ES2697129T3 - Postratamiento de un material zeolítico - Google Patents

Postratamiento de un material zeolítico Download PDF

Info

Publication number
ES2697129T3
ES2697129T3 ES13774183T ES13774183T ES2697129T3 ES 2697129 T3 ES2697129 T3 ES 2697129T3 ES 13774183 T ES13774183 T ES 13774183T ES 13774183 T ES13774183 T ES 13774183T ES 2697129 T3 ES2697129 T3 ES 2697129T3
Authority
ES
Spain
Prior art keywords
zeolitic material
range
hours
treatment
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES13774183T
Other languages
English (en)
Spanish (es)
Inventor
Stefan Maurer
Faruk Özkirim
Andrei-Nicolae Parvulescu
Jeff Yang
Ulrich Müller
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=47115431&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2697129(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2697129T3 publication Critical patent/ES2697129T3/es
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/38—Base treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
ES13774183T 2012-10-18 2013-10-09 Postratamiento de un material zeolítico Active ES2697129T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12189040 2012-10-18
PCT/EP2013/071041 WO2014060260A1 (en) 2012-10-18 2013-10-09 Post-treatment of a zeolitic material

Publications (1)

Publication Number Publication Date
ES2697129T3 true ES2697129T3 (es) 2019-01-22

Family

ID=47115431

Family Applications (1)

Application Number Title Priority Date Filing Date
ES13774183T Active ES2697129T3 (es) 2012-10-18 2013-10-09 Postratamiento de un material zeolítico

Country Status (13)

Country Link
US (1) US10000387B2 (enExample)
EP (1) EP2909144B1 (enExample)
JP (1) JP6367812B2 (enExample)
KR (1) KR102179936B1 (enExample)
CN (1) CN104854031B (enExample)
BR (1) BR112015008391B1 (enExample)
ES (1) ES2697129T3 (enExample)
MX (1) MX357216B (enExample)
MY (1) MY181782A (enExample)
RU (1) RU2637021C2 (enExample)
SG (2) SG11201503017XA (enExample)
WO (1) WO2014060260A1 (enExample)
ZA (1) ZA201503392B (enExample)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107074566A (zh) 2014-10-15 2017-08-18 巴斯夫欧洲公司 沸石材料的固热合成以及由此得到的沸石
WO2016128917A1 (en) 2015-02-12 2016-08-18 Basf Se Process for the preparation of a dealuminated zeolitic material having the bea framework structure
JP6879680B2 (ja) * 2015-06-29 2021-06-02 日揮触媒化成株式会社 高シリカチャバザイト型ゼオライトの製造方法および高シリカチャバザイト型ゼオライト
US10913660B2 (en) * 2015-12-09 2021-02-09 Basf Corporation CHA type zeolitic materials and methods for their preparation using combinations of cycloalkyl and ethyltrimethylammonium compounds
WO2017134581A1 (en) * 2016-02-03 2017-08-10 Basf Corporation Copper and iron co-exchanged chabazite catalyst
US10995008B2 (en) * 2016-03-30 2021-05-04 Basf Se Process for the flash calcination of a zeolitic material
CN109195911B (zh) 2016-05-23 2023-04-07 东曹株式会社 Cha型沸石和其制造方法
ES2901603T3 (es) * 2016-06-07 2022-03-23 Chevron Usa Inc Zeolitas de tipo marco AFX con alto contenido de sílice
JP2020502017A (ja) * 2016-09-30 2020-01-23 ジョンソン、マッセイ、パブリック、リミテッド、カンパニーＪｏｈｎｓｏｎ Ｍａｔｔｈｅｙ Ｐｕｂｌｉｃ Ｌｉｍｉｔｅｄ Ｃｏｍｐａｎｙ フッ化物源を用いる新規ゼオライト合成法
US20190375724A1 (en) 2017-03-15 2019-12-12 Basf Se Process for preparing a cyclic diester or a cyclic diamide by reacting a hydroxycarboxylic acid or amide with an acidic bea-type (h-beta polymorph a) zeolite
CN108946755B (zh) * 2017-05-22 2020-08-07 中国石油化工股份有限公司 无锗iwr沸石分子筛的合成方法
MY190284A (en) * 2017-10-11 2022-04-12 Tosoh Corp Metal-containing cha-type zeolite and method for producing the same
WO2019154071A1 (en) * 2018-02-06 2019-08-15 Basf Se A process for preparing a zeolitic material having a framework structure type RTH
FR3081347B1 (fr) * 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
KR20220069039A (ko) * 2019-09-20 2022-05-26 바스프 에스이 Ith 프레임워크 구조 유형을 갖는 제올라이트 물질의 합성 및 용도
CN111252781B (zh) * 2020-02-05 2022-01-07 浙江大学 无有机模板剂晶种法合成高硅kfi沸石分子筛的方法
JP7514467B2 (ja) * 2020-05-12 2024-07-11 国立大学法人 東京大学 ゼオライトの製造方法、ゼオライト、触媒、及び吸着剤
KR20230157496A (ko) 2021-03-19 2023-11-16 바스프 에스이 제올라이트 물질의 탈알루미늄화 방법
JPWO2024204696A1 (enExample) 2023-03-31 2024-10-03

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2445747A1 (fr) 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
JPH08689B2 (ja) * 1989-07-24 1996-01-10 鐘紡株式会社 安定性のある合成ゼオライト及びその製造法
JP2808033B2 (ja) * 1990-02-20 1998-10-08 鐘紡株式会社 合成ゼオライトをイオン交換すると共に安定化する方法
JPH08690B2 (ja) * 1989-08-18 1996-01-10 鐘紡株式会社 安定化された合成ゼオライト及びその製造法
JP2826868B2 (ja) * 1989-04-24 1998-11-18 鐘紡株式会社 安定化された合成ゼオライト及びその製造法
US5443812A (en) * 1989-04-24 1995-08-22 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
DE69025088T2 (de) * 1989-04-24 1996-06-13 Kanebo Ltd Stabilisierter, synthetischer Zeolith sowie Verfahren zu dessen Herstellung
JPH0596175A (ja) 1991-10-03 1993-04-20 Catalysts & Chem Ind Co Ltd 変性結晶性アルミノシリケートゼオライトの製造方法
WO1995009050A1 (fr) * 1993-09-30 1995-04-06 Sanyo Petrochemical Co., Ltd. Procede de desaluminisation partielle d'un catalyseur zeolitique
US5508019A (en) * 1994-06-30 1996-04-16 Arco Chemical Technology, L.P. Dealumination of aluminosilicates
DE10061715A1 (de) * 2000-12-12 2002-06-13 Basf Ag Verfahren zur Herstellung von Homo- und Copolymeren des Isobutens
AU2002248274A1 (en) 2000-12-22 2002-07-30 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
US20040141911A1 (en) 2002-11-27 2004-07-22 Pq Corporation, Inc. High surface zeolites and methods for preparation and use thereof
EP2025402A1 (en) 2007-07-31 2009-02-18 Total Petrochemicals Research Feluy Phosphorus modified molecular sieves, their use in conversion of organics to olefins
EP2174713A1 (en) * 2008-10-13 2010-04-14 BP Chemicals Limited Dealumination process
JP5508744B2 (ja) 2009-03-13 2014-06-04 出光興産株式会社 ベータゼオライトの製造方法及び水素化分解触媒の製造方法
EP2251314A1 (en) 2009-05-14 2010-11-17 BP Chemicals Limited Carbonylation process
JP5982469B2 (ja) 2011-04-08 2016-08-31 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ アシル化触媒の製造方法
SG11201503031WA (en) 2012-10-18 2015-05-28 Basf Se Post-treatment of deboronated zeolite beta
CN104854028B (zh) 2012-10-18 2017-07-18 巴斯夫欧洲公司 脱硼mww沸石的后处理

Also Published As

Publication number Publication date
JP2015536291A (ja) 2015-12-21
EP2909144B1 (en) 2018-08-15
KR102179936B1 (ko) 2020-11-17
JP6367812B2 (ja) 2018-08-01
RU2637021C2 (ru) 2017-11-29
WO2014060260A1 (en) 2014-04-24
MX2015004946A (es) 2016-02-22
MY181782A (en) 2021-01-06
CN104854031B (zh) 2018-04-06
ZA201503392B (en) 2019-12-18
US10000387B2 (en) 2018-06-19
KR20150074085A (ko) 2015-07-01
BR112015008391B1 (pt) 2022-03-29
MX357216B (es) 2018-06-29
RU2015118227A (ru) 2016-12-10
SG10201703183UA (en) 2017-06-29
EP2909144A1 (en) 2015-08-26
BR112015008391A2 (pt) 2017-08-08
SG11201503017XA (en) 2015-05-28
US20150284255A1 (en) 2015-10-08
CN104854031A (zh) 2015-08-19

Similar Documents

Publication Publication Date Title
ES2697129T3 (es) Postratamiento de un material zeolítico
ES2821890T3 (es) Procedimiento de preparación de melonal
EP2909141B1 (en) Post-treatment of deboronated mww zeolite
CN109081359B (zh) 分子筛scm-15、其合成方法及其用途
KR102389627B1 (ko) 제올라이트 물질의 플래시 소성 방법
KR20180091063A (ko) Cha-형 제올라이트 물질 및 사이클로알킬- 및 에틸트라이메틸암모늄 화합물의 조합을 사용하는 이의 제조 방법
BR112016001518B1 (pt) processo para a regeneração de um catalisador
EP2909143B1 (en) Post-treatment of zeolite beta
JP7592683B2 (ja) フレームワークタイプａｅｉを有するゼオライト系材料を製造する方法
CN104379504B (zh) 沸石材料及其利用烯基三烷基铵化合物的制备方法
WO2021122533A1 (en) Process for continuous interzeolitic conversion
KR102835708B1 (ko) Cha형 제올라이트 물질 및 이의 제조 방법
ES2877670T3 (es) Procedimiento de regeneración de un catalizador de zeolita de titanio para la epoxidación de propileno
ES2748650A1 (es) Material cristalino de naturaleza zeolítica IDM-1
WO2022195076A1 (en) Process for the dealumination of zeolitic materials
Lewis et al. UZM-4: A stable Si-rich form of the BPH framework type
EP4526253A1 (en) A cha type zeolite and the method of synthesising said zeolite