CN104854031B - 沸石材料的后处理 - Google Patents

沸石材料的后处理 Download PDF

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Publication number
CN104854031B
CN104854031B CN201380062829.8A CN201380062829A CN104854031B CN 104854031 B CN104854031 B CN 104854031B CN 201380062829 A CN201380062829 A CN 201380062829A CN 104854031 B CN104854031 B CN 104854031B
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zeolitic material
acid
aqueous solution
zeolitic
range
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Chinese (zh)
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CN104854031A (zh
Inventor
S·毛雷尔
F·奥伊泽克瑞姆
安德烈-尼古拉·帕乌莱斯库
J·杨
U·穆勒
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/38—Base treatment

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
CN201380062829.8A 2012-10-18 2013-10-09 沸石材料的后处理 Active CN104854031B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12189040 2012-10-18
EP12189040.4 2012-10-18
PCT/EP2013/071041 WO2014060260A1 (en) 2012-10-18 2013-10-09 Post-treatment of a zeolitic material

Publications (2)

Publication Number Publication Date
CN104854031A CN104854031A (zh) 2015-08-19
CN104854031B true CN104854031B (zh) 2018-04-06

Family

ID=47115431

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CN201380062829.8A Active CN104854031B (zh) 2012-10-18 2013-10-09 沸石材料的后处理

Country Status (13)

Country Link
US (1) US10000387B2 (enExample)
EP (1) EP2909144B1 (enExample)
JP (1) JP6367812B2 (enExample)
KR (1) KR102179936B1 (enExample)
CN (1) CN104854031B (enExample)
BR (1) BR112015008391B1 (enExample)
ES (1) ES2697129T3 (enExample)
MX (1) MX357216B (enExample)
MY (1) MY181782A (enExample)
RU (1) RU2637021C2 (enExample)
SG (2) SG11201503017XA (enExample)
WO (1) WO2014060260A1 (enExample)
ZA (1) ZA201503392B (enExample)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6656242B2 (ja) 2014-10-15 2020-03-04 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ゼオライト材料の固体熱合成方法及びそれから得られるゼオライト
US10556801B2 (en) 2015-02-12 2020-02-11 Basf Se Process for the preparation of a dealuminated zeolitic material having the BEA framework structure
JP6879680B2 (ja) * 2015-06-29 2021-06-02 日揮触媒化成株式会社 高シリカチャバザイト型ゼオライトの製造方法および高シリカチャバザイト型ゼオライト
KR102659804B1 (ko) * 2015-12-09 2024-04-23 바스프 코포레이션 Cha-형 제올라이트 물질 및 사이클로알킬- 및 에틸트라이메틸암모늄 화합물의 조합을 사용하는 이의 제조 방법
KR102797067B1 (ko) * 2016-02-03 2025-04-18 바스프 모바일 에미션스 카탈리스츠 엘엘씨 구리 및 철 동시-교환된 캐버자이트 촉매
WO2017167622A1 (en) * 2016-03-30 2017-10-05 Basf Se Process for the flash calcination of a zeolitic material
EP3473598A4 (en) 2016-05-23 2020-03-18 Tosoh Corporation CHA TYPE ZEOLITE AND PRODUCTION METHOD THEREFOR
CN109153578A (zh) * 2016-06-07 2019-01-04 雪佛龙美国公司 高硅afx骨架型分子筛
GB2569757B (en) * 2016-09-30 2022-09-14 Johnson Matthey Plc A novel zeolite synthesis with a fluoride source
EP3596057A1 (en) 2017-03-15 2020-01-22 Basf Se Process for preparing a cyclic diester or a cyclic diamide by reacting a hydroxycarboxylic acid or amide with an acidic bea-type (h-beta polymorph a) zeolite
CN108946755B (zh) * 2017-05-22 2020-08-07 中国石油化工股份有限公司 无锗iwr沸石分子筛的合成方法
MY190284A (en) * 2017-10-11 2022-04-12 Tosoh Corp Metal-containing cha-type zeolite and method for producing the same
EP3749611A4 (en) * 2018-02-06 2022-02-23 Basf Se PROCESS FOR PRODUCTION OF A ZEOLITE MATERIAL WITH RTH FRAME STRUCTURE
FR3081347B1 (fr) * 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
JP2022548975A (ja) * 2019-09-20 2022-11-22 ビーエーエスエフ ソシエタス・ヨーロピア 骨格構造型ｉｔｈを有するゼオライト材料の合成方法および使用方法
CN111252781B (zh) * 2020-02-05 2022-01-07 浙江大学 无有机模板剂晶种法合成高硅kfi沸石分子筛的方法
JP7514467B2 (ja) * 2020-05-12 2024-07-11 国立大学法人 東京大学 ゼオライトの製造方法、ゼオライト、触媒、及び吸着剤
JP2024510661A (ja) 2021-03-19 2024-03-08 ビーエーエスエフ ソシエタス・ヨーロピア ゼオライト材料の脱アルミニウム化方法
EP4691986A1 (en) 2023-03-31 2026-02-11 Mitsui Kinzoku Company, Limited Bea-type zeolite

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0394948A2 (en) * 1989-04-24 1990-10-31 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
EP0690024A2 (en) * 1994-06-30 1996-01-03 ARCO Chemical Technology, L.P. Dealumination of aluminosilicates
WO2004050548A2 (en) * 2002-11-27 2004-06-17 Pq Holding, Inc. High surface area zeolites and methods for preparation and use thereof
CN102421740A (zh) * 2009-05-14 2012-04-18 英国石油化学品有限公司 羰基化方法

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FR2445747A1 (fr) 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
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JP2826868B2 (ja) * 1989-04-24 1998-11-18 鐘紡株式会社 安定化された合成ゼオライト及びその製造法
JPH08689B2 (ja) 1989-07-24 1996-01-10 鐘紡株式会社 安定性のある合成ゼオライト及びその製造法
US5443812A (en) * 1989-04-24 1995-08-22 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
JPH0596175A (ja) 1991-10-03 1993-04-20 Catalysts & Chem Ind Co Ltd 変性結晶性アルミノシリケートゼオライトの製造方法
CN1081086C (zh) 1993-09-30 2002-03-20 山阳石油化学株式会社 沸石系催化剂的部分脱铝方法
DE10061715A1 (de) * 2000-12-12 2002-06-13 Basf Ag Verfahren zur Herstellung von Homo- und Copolymeren des Isobutens
US7011802B2 (en) 2000-12-22 2006-03-14 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
EP2025402A1 (en) 2007-07-31 2009-02-18 Total Petrochemicals Research Feluy Phosphorus modified molecular sieves, their use in conversion of organics to olefins
EP2174713A1 (en) 2008-10-13 2010-04-14 BP Chemicals Limited Dealumination process
JP5508744B2 (ja) * 2009-03-13 2014-06-04 出光興産株式会社 ベータゼオライトの製造方法及び水素化分解触媒の製造方法
US8710271B2 (en) 2011-04-08 2014-04-29 Basf Se Process for the production of an acylation catalyst
RU2638851C2 (ru) 2012-10-18 2017-12-18 Басф Се Последующая обработка деборированного цеолита mww
WO2014060259A1 (en) 2012-10-18 2014-04-24 Basf Se Post-treatment of deboronated zeolite beta

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0394948A2 (en) * 1989-04-24 1990-10-31 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
EP0690024A2 (en) * 1994-06-30 1996-01-03 ARCO Chemical Technology, L.P. Dealumination of aluminosilicates
WO2004050548A2 (en) * 2002-11-27 2004-06-17 Pq Holding, Inc. High surface area zeolites and methods for preparation and use thereof
CN102421740A (zh) * 2009-05-14 2012-04-18 英国石油化学品有限公司 羰基化方法

Also Published As

Publication number Publication date
MY181782A (en) 2021-01-06
MX2015004946A (es) 2016-02-22
BR112015008391A2 (pt) 2017-08-08
MX357216B (es) 2018-06-29
SG11201503017XA (en) 2015-05-28
RU2637021C2 (ru) 2017-11-29
KR20150074085A (ko) 2015-07-01
JP2015536291A (ja) 2015-12-21
US20150284255A1 (en) 2015-10-08
SG10201703183UA (en) 2017-06-29
CN104854031A (zh) 2015-08-19
RU2015118227A (ru) 2016-12-10
EP2909144A1 (en) 2015-08-26
ZA201503392B (en) 2019-12-18
EP2909144B1 (en) 2018-08-15
JP6367812B2 (ja) 2018-08-01
KR102179936B1 (ko) 2020-11-17
ES2697129T3 (es) 2019-01-22
WO2014060260A1 (en) 2014-04-24
US10000387B2 (en) 2018-06-19
BR112015008391B1 (pt) 2022-03-29

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