JP2013529588A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2013529588A5 JP2013529588A5 JP2013514837A JP2013514837A JP2013529588A5 JP 2013529588 A5 JP2013529588 A5 JP 2013529588A5 JP 2013514837 A JP2013514837 A JP 2013514837A JP 2013514837 A JP2013514837 A JP 2013514837A JP 2013529588 A5 JP2013529588 A5 JP 2013529588A5
- Authority
- JP
- Japan
- Prior art keywords
- zeolitic material
- mixture
- lev
- type
- framework structure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 35
- 239000000463 material Substances 0.000 claims 30
- 239000000203 mixture Substances 0.000 claims 24
- 239000013078 crystal Substances 0.000 claims 7
- 239000010457 zeolite Substances 0.000 claims 7
- 238000002425 crystallisation Methods 0.000 claims 5
- 230000008025 crystallization Effects 0.000 claims 5
- 238000006467 substitution reaction Methods 0.000 claims 4
- 229910021536 Zeolite Inorganic materials 0.000 claims 3
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 3
- 239000002904 solvent Substances 0.000 claims 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical group [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 2
- 229910052782 aluminium Inorganic materials 0.000 claims 2
- 229910052796 boron Inorganic materials 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- 238000010304 firing Methods 0.000 claims 2
- 229910052733 gallium Inorganic materials 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 229910052738 indium Inorganic materials 0.000 claims 2
- 229910052751 metal Inorganic materials 0.000 claims 2
- 239000002184 metal Substances 0.000 claims 2
- 150000002739 metals Chemical class 0.000 claims 2
- 229910052700 potassium Chemical group 0.000 claims 2
- 239000011591 potassium Chemical group 0.000 claims 2
- 229910052710 silicon Inorganic materials 0.000 claims 2
- 229910052708 sodium Inorganic materials 0.000 claims 2
- 239000011734 sodium Substances 0.000 claims 2
- 125000005207 tetraalkylammonium group Chemical group 0.000 claims 2
- 229910052718 tin Inorganic materials 0.000 claims 2
- 229910052719 titanium Inorganic materials 0.000 claims 2
- 229910052726 zirconium Inorganic materials 0.000 claims 2
- 239000003463 adsorbent Substances 0.000 claims 1
- 238000013019 agitation Methods 0.000 claims 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims 1
- 238000001354 calcination Methods 0.000 claims 1
- UNYSKUBLZGJSLV-UHFFFAOYSA-L calcium;1,3,5,2,4,6$l^{2}-trioxadisilaluminane 2,4-dioxide;dihydroxide;hexahydrate Chemical compound O.O.O.O.O.O.[OH-].[OH-].[Ca+2].O=[Si]1O[Al]O[Si](=O)O1.O=[Si]1O[Al]O[Si](=O)O1 UNYSKUBLZGJSLV-UHFFFAOYSA-L 0.000 claims 1
- 125000002091 cationic group Chemical group 0.000 claims 1
- 150000001768 cations Chemical class 0.000 claims 1
- 229910052676 chabazite Inorganic materials 0.000 claims 1
- ZJHQDSMOYNLVLX-UHFFFAOYSA-N diethyl(dimethyl)azanium Chemical compound CC[N+](C)(C)CC ZJHQDSMOYNLVLX-UHFFFAOYSA-N 0.000 claims 1
- 238000006073 displacement reaction Methods 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 238000005342 ion exchange Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000002808 molecular sieve Substances 0.000 claims 1
- 239000002798 polar solvent Substances 0.000 claims 1
- 238000000634 powder X-ray diffraction Methods 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims 1
- -1 tetraalkylammonium compound Chemical class 0.000 claims 1
- SEACXNRNJAXIBM-UHFFFAOYSA-N triethyl(methyl)azanium Chemical class CC[N+](C)(CC)CC SEACXNRNJAXIBM-UHFFFAOYSA-N 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNPCT/CN2010/074073 | 2010-06-18 | ||
| CNPCT/CN2010/074073 | 2010-06-18 | ||
| CNPCT/CN2010/078062 | 2010-10-25 | ||
| CNPCT/CN2010/078062 | 2010-10-25 | ||
| PCT/IB2011/052658 WO2011158219A1 (en) | 2010-06-18 | 2011-06-17 | Alkali-free synthesis of zeolitic materials of lev-type structure |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013529588A JP2013529588A (ja) | 2013-07-22 |
| JP2013529588A5 true JP2013529588A5 (enExample) | 2014-07-31 |
| JP6034286B2 JP6034286B2 (ja) | 2016-11-30 |
Family
ID=45329179
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013514837A Expired - Fee Related JP6034286B2 (ja) | 2010-06-18 | 2011-06-17 | Ｌｅｖ型構造ゼオライト系材料のアルカリフリー合成 |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US9334171B2 (enExample) |
| EP (1) | EP2582628A4 (enExample) |
| JP (1) | JP6034286B2 (enExample) |
| WO (1) | WO2011158219A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2582628A4 (en) * | 2010-06-18 | 2014-12-31 | Basf Se | ALKALINE-FREE SYNTHESIS OF LEVEL-LIKE TYPE ZEOLITIC MATERIALS |
| US9527751B2 (en) | 2011-11-11 | 2016-12-27 | Basf Se | Organotemplate-free synthetic process for the production of a zeolitic material of the CHA-type structure |
| PL2953897T3 (pl) * | 2013-02-05 | 2022-01-03 | Basf Se | Sposób wytwarzania materiału zeolitowego zawierającego bor o strukturze szkieletowej MWW |
| CN103601211B (zh) * | 2013-12-04 | 2015-07-22 | 北京化工大学 | 一种合成分子筛ssz-13的方法 |
| ES2574500B1 (es) | 2014-12-17 | 2017-03-31 | Consejo Superior De Investigaciones Científicas (Csic) | Síntesis de la zeolita con la estructura cristalina CHA, procedimiento de síntesis y su uso en aplicaciones catalíticas |
| JP2018079428A (ja) * | 2016-11-17 | 2018-05-24 | 東ソー株式会社 | 炭化水素吸着剤及び炭化水素の吸着除去方法 |
| WO2019173711A1 (en) | 2018-03-09 | 2019-09-12 | Pq Corporation | Production of hydrothermally stable cha zeolites |
| CN112654582A (zh) | 2018-08-24 | 2021-04-13 | 优米科尔股份公司及两合公司 | Cha型分子筛的制备方法 |
| CN109850915B (zh) * | 2019-03-29 | 2022-07-12 | 金华职业技术学院 | 一种y分子筛转晶合成的rub-50分子筛及其方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3459676A (en) * | 1966-06-14 | 1969-08-05 | Mobil Oil Corp | Synthetic zeolite and method for preparing the same |
| EP0040016B1 (en) * | 1980-05-13 | 1984-09-12 | Imperial Chemical Industries Plc | Zeolite nu-3 |
| CA1205443A (en) * | 1982-03-29 | 1986-06-03 | Thomas R. Cannan | Zeolite lz- 132 |
| JPS5978923A (ja) * | 1982-09-27 | 1984-05-08 | モ−ビル・オイル・コ−ポレ−シヨン | ゼオライト |
| US5334367A (en) * | 1982-09-27 | 1994-08-02 | Mobil Oil Corp. | Zeolite ZSM-45 |
| CA1204718A (en) | 1982-09-27 | 1986-05-20 | Edward J. Rosinski | Zeolite |
| US4495303A (en) * | 1983-11-29 | 1985-01-22 | Mobil Oil Corporation | Process for making zeolite ZSM-45 with a dimethyldiethylammonium directing agent |
| KR20010079583A (ko) * | 1998-07-29 | 2001-08-22 | 엑손 케미칼 패턴츠 인코포레이티드 | 분자체의 제조방법 |
| US7375050B2 (en) * | 2003-04-28 | 2008-05-20 | Exxonmobil Chemical Patents Inc. | Synthesis and use of aluminophosphates and silicoaluminophosphates |
| ES2396233T3 (es) * | 2003-12-23 | 2013-02-20 | Exxonmobil Chemical Patents, Inc. | Zeolita de tipo AEI y su uso en la conversión de compuestos oxigenados en olefinas |
| CN101607716A (zh) * | 2003-12-23 | 2009-12-23 | 埃克森美孚化学专利公司 | 菱沸石型分子筛、其合成及其在含氧化合物转化成烯烃中的应用 |
| WO2007094949A1 (en) * | 2006-02-14 | 2007-08-23 | Exxonmobil Chemical Patents Inc. | Process for manufacturing molecular sieve of mfs framework type and its use |
| MX2009010369A (es) * | 2007-03-26 | 2010-02-17 | Pq Corp | Material cristalino, microporoso, novedoso, que comprende un tamiz molecular o zeolita que tiene una estructura de abertura de poro de 8 anillos y metodos para hacer y utilizar los mismos. |
| EP2082803A1 (en) * | 2008-01-25 | 2009-07-29 | Total Petrochemicals Research Feluy | Process for obtaining catalyst composites comprising MeAPO and their use in conversion of organics to olefins |
| EP2582628A4 (en) * | 2010-06-18 | 2014-12-31 | Basf Se | ALKALINE-FREE SYNTHESIS OF LEVEL-LIKE TYPE ZEOLITIC MATERIALS |
| WO2011158218A1 (en) * | 2010-06-18 | 2011-12-22 | Basf Se | Zeolitic materials of lev-type structure and methods for their production |
-
2011
- 2011-06-17 EP EP11795287.9A patent/EP2582628A4/en not_active Withdrawn
- 2011-06-17 WO PCT/IB2011/052658 patent/WO2011158219A1/en not_active Ceased
- 2011-06-17 US US13/163,377 patent/US9334171B2/en not_active Expired - Fee Related
- 2011-06-17 JP JP2013514837A patent/JP6034286B2/ja not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2013529587A5 (enExample) | ||
| JP2013529588A5 (enExample) | ||
| JP6656242B2 (ja) | ゼオライト材料の固体熱合成方法及びそれから得られるゼオライト | |
| JP2015511919A5 (enExample) | ||
| JP2013532112A5 (enExample) | ||
| JP5485369B2 (ja) | 新規構造制御剤を使用してｃｈａ型モレキュラーシーブを調製する方法 | |
| JP2017532282A5 (enExample) | ||
| RU2014153662A (ru) | Цеолитные материалы типа сна и способы их получения с применением циклоалкиламмониевых соединений | |
| JP6318990B2 (ja) | Ａｅｉ型ゼオライトの製造方法 | |
| CN105636905B (zh) | 合成硼硅酸盐ton骨架型分子筛 | |
| JP2016502487A5 (enExample) | ||
| JP2016502490A (ja) | コロイドアルミノケイ酸塩を使用するｃｈａ型モレキュラーシーブを調製する方法 | |
| JP6759833B2 (ja) | Ａｅｉ型ゼオライトの製造方法 | |
| JP2014511819A5 (enExample) | ||
| JP2014526429A5 (enExample) | ||
| KR20170016339A (ko) | 분자체 ssz-99 | |
| JP2016539893A5 (enExample) | ||
| JP2021121579A (ja) | Ａｅｉ型ゼオライトの製造方法 | |
| JP2015519282A5 (enExample) | ||
| JP2020502023A5 (enExample) | ||
| EP3224198B1 (en) | Method for preparing aluminosilicate molecular sieves having the cha framework type | |
| JP2014530164A (ja) | 新規な構造指向剤を用いるｌｔａ型ゼオライトを調製するための方法 | |
| US20190308929A1 (en) | Process for the conversion of ethylene glycol to ethylenediamine employing a zeolite catalyst | |
| JP2017538655A5 (enExample) | ||
| JP6100361B2 (ja) | モレキュラーシーブｓｓｚ−８７及びその合成 |