ES2697129T3 - Postratamiento de un material zeolítico - Google Patents

Postratamiento de un material zeolítico Download PDF

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Publication number
ES2697129T3
ES2697129T3 ES13774183T ES13774183T ES2697129T3 ES 2697129 T3 ES2697129 T3 ES 2697129T3 ES 13774183 T ES13774183 T ES 13774183T ES 13774183 T ES13774183 T ES 13774183T ES 2697129 T3 ES2697129 T3 ES 2697129T3
Authority
ES
Spain
Prior art keywords
zeolitic material
range
hours
treatment
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES13774183T
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English (en)
Spanish (es)
Inventor
Stefan Maurer
Faruk Özkirim
Andrei-Nicolae Parvulescu
Jeff Yang
Ulrich Müller
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=47115431&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2697129(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2697129T3 publication Critical patent/ES2697129T3/es
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/38—Base treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
ES13774183T 2012-10-18 2013-10-09 Postratamiento de un material zeolítico Active ES2697129T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12189040 2012-10-18
PCT/EP2013/071041 WO2014060260A1 (en) 2012-10-18 2013-10-09 Post-treatment of a zeolitic material

Publications (1)

Publication Number Publication Date
ES2697129T3 true ES2697129T3 (es) 2019-01-22

Family

ID=47115431

Family Applications (1)

Application Number Title Priority Date Filing Date
ES13774183T Active ES2697129T3 (es) 2012-10-18 2013-10-09 Postratamiento de un material zeolítico

Country Status (13)

Country Link
US (1) US10000387B2 (enExample)
EP (1) EP2909144B1 (enExample)
JP (1) JP6367812B2 (enExample)
KR (1) KR102179936B1 (enExample)
CN (1) CN104854031B (enExample)
BR (1) BR112015008391B1 (enExample)
ES (1) ES2697129T3 (enExample)
MX (1) MX357216B (enExample)
MY (1) MY181782A (enExample)
RU (1) RU2637021C2 (enExample)
SG (2) SG10201703183UA (enExample)
WO (1) WO2014060260A1 (enExample)
ZA (1) ZA201503392B (enExample)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107074566A (zh) 2014-10-15 2017-08-18 巴斯夫欧洲公司 沸石材料的固热合成以及由此得到的沸石
JP6685314B2 (ja) * 2015-02-12 2020-04-22 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Ｂｅａ骨格構造を有する脱アルミニウム化ゼオライト材料を製造する方法
JP6879680B2 (ja) * 2015-06-29 2021-06-02 日揮触媒化成株式会社 高シリカチャバザイト型ゼオライトの製造方法および高シリカチャバザイト型ゼオライト
US10913660B2 (en) * 2015-12-09 2021-02-09 Basf Corporation CHA type zeolitic materials and methods for their preparation using combinations of cycloalkyl and ethyltrimethylammonium compounds
KR102797067B1 (ko) * 2016-02-03 2025-04-18 바스프 모바일 에미션스 카탈리스츠 엘엘씨 구리 및 철 동시-교환된 캐버자이트 촉매
WO2017167622A1 (en) * 2016-03-30 2017-10-05 Basf Se Process for the flash calcination of a zeolitic material
MY197118A (en) 2016-05-23 2023-05-26 Tosoh Corp Cha-type zeolite and production method therefor
ES2901603T3 (es) * 2016-06-07 2022-03-23 Chevron Usa Inc Zeolitas de tipo marco AFX con alto contenido de sílice
GB2569757B (en) * 2016-09-30 2022-09-14 Johnson Matthey Plc A novel zeolite synthesis with a fluoride source
CN110402246A (zh) 2017-03-15 2019-11-01 巴斯夫欧洲公司 通过使羟基羧酸或酰胺与酸性BEA(H-β多晶型A)型沸石反应而制备环状二酯或环状二酰胺的方法
CN108946755B (zh) * 2017-05-22 2020-08-07 中国石油化工股份有限公司 无锗iwr沸石分子筛的合成方法
MY190284A (en) * 2017-10-11 2022-04-12 Tosoh Corp Metal-containing cha-type zeolite and method for producing the same
WO2019154071A1 (en) * 2018-02-06 2019-08-15 Basf Se A process for preparing a zeolitic material having a framework structure type RTH
FR3081347B1 (fr) * 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
KR20220069039A (ko) * 2019-09-20 2022-05-26 바스프 에스이 Ith 프레임워크 구조 유형을 갖는 제올라이트 물질의 합성 및 용도
CN111252781B (zh) * 2020-02-05 2022-01-07 浙江大学 无有机模板剂晶种法合成高硅kfi沸石分子筛的方法
JP7514467B2 (ja) * 2020-05-12 2024-07-11 国立大学法人 東京大学 ゼオライトの製造方法、ゼオライト、触媒、及び吸着剤
KR20230157496A (ko) 2021-03-19 2023-11-16 바스프 에스이 제올라이트 물질의 탈알루미늄화 방법
EP4691986A4 (en) 2023-03-31 2026-06-24 Mitsui Kinzoku Co Limited BEA TYPE ZEOLITH

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FR2445747A1 (fr) 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
JPH08689B2 (ja) * 1989-07-24 1996-01-10 鐘紡株式会社 安定性のある合成ゼオライト及びその製造法
US5443812A (en) * 1989-04-24 1995-08-22 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
JP2826868B2 (ja) * 1989-04-24 1998-11-18 鐘紡株式会社 安定化された合成ゼオライト及びその製造法
JPH08690B2 (ja) * 1989-08-18 1996-01-10 鐘紡株式会社 安定化された合成ゼオライト及びその製造法
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JP2808033B2 (ja) * 1990-02-20 1998-10-08 鐘紡株式会社 合成ゼオライトをイオン交換すると共に安定化する方法
JPH0596175A (ja) 1991-10-03 1993-04-20 Catalysts & Chem Ind Co Ltd 変性結晶性アルミノシリケートゼオライトの製造方法
JP3809958B2 (ja) * 1993-09-30 2006-08-16 山陽石油化学株式会社 ゼオライト系触媒の部分的脱アルミニウム方法
US5508019A (en) * 1994-06-30 1996-04-16 Arco Chemical Technology, L.P. Dealumination of aluminosilicates
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MY169039A (en) 2012-10-18 2019-02-07 Basf Se Post-treatment of deboronated mww zeolite

Also Published As

Publication number Publication date
US20150284255A1 (en) 2015-10-08
MX357216B (es) 2018-06-29
JP6367812B2 (ja) 2018-08-01
BR112015008391A2 (pt) 2017-08-08
SG11201503017XA (en) 2015-05-28
RU2637021C2 (ru) 2017-11-29
ZA201503392B (en) 2019-12-18
RU2015118227A (ru) 2016-12-10
MY181782A (en) 2021-01-06
EP2909144A1 (en) 2015-08-26
US10000387B2 (en) 2018-06-19
EP2909144B1 (en) 2018-08-15
BR112015008391B1 (pt) 2022-03-29
KR20150074085A (ko) 2015-07-01
KR102179936B1 (ko) 2020-11-17
CN104854031B (zh) 2018-04-06
JP2015536291A (ja) 2015-12-21
WO2014060260A1 (en) 2014-04-24
MX2015004946A (es) 2016-02-22
CN104854031A (zh) 2015-08-19
SG10201703183UA (en) 2017-06-29

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