) 2019-12-18
RU2015118227A (ru) 2016-12-10
WO2014060260A1 (en) 2014-04-24
BR112015008391A2 (pt) 2017-08-08
KR20150074085A (ko) 2015-07-01
MY181782A (en) 2021-01-06
MX357216B (es) 2018-06-29
CN104854031A (zh) 2015-08-19
EP2909144A1 (en) 2015-08-26
ES2697129T3 (es) 2019-01-22
JP2015536291A (ja) 2015-12-21
JP6367812B2 (ja) 2018-08-01

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