JP2013542309A5 - - Google Patents
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- JP2013542309A5 JP2013542309A5 JP2013538854A JP2013538854A JP2013542309A5 JP 2013542309 A5 JP2013542309 A5 JP 2013542309A5 JP 2013538854 A JP2013538854 A JP 2013538854A JP 2013538854 A JP2013538854 A JP 2013538854A JP 2013542309 A5 JP2013542309 A5 JP 2013542309A5
- Authority
- JP
- Japan
- Prior art keywords
- dispersion
- hydrocarbon
- fluoropolymer
- fluoromonomer
- added
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000034 method Methods 0.000 claims description 33
- 239000004215 Carbon black (E152) Substances 0.000 claims description 20
- 229930195733 hydrocarbon Natural products 0.000 claims description 20
- 150000002430 hydrocarbons Chemical class 0.000 claims description 18
- 239000006185 dispersion Substances 0.000 claims description 13
- 229920002313 fluoropolymer Polymers 0.000 claims description 12
- 239000004811 fluoropolymer Substances 0.000 claims description 12
- 150000001875 compounds Chemical class 0.000 claims description 11
- 239000004094 surface-active agent Substances 0.000 claims description 11
- 238000006116 polymerization reaction Methods 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 239000012736 aqueous medium Substances 0.000 claims description 7
- 239000003505 polymerization initiator Substances 0.000 claims description 7
- 230000006911 nucleation Effects 0.000 claims description 5
- 238000010899 nucleation Methods 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 4
- 230000000379 polymerizing effect Effects 0.000 claims description 4
- 238000000354 decomposition reaction Methods 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 238000002955 isolation Methods 0.000 claims description 2
- 239000002609 medium Substances 0.000 claims description 2
- 239000000178 monomer Substances 0.000 description 5
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 5
- -1 perfluoro Chemical group 0.000 description 4
- 230000006641 stabilisation Effects 0.000 description 4
- 238000011105 stabilization Methods 0.000 description 4
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 3
- YSYRISKCBOPJRG-UHFFFAOYSA-N 4,5-difluoro-2,2-bis(trifluoromethyl)-1,3-dioxole Chemical compound FC1=C(F)OC(C(F)(F)F)(C(F)(F)F)O1 YSYRISKCBOPJRG-UHFFFAOYSA-N 0.000 description 2
- UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 description 2
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 description 2
- 229910017053 inorganic salt Inorganic materials 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- MIZLGWKEZAPEFJ-UHFFFAOYSA-N 1,1,2-trifluoroethene Chemical group FC=C(F)F MIZLGWKEZAPEFJ-UHFFFAOYSA-N 0.000 description 1
- JMGNVALALWCTLC-UHFFFAOYSA-N 1-fluoro-2-(2-fluoroethenoxy)ethene Chemical compound FC=COC=CF JMGNVALALWCTLC-UHFFFAOYSA-N 0.000 description 1
- RFJVDJWCXSPUBY-UHFFFAOYSA-N 2-(difluoromethylidene)-4,4,5-trifluoro-5-(trifluoromethyl)-1,3-dioxolane Chemical compound FC(F)=C1OC(F)(F)C(F)(C(F)(F)F)O1 RFJVDJWCXSPUBY-UHFFFAOYSA-N 0.000 description 1
- QMIWYOZFFSLIAK-UHFFFAOYSA-N 3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene Chemical group FC(F)(F)C(=C)C(F)(F)F QMIWYOZFFSLIAK-UHFFFAOYSA-N 0.000 description 1
- ZXABMDQSAABDMG-UHFFFAOYSA-N 3-ethenoxyprop-1-ene Chemical compound C=CCOC=C ZXABMDQSAABDMG-UHFFFAOYSA-N 0.000 description 1
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 1
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 125000001183 hydrocarbyl group Chemical group 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US41161610P | 2010-11-09 | 2010-11-09 | |
| US61/411,616 | 2010-11-09 | ||
| US201161498791P | 2011-06-20 | 2011-06-20 | |
| US61/498,791 | 2011-06-20 | ||
| PCT/US2011/059978 WO2012064846A1 (en) | 2010-11-09 | 2011-11-09 | Nucleation in aqueous polymerization of fluoromonomer |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013542309A JP2013542309A (ja) | 2013-11-21 |
| JP2013542309A5 true JP2013542309A5 (https=) | 2014-12-25 |
| JP6201236B2 JP6201236B2 (ja) | 2017-09-27 |
Family
ID=45034188
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013538854A Active JP6201236B2 (ja) | 2010-11-09 | 2011-11-09 | フルオロモノマーの水性重合における核形成 |
Country Status (5)
| Country | Link |
|---|---|
| US (2) | US8563670B2 (https=) |
| EP (2) | EP3533811B1 (https=) |
| JP (1) | JP6201236B2 (https=) |
| CN (2) | CN106674392B (https=) |
| WO (1) | WO2012064846A1 (https=) |
Families Citing this family (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012064858A1 (en) * | 2010-11-09 | 2012-05-18 | E. I. Du Pont De Nemours And Company | Reducing the telogenic behavior of hydrocarbon-containing surfactants in aqueous dispersion fluoromonomer polymerization |
| JP6109073B2 (ja) | 2010-11-09 | 2017-04-05 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ | 炭化水素界面活性剤を用いたフルオロモノマーの水性重合 |
| DE102012021494A1 (de) * | 2012-11-02 | 2014-05-08 | Volkswagen Aktiengesellschaft | Schichtstruktur auf Silikonbasis mit oleophob-hydrophober Oberfläche sowie elektrische Maschine mit einer solchen |
| JP6622209B2 (ja) * | 2013-11-26 | 2019-12-18 | ザ ケマーズ カンパニー エフシー リミテッド ライアビリティ カンパニー | フルオロモノマーの水性重合において核を形成するためのポリアルキレンオキシドの使用 |
| KR101930385B1 (ko) * | 2014-11-05 | 2018-12-18 | 씨에이엠 홀딩 코포레이션 | 은 나노와이어-기반 투명 전도성 필름을 형성하기 위한 아이오다이드 첨가제를 갖는 단쇄 플루오로계면활성제 |
| RU2766151C2 (ru) | 2017-08-10 | 2022-02-08 | Дайкин Индастриз, Лтд. | Способ производства водной жидкой дисперсии очищенного политетрафторэтилена, способ производства модифицированного порошкообразного политетрафторэтилена, способ производства формованного тела из политетрафторэтилена и композиция |
| CN110997735B (zh) | 2017-08-10 | 2024-03-01 | 大金工业株式会社 | 精制聚四氟乙烯水性分散液的制造方法、改性聚四氟乙烯粉末的制造方法、聚四氟乙烯成型体的制造方法以及组合物 |
| WO2019131633A1 (ja) | 2017-12-25 | 2019-07-04 | ダイキン工業株式会社 | ポリテトラフルオロエチレン粉末の製造方法 |
| WO2019172382A1 (ja) | 2018-03-07 | 2019-09-12 | ダイキン工業株式会社 | フルオロポリマーの製造方法 |
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| EP3862368A4 (en) | 2018-10-03 | 2022-06-29 | Daikin Industries, Ltd. | Polytetrafluoroethylene production method |
| CN112771006A (zh) | 2018-10-03 | 2021-05-07 | 大金工业株式会社 | 从排水除去含氟化合物的方法 |
| JP7277799B2 (ja) | 2018-10-03 | 2023-05-19 | ダイキン工業株式会社 | ポリテトラフルオロエチレンの製造方法 |
| EP3880719A4 (en) | 2018-11-12 | 2022-08-10 | Arkema, Inc. | PROCESS FOR PREPARING A FLUOROPOLYMER DISPERSION |
| US20220119561A1 (en) | 2019-02-01 | 2022-04-21 | Daikin Industries, Ltd. | Method for producing polytetrafluoroethylene |
| JP7104354B2 (ja) | 2019-02-07 | 2022-07-21 | ダイキン工業株式会社 | 組成物、延伸体及びその製造方法 |
| JP7236004B2 (ja) | 2019-04-26 | 2023-03-09 | ダイキン工業株式会社 | フルオロポリマー水性分散液の製造方法及びフルオロポリマー水性分散液 |
| JP7564452B2 (ja) | 2019-04-26 | 2024-10-09 | ダイキン工業株式会社 | フルオロポリマー水性分散液の製造方法 |
| US20220267483A1 (en) | 2019-07-16 | 2022-08-25 | Daikin Industries, Ltd. | Method for producing fluorine-containing elastomer, and composition |
| CN118146427A (zh) | 2019-07-23 | 2024-06-07 | 大金工业株式会社 | 含氟聚合物的制造方法、聚四氟乙烯组合物和聚四氟乙烯粉末 |
| WO2021066189A1 (ja) | 2019-10-03 | 2021-04-08 | ダイキン工業株式会社 | ポリテトラフルオロエチレンおよびその製造方法 |
| EP4053181A4 (en) * | 2019-10-29 | 2024-03-06 | Agc Inc. | METHOD FOR PRODUCING AN AQUEOUS POLYTETRAFLUORETHYLENE DISPERSION |
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| CN116234794A (zh) | 2020-10-01 | 2023-06-06 | 科慕埃弗西有限公司 | 含氟聚合物的水性聚合反应中的低反应性烃分散剂 |
| CN112409528B (zh) * | 2020-10-21 | 2021-11-16 | 浙江巨化技术中心有限公司 | 一种核壳结构ptfe分散树脂的制备方法 |
| CN117015557A (zh) | 2021-03-18 | 2023-11-07 | 大金工业株式会社 | 氟树脂的制造方法、氟树脂和水性分散液 |
| JP7323832B2 (ja) | 2021-03-31 | 2023-08-09 | ダイキン工業株式会社 | フッ素樹脂組成物、及び、成形体 |
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| KR20230160917A (ko) | 2021-03-31 | 2023-11-24 | 다이킨 고교 가부시키가이샤 | 불소 수지 조성물의 제조 방법, 불소 수지 조성물 및 성형체 |
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| CN116144008A (zh) * | 2021-11-23 | 2023-05-23 | 中昊晨光化工研究院有限公司 | 一种稳定剂及其在制备含氟聚合物中的应用 |
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| WO2023247225A1 (en) * | 2022-06-23 | 2023-12-28 | Solvay Specialty Polymers Italy S.P.A. | Process for manufacturing aqueous dispersion comprising particles of a fluorinated polymer (f) |
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| US20260098161A1 (en) * | 2022-09-30 | 2026-04-09 | Arkema Inc. | Large particle size functionalized fluoropolymer latex preparation |
| EP4525095A4 (en) | 2023-01-18 | 2026-04-08 | Daikin Ind Ltd | Tetrafluoroethylene polymer composition, binder for semiconductor secondary batteries, electrolyte layer mixture, electrode mixture, electrode and semiconductor secondary battery |
| EP4481860A4 (en) | 2023-01-18 | 2025-07-23 | Daikin Ind Ltd | MIXTURE FOR ELECTROCHEMICAL DEVICE, MIXTURE SHEET FOR ELECTROCHEMICAL DEVICE, ELECTRODE, AND ELECTROCHEMICAL DEVICE |
| JP7560797B2 (ja) | 2023-01-18 | 2024-10-03 | ダイキン工業株式会社 | 電気化学デバイス用合剤自立膜、電極、及び、電気化学デバイス |
| CN120530158A (zh) | 2023-01-18 | 2025-08-22 | 大金工业株式会社 | 聚四氟乙烯组合物 |
| EP4471908A4 (en) | 2023-01-18 | 2025-10-01 | Daikin Ind Ltd | TETRAFLUOROETHYLENE-BASED POLYMER COMPOSITION, BINDER FOR ELECTROCHEMICAL DEVICE, MIXTURE FOR ELECTRODE, ELECTRODE, AND SECONDARY BATTERY |
| JP7741457B2 (ja) | 2024-01-18 | 2025-09-18 | ダイキン工業株式会社 | テトラフルオロエチレン系ポリマー組成物、電気化学デバイス用バインダー、電極合剤、電極、及び、二次電池 |
| JP7719418B1 (ja) | 2024-01-18 | 2025-08-06 | ダイキン工業株式会社 | 組成物、電気化学デバイス用バインダー、電極合剤、電極、及び、二次電池 |
| EP4645423A1 (en) | 2024-01-18 | 2025-11-05 | Daikin Industries, Ltd. | Electrochemical device, composition, electrode mixture, electrode, and secondary battery |
| CN118562034B (zh) * | 2024-08-05 | 2024-10-18 | 黄山熠能科技有限公司 | 一种氟乙烯聚合方法 |
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| WO2007046377A1 (ja) | 2005-10-20 | 2007-04-26 | Asahi Glass Company, Limited | 溶融成形可能なフッ素樹脂の製造方法 |
| JP5141256B2 (ja) | 2005-10-20 | 2013-02-13 | 旭硝子株式会社 | ポリテトラフルオロエチレン水性分散液およびその製品 |
| EP1942118B1 (en) | 2005-10-26 | 2013-09-11 | Asahi Glass Company, Limited | Fluororesin with low fluorine-containing emulsifier residual and method for producing same |
| EP1948706B1 (en) | 2005-11-18 | 2012-09-19 | E.I. Du Pont De Nemours And Company | Core/shell polymer |
| US20070282044A1 (en) | 2006-05-31 | 2007-12-06 | Robert John Cavanaugh | Concentrated fluoropolymer dispersions stabilized with anionic polyelectrolyte dispersing agents |
| WO2008019155A1 (en) | 2006-08-11 | 2008-02-14 | The University Of North Carolina At Chapel Hill | Process of fluoromonomer polymerization |
| WO2008060462A1 (en) | 2006-11-09 | 2008-05-22 | E. I. Du Pont De Nemours And Company | Aqueous polymerization of fluorinated monomers using polymerization agent comprising fluoropolyether acid or salt and siloxane surfactant |
| EP2079766B1 (en) | 2006-11-09 | 2011-05-18 | E.I. Du Pont De Nemours And Company | Aqueous polymerization of fluorinated monomer using polymerization agent comprising high molecular weight fluoropolyether acid or salt and fluoropolyether acid or salt surfactant |
| JP5439186B2 (ja) * | 2006-11-09 | 2014-03-12 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | フルオロポリエーテル酸または塩および炭化水素系界面活性剤を含む重合剤を用いるフッ素化モノマーの水性重合 |
| US7521513B2 (en) * | 2006-11-29 | 2009-04-21 | Dupont Performance Elastomers Llc | Semi-batch process for producing fluoroelastomers |
| US20080262177A1 (en) | 2006-12-19 | 2008-10-23 | Lyons Donald F | Process for producing fluoroelastomers |
| US20080146757A1 (en) | 2006-12-19 | 2008-06-19 | Lyons Donald F | Process for producing fluoroelastomers |
| WO2009013214A1 (en) | 2007-07-20 | 2009-01-29 | Solvay Solexis S.P.A. | Process for polymer dispersions |
| EP2274345B1 (en) | 2008-04-07 | 2017-01-04 | Arkema Inc. | Polymerization of fluoropolymers using polycaprolactone |
| US8153738B2 (en) | 2008-12-23 | 2012-04-10 | E I Du Pont De Nemours And Company | Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer |
| EP2284200A1 (en) * | 2009-07-31 | 2011-02-16 | 3M Innovative Properties Company | Aqueous fluoropolymer dispersions containing a polyol comprising at least one long chain residue and method for producing them |
| WO2011024857A1 (ja) | 2009-08-28 | 2011-03-03 | ダイキン工業株式会社 | 含フッ素重合体の製造方法 |
| WO2011024856A1 (ja) | 2009-08-28 | 2011-03-03 | ダイキン工業株式会社 | 含フッ素重合体の製造方法 |
| WO2012064858A1 (en) * | 2010-11-09 | 2012-05-18 | E. I. Du Pont De Nemours And Company | Reducing the telogenic behavior of hydrocarbon-containing surfactants in aqueous dispersion fluoromonomer polymerization |
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2011
- 2011-11-09 EP EP19168595.7A patent/EP3533811B1/en active Active
- 2011-11-09 US US13/292,344 patent/US8563670B2/en active Active
- 2011-11-09 WO PCT/US2011/059978 patent/WO2012064846A1/en not_active Ceased
- 2011-11-09 JP JP2013538854A patent/JP6201236B2/ja active Active
- 2011-11-09 EP EP11787984.1A patent/EP2638082B1/en active Active
- 2011-11-09 CN CN201710049835.XA patent/CN106674392B/zh active Active
- 2011-11-09 CN CN201180053785.3A patent/CN103201301B/zh active Active
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2013
- 2013-09-19 US US14/031,335 patent/US9371405B2/en active Active
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