ES2697129T3 - Postratamiento de un material zeolítico - Google Patents

Postratamiento de un material zeolítico Download PDF

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Publication number
ES2697129T3
ES2697129T3 ES13774183T ES13774183T ES2697129T3 ES 2697129 T3 ES2697129 T3 ES 2697129T3 ES 13774183 T ES13774183 T ES 13774183T ES 13774183 T ES13774183 T ES 13774183T ES 2697129 T3 ES2697129 T3 ES 2697129T3
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ES
Spain
Prior art keywords
zeolitic material
range
hours
treatment
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES13774183T
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English (en)
Spanish (es)
Inventor
Stefan Maurer
Faruk Özkirim
Andrei-Nicolae Parvulescu
Jeff Yang
Ulrich Müller
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BASF SE
Original Assignee
BASF SE
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Application filed by BASF SE filed Critical BASF SE
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Publication of ES2697129T3 publication Critical patent/ES2697129T3/es
Active legal-status Critical Current
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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026After-treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007Zeolite Beta
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015CHA-type, e.g. Chabazite, LZ-218
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/60Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61Surface area
    • B01J35/61310-100 m2/g
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46Other types characterised by their X-ray diffraction pattern and their defined composition
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30After treatment, characterised by the means used
    • B01J2229/38Base treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
ES13774183T 2012-10-18 2013-10-09 Postratamiento de un material zeolítico Active ES2697129T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12189040 2012-10-18
PCT/EP2013/071041 WO2014060260A1 (en) 2012-10-18 2013-10-09 Post-treatment of a zeolitic material

Publications (1)

Publication Number Publication Date
ES2697129T3 true ES2697129T3 (es) 2019-01-22

Family

ID=47115431

Family Applications (1)

Application Number Title Priority Date Filing Date
ES13774183T Active ES2697129T3 (es) 2012-10-18 2013-10-09 Postratamiento de un material zeolítico

Country Status (13)

Country Link
US (1) US10000387B2 (enExample)
EP (1) EP2909144B1 (enExample)
JP (1) JP6367812B2 (enExample)
KR (1) KR102179936B1 (enExample)
CN (1) CN104854031B (enExample)
BR (1) BR112015008391B1 (enExample)
ES (1) ES2697129T3 (enExample)
MX (1) MX357216B (enExample)
MY (1) MY181782A (enExample)
RU (1) RU2637021C2 (enExample)
SG (2) SG11201503017XA (enExample)
WO (1) WO2014060260A1 (enExample)
ZA (1) ZA201503392B (enExample)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016058541A1 (en) 2014-10-15 2016-04-21 Basf Se Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom
JP6685314B2 (ja) * 2015-02-12 2020-04-22 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se Bea骨格構造を有する脱アルミニウム化ゼオライト材料を製造する方法
JP6879680B2 (ja) * 2015-06-29 2021-06-02 日揮触媒化成株式会社 高シリカチャバザイト型ゼオライトの製造方法および高シリカチャバザイト型ゼオライト
CN108602056B (zh) * 2015-12-09 2022-06-28 巴斯夫公司 Cha型沸石材料和使用环烷基-和乙基三甲基铵化合物的组合制备它们的方法
WO2017134581A1 (en) * 2016-02-03 2017-08-10 Basf Corporation Copper and iron co-exchanged chabazite catalyst
WO2017167622A1 (en) * 2016-03-30 2017-10-05 Basf Se Process for the flash calcination of a zeolitic material
MY197118A (en) * 2016-05-23 2023-05-26 Tosoh Corp Cha-type zeolite and production method therefor
CN109153578A (zh) * 2016-06-07 2019-01-04 雪佛龙美国公司 高硅afx骨架型分子筛
CN109923070A (zh) * 2016-09-30 2019-06-21 庄信万丰股份有限公司 采用氟化物源的新的沸石合成
CN110402246A (zh) 2017-03-15 2019-11-01 巴斯夫欧洲公司 通过使羟基羧酸或酰胺与酸性BEA(H-β多晶型A)型沸石反应而制备环状二酯或环状二酰胺的方法
CN108946755B (zh) * 2017-05-22 2020-08-07 中国石油化工股份有限公司 无锗iwr沸石分子筛的合成方法
MY190284A (en) * 2017-10-11 2022-04-12 Tosoh Corp Metal-containing cha-type zeolite and method for producing the same
KR20200118129A (ko) * 2018-02-06 2020-10-14 바스프 에스이 Rth 골격 구조 유형을 갖는 제올라이트 물질의 제조 방법
FR3081347B1 (fr) * 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
CN114423711A (zh) * 2019-09-20 2022-04-29 巴斯夫欧洲公司 具有ith骨架结构类型的沸石材料的合成和用途
CN111252781B (zh) * 2020-02-05 2022-01-07 浙江大学 无有机模板剂晶种法合成高硅kfi沸石分子筛的方法
JP7514467B2 (ja) * 2020-05-12 2024-07-11 国立大学法人 東京大学 ゼオライトの製造方法、ゼオライト、触媒、及び吸着剤
CN117098726A (zh) 2021-03-19 2023-11-21 巴斯夫欧洲公司 使沸石材料脱铝的方法
WO2024204696A1 (ja) 2023-03-31 2024-10-03 三井金属鉱業株式会社 Bea型ゼオライト

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2445747A1 (fr) 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
US5443812A (en) 1989-04-24 1995-08-22 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
JP2826868B2 (ja) * 1989-04-24 1998-11-18 鐘紡株式会社 安定化された合成ゼオライト及びその製造法
JP2808033B2 (ja) * 1990-02-20 1998-10-08 鐘紡株式会社 合成ゼオライトをイオン交換すると共に安定化する方法
JPH08689B2 (ja) * 1989-07-24 1996-01-10 鐘紡株式会社 安定性のある合成ゼオライト及びその製造法
CA2015277C (en) * 1989-04-24 2000-01-11 Kazuhiko Nakajima Stabilized synthetic zeolite and a process for the preparation thereof
JPH08690B2 (ja) * 1989-08-18 1996-01-10 鐘紡株式会社 安定化された合成ゼオライト及びその製造法
JPH0596175A (ja) 1991-10-03 1993-04-20 Catalysts & Chem Ind Co Ltd 変性結晶性アルミノシリケートゼオライトの製造方法
EP0671212B1 (en) 1993-09-30 2000-05-17 Sanyo Petrochemical Co. Ltd. Method of partial dealuminization of zeolitic catalyst
US5508019A (en) * 1994-06-30 1996-04-16 Arco Chemical Technology, L.P. Dealumination of aluminosilicates
DE10061715A1 (de) * 2000-12-12 2002-06-13 Basf Ag Verfahren zur Herstellung von Homo- und Copolymeren des Isobutens
US7011802B2 (en) 2000-12-22 2006-03-14 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
AU2003295841A1 (en) 2002-11-27 2004-06-23 Pq Holding, Inc. High surface area zeolites and methods for preparation and use thereof
EP2025402A1 (en) 2007-07-31 2009-02-18 Total Petrochemicals Research Feluy Phosphorus modified molecular sieves, their use in conversion of organics to olefins
EP2174713A1 (en) 2008-10-13 2010-04-14 BP Chemicals Limited Dealumination process
JP5508744B2 (ja) * 2009-03-13 2014-06-04 出光興産株式会社 ベータゼオライトの製造方法及び水素化分解触媒の製造方法
EP2251314A1 (en) * 2009-05-14 2010-11-17 BP Chemicals Limited Carbonylation process
JP5982469B2 (ja) 2011-04-08 2016-08-31 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se アシル化触媒の製造方法
JP6267211B2 (ja) 2012-10-18 2018-01-24 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 脱ホウ素化mwwゼオライトの後処理
JP6306029B2 (ja) 2012-10-18 2018-04-04 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 脱ホウ素化ゼオライトベータの後処理

Also Published As

Publication number Publication date
BR112015008391A2 (pt) 2017-08-08
SG11201503017XA (en) 2015-05-28
MX357216B (es) 2018-06-29
MY181782A (en) 2021-01-06
MX2015004946A (es) 2016-02-22
KR102179936B1 (ko) 2020-11-17
RU2015118227A (ru) 2016-12-10
CN104854031A (zh) 2015-08-19
US20150284255A1 (en) 2015-10-08
JP6367812B2 (ja) 2018-08-01
RU2637021C2 (ru) 2017-11-29
CN104854031B (zh) 2018-04-06
US10000387B2 (en) 2018-06-19
SG10201703183UA (en) 2017-06-29
EP2909144B1 (en) 2018-08-15
KR20150074085A (ko) 2015-07-01
ZA201503392B (en) 2019-12-18
BR112015008391B1 (pt) 2022-03-29
JP2015536291A (ja) 2015-12-21
WO2014060260A1 (en) 2014-04-24
EP2909144A1 (en) 2015-08-26

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