JP2015524806A5 - - Google Patents
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- Publication number
- JP2015524806A5 JP2015524806A5 JP2015524381A JP2015524381A JP2015524806A5 JP 2015524806 A5 JP2015524806 A5 JP 2015524806A5 JP 2015524381 A JP2015524381 A JP 2015524381A JP 2015524381 A JP2015524381 A JP 2015524381A JP 2015524806 A5 JP2015524806 A5 JP 2015524806A5
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- JP
- Japan
- Prior art keywords
- preparation
- compound
- alkyl
- group
- formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 claims description 37
- 238000002360 preparation method Methods 0.000 claims description 37
- 125000005843 halogen group Chemical group 0.000 claims description 26
- -1 C 1 -C 4 alkyl Chemical group 0.000 claims description 22
- 125000000217 alkyl group Chemical group 0.000 claims description 22
- 125000004765 (C1-C4) haloalkyl group Chemical group 0.000 claims description 20
- 125000001424 substituent group Chemical group 0.000 claims description 20
- 125000004767 (C1-C4) haloalkoxy group Chemical group 0.000 claims description 19
- 125000003545 alkoxy group Chemical group 0.000 claims description 19
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical group CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 claims description 14
- 125000003342 alkenyl group Chemical group 0.000 claims description 12
- 125000000304 alkynyl group Chemical group 0.000 claims description 12
- 125000003118 aryl group Chemical group 0.000 claims description 12
- 125000000753 cycloalkyl group Chemical group 0.000 claims description 12
- 239000002904 solvent Substances 0.000 claims description 12
- 150000003983 crown ethers Chemical class 0.000 claims description 9
- 235000003270 potassium fluoride Nutrition 0.000 claims description 7
- 239000011698 potassium fluoride Substances 0.000 claims description 7
- 239000003054 catalyst Substances 0.000 claims description 6
- 229910001512 metal fluoride Inorganic materials 0.000 claims description 6
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 claims description 5
- XJHCXCQVJFPJIK-UHFFFAOYSA-M caesium fluoride Chemical compound [F-].[Cs+] XJHCXCQVJFPJIK-UHFFFAOYSA-M 0.000 claims description 4
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims description 3
- 125000003107 substituted aryl group Chemical group 0.000 claims description 3
- 150000003990 18-crown-6 derivatives Chemical group 0.000 claims description 2
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 2
- 125000001153 fluoro group Chemical group F* 0.000 claims description 2
- 229910052736 halogen Inorganic materials 0.000 claims description 2
- 150000002367 halogens Chemical group 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 229920000570 polyether Polymers 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 235000013024 sodium fluoride Nutrition 0.000 claims description 2
- 239000011775 sodium fluoride Substances 0.000 claims description 2
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 claims description 2
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical group CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims 3
- 125000005270 trialkylamine group Chemical group 0.000 claims 2
- 0 C*c1cccc(C(F)=O)n1 Chemical compound C*c1cccc(C(F)=O)n1 0.000 description 1
- QERMRZQVBGYSFJ-UHFFFAOYSA-N O=C(c(cc1F)nc(F)c1F)F Chemical compound O=C(c(cc1F)nc(F)c1F)F QERMRZQVBGYSFJ-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261675229P | 2012-07-24 | 2012-07-24 | |
| US61/675,229 | 2012-07-24 | ||
| PCT/US2013/051629 WO2014018506A1 (en) | 2012-07-24 | 2013-07-23 | Fluoropicolinoyl fluorides and processes for their preparation |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015524806A JP2015524806A (ja) | 2015-08-27 |
| JP2015524806A5 true JP2015524806A5 (enExample) | 2016-09-08 |
| JP6062050B2 JP6062050B2 (ja) | 2017-01-18 |
Family
ID=48998691
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015524381A Active JP6062050B2 (ja) | 2012-07-24 | 2013-07-23 | フルオロピコリノイルフルオライドおよびそれらの調製方法 |
Country Status (21)
| Country | Link |
|---|---|
| US (2) | US9045427B2 (enExample) |
| EP (1) | EP2877452B1 (enExample) |
| JP (1) | JP6062050B2 (enExample) |
| KR (1) | KR101946680B1 (enExample) |
| CN (1) | CN104583183B (enExample) |
| AR (1) | AR092355A1 (enExample) |
| AU (1) | AU2013293204B2 (enExample) |
| BR (1) | BR112015001445B8 (enExample) |
| CA (1) | CA2879518C (enExample) |
| CO (1) | CO7200264A2 (enExample) |
| ES (1) | ES2641724T3 (enExample) |
| IL (1) | IL236817B (enExample) |
| IN (1) | IN2015DN01482A (enExample) |
| MX (1) | MX351309B (enExample) |
| NZ (1) | NZ704104A (enExample) |
| PL (1) | PL2877452T3 (enExample) |
| RU (1) | RU2627659C2 (enExample) |
| TW (1) | TWI586650B (enExample) |
| UY (1) | UY34945A (enExample) |
| WO (1) | WO2014018506A1 (enExample) |
| ZA (1) | ZA201500601B (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW201609651A (zh) | 2013-11-12 | 2016-03-16 | 陶氏農業科學公司 | 用於氟化化合物之過程（一） |
| BR102014028162A2 (pt) | 2013-11-12 | 2015-09-08 | Dow Agrosciences Llc | processo para fluoração de compostos |
| BR102014028164A2 (pt) * | 2013-11-12 | 2015-09-08 | Dow Agrosciences Llc | processo para fluoração de compostos |
| TWI726900B (zh) | 2015-08-04 | 2021-05-11 | 美商陶氏農業科學公司 | 用於氟化化合物之過程 |
| CN113233974A (zh) * | 2021-04-09 | 2021-08-10 | 山东领海生物科技有限公司 | 一种酰基氟化物的合成方法 |
| KR102817626B1 (ko) * | 2023-06-21 | 2025-06-10 | (주)후성 | 트리플루오로아세틸 플루오라이드의 액상 제조방법 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE385883B (sv) * | 1972-04-10 | 1976-07-26 | Ciba Geigy Ag | Forfarande for framstellning av nya pyridinkarbonsyraestrar |
| JPS62181257A (ja) * | 1986-02-04 | 1987-08-08 | Asahi Glass Co Ltd | フルオロピリジン類の製造法 |
| JP2520254B2 (ja) * | 1987-04-28 | 1996-07-31 | イハラケミカル工業株式会社 | ３，４，５−トリフルオロ安息香酸誘導体およびその製造方法 |
| US4847442A (en) * | 1988-07-18 | 1989-07-11 | Allied-Signal Inc. | Process for the preparation of difluorobenzenes |
| US6297197B1 (en) | 2000-01-14 | 2001-10-02 | Dow Agrosciences Llc | 4-aminopicolinates and their use as herbicides |
| DK1498413T3 (da) * | 2000-01-14 | 2011-12-05 | Dow Agrosciences Llc | 4-aminopicolinater og deres anvendelse som herbicider |
| JP4608140B2 (ja) * | 2000-07-05 | 2011-01-05 | 石原産業株式会社 | ベンゾイルピリジン誘導体またはその塩、それらを有効成分として含有する殺菌剤、それらの製造方法ならびにそれらを製造するための中間体 |
| AR037228A1 (es) | 2001-07-30 | 2004-11-03 | Dow Agrosciences Llc | Compuestos del acido 6-(aril o heteroaril)-4-aminopicolinico, composicion herbicida que los comprende y metodo para controlar vegetacion no deseada |
| JP2003321406A (ja) * | 2002-04-30 | 2003-11-11 | Mitsubishi Gas Chem Co Inc | 高純度フルオロアルキルベンゼン誘導体及びその製造法 |
| UA82358C2 (uk) | 2003-04-02 | 2008-04-10 | Дау Агросайенсиз Ллс | 6-алкіл або алкеніл-4-амінопіколінати гербіцидна композиція, спосіб боротьби з небажаною рослинністю |
| EP2338335A1 (en) * | 2003-10-31 | 2011-06-29 | Ishihara Sangyo Kaisha, Ltd. | Preparation of fungicidal benzoylpyridine derivatives |
| KR101350071B1 (ko) | 2006-01-13 | 2014-01-14 | 다우 아그로사이언시즈 엘엘씨 | 6-(다-치환 아릴)-4-아미노피콜리네이트 및 그의제초제로서의 용도 |
| TWI529163B (zh) | 2011-01-25 | 2016-04-11 | 陶氏農業科學公司 | 用於製備４－胺基－５－氟－３－鹵素－６－（經取代之）吡啶甲酸酯的方法 |
| TWI537252B (zh) | 2011-01-25 | 2016-06-11 | 陶氏農業科學公司 | 用於製備４－胺基－５－氟－３－鹵素－６－（經取代之）吡啶甲酸酯的方法（一） |
| AR091856A1 (es) * | 2012-07-24 | 2015-03-04 | Dow Agrosciences Llc | Proceso para la preparacion de 4-amino-5-fluor-3-halo-6-(substituido) picolinatos |
-
2013
- 2013-07-22 AR ARP130102596A patent/AR092355A1/es active IP Right Grant
- 2013-07-23 KR KR1020157004098A patent/KR101946680B1/ko active Active
- 2013-07-23 CA CA2879518A patent/CA2879518C/en active Active
- 2013-07-23 IN IN1482DEN2015 patent/IN2015DN01482A/en unknown
- 2013-07-23 AU AU2013293204A patent/AU2013293204B2/en active Active
- 2013-07-23 US US13/949,053 patent/US9045427B2/en active Active
- 2013-07-23 NZ NZ704104A patent/NZ704104A/en unknown
- 2013-07-23 EP EP13750414.8A patent/EP2877452B1/en active Active
- 2013-07-23 ES ES13750414.8T patent/ES2641724T3/es active Active
- 2013-07-23 CN CN201380042976.9A patent/CN104583183B/zh active Active
- 2013-07-23 RU RU2015106018A patent/RU2627659C2/ru active
- 2013-07-23 JP JP2015524381A patent/JP6062050B2/ja active Active
- 2013-07-23 BR BR112015001445A patent/BR112015001445B8/pt active IP Right Grant
- 2013-07-23 PL PL13750414T patent/PL2877452T3/pl unknown
- 2013-07-23 WO PCT/US2013/051629 patent/WO2014018506A1/en not_active Ceased
- 2013-07-23 MX MX2015001138A patent/MX351309B/es active IP Right Grant
- 2013-07-23 UY UY0001034945A patent/UY34945A/es active IP Right Grant
- 2013-07-23 TW TW102126267A patent/TWI586650B/zh active
-
2015
- 2015-01-20 IL IL236817A patent/IL236817B/en active IP Right Grant
- 2015-01-27 ZA ZA2015/00601A patent/ZA201500601B/en unknown
- 2015-02-05 CO CO15023712A patent/CO7200264A2/es unknown
- 2015-03-24 US US14/667,109 patent/US9376388B2/en active Active