JP2014526429A5 - - Google Patents
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- Publication number
- JP2014526429A5 JP2014526429A5 JP2014529123A JP2014529123A JP2014526429A5 JP 2014526429 A5 JP2014526429 A5 JP 2014526429A5 JP 2014529123 A JP2014529123 A JP 2014529123A JP 2014529123 A JP2014529123 A JP 2014529123A JP 2014526429 A5 JP2014526429 A5 JP 2014526429A5
- Authority
- JP
- Japan
- Prior art keywords
- zeolitic material
- mixture
- crystallization
- mother liquor
- seed crystals
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 28
- 239000000463 material Substances 0.000 claims 18
- 239000000203 mixture Substances 0.000 claims 15
- 239000013078 crystal Substances 0.000 claims 9
- 238000002425 crystallisation Methods 0.000 claims 7
- 230000008025 crystallization Effects 0.000 claims 7
- 239000012452 mother liquor Substances 0.000 claims 7
- 239000010457 zeolite Substances 0.000 claims 5
- 229910018557 Si O Inorganic materials 0.000 claims 3
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Inorganic materials [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 claims 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 2
- 229910021536 Zeolite Inorganic materials 0.000 claims 2
- 238000001354 calcination Methods 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- 238000010189 synthetic method Methods 0.000 claims 2
- 238000005406 washing Methods 0.000 claims 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims 1
- 239000003463 adsorbent Substances 0.000 claims 1
- 150000004645 aluminates Chemical class 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- 229910052796 boron Inorganic materials 0.000 claims 1
- 238000005119 centrifugation Methods 0.000 claims 1
- 238000010908 decantation Methods 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 229910052733 gallium Inorganic materials 0.000 claims 1
- 229910052732 germanium Inorganic materials 0.000 claims 1
- 229910052738 indium Inorganic materials 0.000 claims 1
- 238000005342 ion exchange Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000002808 molecular sieve Substances 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims 1
- 229910052718 tin Inorganic materials 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- 238000011282 treatment Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011079502 | 2011-09-09 | ||
| CNPCT/CN2011/079502 | 2011-09-09 | ||
| PCT/IB2012/054637 WO2013035077A1 (en) | 2011-09-09 | 2012-09-07 | Process for the organotemplate-free synthetic production of a zeolitic material using recycled mother liquor |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014526429A JP2014526429A (ja) | 2014-10-06 |
| JP2014526429A5 true JP2014526429A5 (enExample) | 2015-10-29 |
| JP6054969B2 JP6054969B2 (ja) | 2016-12-27 |
Family
ID=47830008
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014529123A Active JP6054969B2 (ja) | 2011-09-09 | 2012-09-07 | 有機テンプレートを用いずにリサイクル母液を使用してゼオライト材料を合成する方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US9028795B2 (enExample) |
| EP (1) | EP2753578B1 (enExample) |
| JP (1) | JP6054969B2 (enExample) |
| CN (1) | CN103917492B (enExample) |
| WO (1) | WO2013035077A1 (enExample) |
| ZA (1) | ZA201402508B (enExample) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2011157839A1 (en) * | 2010-06-18 | 2011-12-22 | Basf Se | Organotemplate-free synthetic process for the production of a zeolitic material of the lev-type structure |
| US20130202524A1 (en) | 2012-02-06 | 2013-08-08 | Basf Se | Iron- And Copper-Containing Zeolite Beta From Organotemplate-Free Synthesis And Use Thereof In The Selective Catalytic Reduction Of NOx |
| CN103979569B (zh) * | 2014-06-04 | 2016-06-22 | 陕西省煤化工工程技术研究中心 | 一种具有多级孔结构的磷酸硅铝分子筛的制备方法 |
| JP6546738B2 (ja) * | 2014-11-12 | 2019-07-17 | 日立造船株式会社 | アルデヒド分解触媒および排ガス処理設備ならびに排ガス処理方法 |
| JP6271405B2 (ja) * | 2014-12-05 | 2018-01-31 | 三井造船株式会社 | ゼオライト膜を用いた脱水方法 |
| JP6759596B2 (ja) * | 2016-01-18 | 2020-09-23 | 東ソー株式会社 | Ａｆｘ型ゼオライト及びその製造方法 |
| KR102461888B1 (ko) * | 2016-06-17 | 2022-11-02 | 바스프 에스이 | 제올라이트계 물질의 연속 합성 방법 |
| JP6345372B1 (ja) * | 2017-01-13 | 2018-06-20 | 三井金属鉱業株式会社 | 排気ガス浄化用組成物 |
| EP3661646B1 (en) * | 2017-08-04 | 2025-12-03 | BASF Mobile Emissions Catalysts LLC | A zeolitic material having framework type cha and comprising a transition metal and one or more of potassium and cesium |
| US11897778B2 (en) | 2017-11-22 | 2024-02-13 | Basf Se | Zeolite synthesis in a reactor with controlled velocity profile |
| CN118439628A (zh) | 2017-12-14 | 2024-08-06 | 东曹株式会社 | β型沸石及其制造方法 |
| JP7207154B2 (ja) * | 2018-05-16 | 2023-01-18 | 三菱ケミカル株式会社 | ゼオライトの製造方法 |
| JP7412411B2 (ja) * | 2018-08-02 | 2024-01-12 | ビーエーエスエフ ソシエタス・ヨーロピア | 有機テンプレートを担持した種結晶を用いたゼオライト材料の連続合成方法 |
| CN110040742B (zh) * | 2019-05-09 | 2022-10-21 | 嘉兴学院 | 晶种导向法合成全硅zsm-51沸石的方法 |
| CN110407221B (zh) * | 2019-06-21 | 2020-12-04 | 合肥派森新材料技术有限公司 | 一种菱沸石分子筛的制备方法、scr催化剂的制备方法 |
| CN112010322B (zh) * | 2020-08-20 | 2022-02-15 | 华中科技大学 | 一种分子筛的制备方法及其应用和废水的利用方法 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3308069A (en) | 1964-05-01 | 1967-03-07 | Mobil Oil Corp | Catalytic composition of a crystalline zeolite |
| GB1157477A (en) * | 1966-03-07 | 1969-07-09 | Exxon Research Engineering Co | Synthetic Zeolite Process |
| DE2640541C2 (de) * | 1976-09-09 | 1984-04-19 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Synthese von Zeolithen |
| US4164551A (en) * | 1977-12-19 | 1979-08-14 | W. R. Grace & Co. | Preparation of zeolite |
| GB8329973D0 (en) * | 1983-11-10 | 1983-12-14 | Exxon Research Engineering Co | Recycled zeolite l preparation |
| US4554145A (en) | 1984-04-16 | 1985-11-19 | Mobil Oil Corporation | Preparation of crystalline silicate zeolite Beta |
| US4642226A (en) | 1984-04-16 | 1987-02-10 | Mobil Oil Corporation | Process for the preparation of zeolite Beta using dibenzyldimethylammonium ions and the product produced |
| SU1610778A1 (ru) * | 1988-10-04 | 1996-10-27 | Л.В. Будовская | Способ получения цеолита типа у |
| FR2712894B1 (fr) * | 1993-11-25 | 1995-12-29 | Pechiney Aluminium | Zéolite A à blancheur contrôlée, procédé de fabrication et application. |
| CN1079372C (zh) * | 1997-11-13 | 2002-02-20 | 中国石油化工总公司 | 钛硅分子筛制备工艺 |
| RU2151739C1 (ru) * | 1998-06-03 | 2000-06-27 | ООО Компания Катахим | Способ получения высокомодульного цеолита типа y |
| WO2000006494A1 (en) * | 1998-07-29 | 2000-02-10 | Exxon Chemical Patents, Inc. | Crystalline molecular sieves |
| US6099820A (en) * | 1999-08-17 | 2000-08-08 | Chevron U.S.A. Inc. | Method for making MTT zeolites without an organic template |
| DE102005049362A1 (de) * | 2005-10-12 | 2007-04-19 | Basf Ag | Verfahren zur Herstellung eines Silikates |
| JP6176891B2 (ja) * | 2007-08-13 | 2017-08-09 | ピーキュー コーポレイション | 新規鉄含有アルミノケイ酸塩ゼオライト、ならびにその作製方法および使用方法 |
| CN101249968B (zh) * | 2008-03-10 | 2010-06-02 | 吉林大学 | 无有机模板剂合成Beta分子筛的方法 |
| WO2010084930A1 (ja) * | 2009-01-22 | 2010-07-29 | 三菱化学株式会社 | 窒素酸化物浄化用触媒及びその製造方法 |
| CN104876237A (zh) | 2009-06-18 | 2015-09-02 | 巴斯夫欧洲公司 | 生产沸石材料的无有机模板合成方法 |
| US8865121B2 (en) * | 2009-06-18 | 2014-10-21 | Basf Se | Organotemplate-free synthetic process for the production of a zeolitic material |
| JP4904417B2 (ja) * | 2009-07-27 | 2012-03-28 | 日本化学工業株式会社 | ベータ型ゼオライト及びその製造方法 |
| CN102040229B (zh) * | 2009-10-21 | 2012-11-21 | 中国石油化工股份有限公司 | 一种mcm-22分子筛的合成方法 |
-
2012
- 2012-09-07 WO PCT/IB2012/054637 patent/WO2013035077A1/en not_active Ceased
- 2012-09-07 US US13/606,614 patent/US9028795B2/en active Active
- 2012-09-07 JP JP2014529123A patent/JP6054969B2/ja active Active
- 2012-09-07 CN CN201280054364.7A patent/CN103917492B/zh active Active
- 2012-09-07 EP EP12830180.1A patent/EP2753578B1/en active Active
-
2014
- 2014-04-07 ZA ZA2014/02508A patent/ZA201402508B/en unknown
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