JP2013542309A5 - - Google Patents
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- JP2013542309A5 JP2013542309A5 JP2013538854A JP2013538854A JP2013542309A5 JP 2013542309 A5 JP2013542309 A5 JP 2013542309A5 JP 2013538854 A JP2013538854 A JP 2013538854A JP 2013538854 A JP2013538854 A JP 2013538854A JP 2013542309 A5 JP2013542309 A5 JP 2013542309A5
- Authority
- JP
- Japan
- Prior art keywords
- dispersion
- hydrocarbon
- fluoropolymer
- fluoromonomer
- added
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000034 method Methods 0.000 claims description 33
- 239000004215 Carbon black (E152) Substances 0.000 claims description 20
- 229930195733 hydrocarbon Natural products 0.000 claims description 20
- 150000002430 hydrocarbons Chemical class 0.000 claims description 18
- 239000006185 dispersion Substances 0.000 claims description 13
- 229920002313 fluoropolymer Polymers 0.000 claims description 12
- 239000004811 fluoropolymer Substances 0.000 claims description 12
- 150000001875 compounds Chemical class 0.000 claims description 11
- 239000004094 surface-active agent Substances 0.000 claims description 11
- 238000006116 polymerization reaction Methods 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 239000012736 aqueous medium Substances 0.000 claims description 7
- 239000003505 polymerization initiator Substances 0.000 claims description 7
- 230000006911 nucleation Effects 0.000 claims description 5
- 238000010899 nucleation Methods 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 4
- 230000000379 polymerizing effect Effects 0.000 claims description 4
- 238000000354 decomposition reaction Methods 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 238000002955 isolation Methods 0.000 claims description 2
- 239000002609 medium Substances 0.000 claims description 2
- 239000000178 monomer Substances 0.000 description 5
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 5
- -1 perfluoro Chemical group 0.000 description 4
- 230000006641 stabilisation Effects 0.000 description 4
- 238000011105 stabilization Methods 0.000 description 4
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 3
- YSYRISKCBOPJRG-UHFFFAOYSA-N 4,5-difluoro-2,2-bis(trifluoromethyl)-1,3-dioxole Chemical compound FC1=C(F)OC(C(F)(F)F)(C(F)(F)F)O1 YSYRISKCBOPJRG-UHFFFAOYSA-N 0.000 description 2
- UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 description 2
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 description 2
- 229910017053 inorganic salt Inorganic materials 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- MIZLGWKEZAPEFJ-UHFFFAOYSA-N 1,1,2-trifluoroethene Chemical group FC=C(F)F MIZLGWKEZAPEFJ-UHFFFAOYSA-N 0.000 description 1
- JMGNVALALWCTLC-UHFFFAOYSA-N 1-fluoro-2-(2-fluoroethenoxy)ethene Chemical compound FC=COC=CF JMGNVALALWCTLC-UHFFFAOYSA-N 0.000 description 1
- RFJVDJWCXSPUBY-UHFFFAOYSA-N 2-(difluoromethylidene)-4,4,5-trifluoro-5-(trifluoromethyl)-1,3-dioxolane Chemical compound FC(F)=C1OC(F)(F)C(F)(C(F)(F)F)O1 RFJVDJWCXSPUBY-UHFFFAOYSA-N 0.000 description 1
- QMIWYOZFFSLIAK-UHFFFAOYSA-N 3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene Chemical group FC(F)(F)C(=C)C(F)(F)F QMIWYOZFFSLIAK-UHFFFAOYSA-N 0.000 description 1
- ZXABMDQSAABDMG-UHFFFAOYSA-N 3-ethenoxyprop-1-ene Chemical compound C=CCOC=C ZXABMDQSAABDMG-UHFFFAOYSA-N 0.000 description 1
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 1
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 125000001183 hydrocarbyl group Chemical group 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US41161610P | 2010-11-09 | 2010-11-09 | |
| US61/411,616 | 2010-11-09 | ||
| US201161498791P | 2011-06-20 | 2011-06-20 | |
| US61/498,791 | 2011-06-20 | ||
| PCT/US2011/059978 WO2012064846A1 (en) | 2010-11-09 | 2011-11-09 | Nucleation in aqueous polymerization of fluoromonomer |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013542309A JP2013542309A (ja) | 2013-11-21 |
| JP2013542309A5 true JP2013542309A5 (https=) | 2014-12-25 |
| JP6201236B2 JP6201236B2 (ja) | 2017-09-27 |
Family
ID=45034188
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013538854A Active JP6201236B2 (ja) | 2010-11-09 | 2011-11-09 | フルオロモノマーの水性重合における核形成 |
Country Status (5)
| Country | Link |
|---|---|
| US (2) | US8563670B2 (https=) |
| EP (2) | EP2638082B1 (https=) |
| JP (1) | JP6201236B2 (https=) |
| CN (2) | CN106674392B (https=) |
| WO (1) | WO2012064846A1 (https=) |
Families Citing this family (45)
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| CN103210003B (zh) * | 2010-11-09 | 2016-09-07 | 纳幕尔杜邦公司 | 减弱含烃表面活性剂在含氟单体含水分散体聚合反应中的调聚性能 |
| CN103201300B (zh) | 2010-11-09 | 2016-11-09 | 纳幕尔杜邦公司 | 使用烃表面活性剂的含氟单体的含水聚合 |
| DE102012021494A1 (de) * | 2012-11-02 | 2014-05-08 | Volkswagen Aktiengesellschaft | Schichtstruktur auf Silikonbasis mit oleophob-hydrophober Oberfläche sowie elektrische Maschine mit einer solchen |
| US9676929B2 (en) * | 2013-11-26 | 2017-06-13 | The Chemours Company Fc, Llc | Employing polyalkylene oxides for nucleation in aqueous polymerization of fluoromonomer |
| US10040956B2 (en) * | 2014-11-05 | 2018-08-07 | Cam Holding Corporation | Short-chain fluorosurfactants with iodide additives for forming silver nanowire-based transparent conductive films |
| SG11202000862YA (en) | 2017-08-10 | 2020-02-27 | Daikin Ind Ltd | Method for producing purified polytetrafluoroethylene aqueous dispersion liquid, method for producing modified polytetrafluoroethylene powder, method for producing polytetrafluoroethylene molded body, and composition |
| WO2019031617A1 (ja) | 2017-08-10 | 2019-02-14 | ダイキン工業株式会社 | 精製ポリテトラフルオロエチレン水性分散液の製造方法、改質ポリテトラフルオロエチレン粉末の製造方法、ポリテトラフルオロエチレン成形体の製造方法、及び、組成物 |
| JP7014976B2 (ja) | 2017-12-25 | 2022-02-15 | ダイキン工業株式会社 | ポリテトラフルオロエチレン粉末の製造方法 |
| US12583947B2 (en) | 2018-03-07 | 2026-03-24 | Daikin Industries, Ltd. | Method for producing fluoropolymer |
| JP7410045B2 (ja) * | 2018-03-16 | 2024-01-09 | アーケマ・インコーポレイテッド | 高固形分、無界面活性剤フルオロポリマー |
| WO2020022355A1 (ja) | 2018-07-23 | 2020-01-30 | ダイキン工業株式会社 | ポリテトラフルオロエチレン及び延伸体 |
| JP7277799B2 (ja) | 2018-10-03 | 2023-05-19 | ダイキン工業株式会社 | ポリテトラフルオロエチレンの製造方法 |
| CN112771006A (zh) | 2018-10-03 | 2021-05-07 | 大金工业株式会社 | 从排水除去含氟化合物的方法 |
| CN112739728B (zh) | 2018-10-03 | 2023-03-10 | 大金工业株式会社 | 聚四氟乙烯的制造方法 |
| KR102913501B1 (ko) * | 2018-11-12 | 2026-01-16 | 알케마 인코포레이티드 | 플루오로 중합체 분산액의 제조방법 |
| CN113366034B (zh) | 2019-02-01 | 2022-11-11 | 大金工业株式会社 | 聚四氟乙烯的制造方法 |
| EP3922435A4 (en) | 2019-02-07 | 2022-11-02 | Daikin Industries, Ltd. | Composition, stretched body and method of manufacturing thereof |
| WO2020218618A1 (ja) | 2019-04-26 | 2020-10-29 | ダイキン工業株式会社 | フルオロポリマー水性分散液の製造方法 |
| JP7236004B2 (ja) | 2019-04-26 | 2023-03-09 | ダイキン工業株式会社 | フルオロポリマー水性分散液の製造方法及びフルオロポリマー水性分散液 |
| CN114096573A (zh) | 2019-07-16 | 2022-02-25 | 大金工业株式会社 | 含氟弹性体的制造方法和组合物 |
| EP4006063A4 (en) | 2019-07-23 | 2023-10-25 | Daikin Industries, Ltd. | METHOD FOR PRODUCING A FLUROPOLYMER, POLYTETRAFLUORETHYLENE COMPOSITION AND POLYTETRAFLUORETHYLENE POWDER |
| EP4039716A4 (en) | 2019-10-03 | 2023-10-25 | Daikin Industries, Ltd. | Polytetrafluoroethylene and method for producing same |
| JP7586090B2 (ja) * | 2019-10-29 | 2024-11-19 | Ａｇｃ株式会社 | ポリテトラフルオロエチレン水性分散液の製造方法 |
| JP6989792B2 (ja) | 2019-12-25 | 2022-01-12 | ダイキン工業株式会社 | フルオロポリマーの製造方法 |
| WO2022072693A1 (en) | 2020-10-01 | 2022-04-07 | The Chemours Company Fc, Llc | Low reactivity hydrocarbon dispersing agents in the aqueous polymerization of fluoropolymers |
| CN112409528B (zh) * | 2020-10-21 | 2021-11-16 | 浙江巨化技术中心有限公司 | 一种核壳结构ptfe分散树脂的制备方法 |
| WO2022196804A1 (ja) | 2021-03-18 | 2022-09-22 | ダイキン工業株式会社 | フッ素樹脂の製造方法、フッ素樹脂および水性分散液 |
| JP7323833B2 (ja) | 2021-03-31 | 2023-08-09 | ダイキン工業株式会社 | フッ素樹脂組成物の製造方法、フッ素樹脂組成物、及び、成形体 |
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| TW202530278A (zh) | 2021-03-31 | 2025-08-01 | 日商大金工業股份有限公司 | 氟樹脂組成物、及成形體 |
| CN117043262A (zh) | 2021-03-31 | 2023-11-10 | 大金工业株式会社 | 氟树脂组合物和成型体 |
| CN116144008A (zh) * | 2021-11-23 | 2023-05-23 | 中昊晨光化工研究院有限公司 | 一种稳定剂及其在制备含氟聚合物中的应用 |
| WO2023191061A1 (ja) | 2022-03-31 | 2023-10-05 | ダイキン工業株式会社 | フッ素樹脂組成物、及び、成形体 |
| CN119421906A (zh) * | 2022-06-23 | 2025-02-11 | 索尔维特殊聚合物意大利有限公司 | 用于制造包含氟化聚合物(f)颗粒的水性分散体的方法 |
| JP2025534604A (ja) * | 2022-09-30 | 2025-10-17 | アーケマ・インコーポレイテッド | 大粒子径フッ素樹脂ラテックスの製造 |
| WO2024073017A2 (en) * | 2022-09-30 | 2024-04-04 | Arkema Inc. | Large particle size functionalized fluoropolymer latex preparation |
| WO2024154805A1 (ja) | 2023-01-18 | 2024-07-25 | ダイキン工業株式会社 | テトラフルオロエチレン系ポリマー組成物、固体二次電池用バインダー、電解質層用合剤、電極合剤、電極、及び、固体二次電池 |
| JP7583340B2 (ja) | 2023-01-18 | 2024-11-14 | ダイキン工業株式会社 | 電気化学デバイス用合剤、電気化学デバイス用合剤シート、電極、及び、電気化学デバイス |
| JP7538458B2 (ja) | 2023-01-18 | 2024-08-22 | ダイキン工業株式会社 | ポリテトラフルオロエチレン組成物 |
| KR102932815B1 (ko) | 2023-01-18 | 2026-03-05 | 다이킨 고교 가부시키가이샤 | 전기 화학 디바이스용 합제 자립막, 전극, 및 전기 화학 디바이스 |
| WO2024154803A1 (ja) | 2023-01-18 | 2024-07-25 | ダイキン工業株式会社 | テトラフルオロエチレン系ポリマー組成物、電気化学デバイス用バインダー、電極合剤、電極、及び、二次電池 |
| WO2025154806A1 (ja) | 2024-01-18 | 2025-07-24 | ダイキン工業株式会社 | 電気化学デバイス、組成物、電極合剤、電極、及び、二次電池 |
| JP7741457B2 (ja) | 2024-01-18 | 2025-09-18 | ダイキン工業株式会社 | テトラフルオロエチレン系ポリマー組成物、電気化学デバイス用バインダー、電極合剤、電極、及び、二次電池 |
| EP4657572A1 (en) | 2024-01-18 | 2025-12-03 | Daikin Industries, Ltd. | Composition, electrochemical device binder, electrode mixture, electrode, and secondary battery |
| CN118562034B (zh) * | 2024-08-05 | 2024-10-18 | 黄山熠能科技有限公司 | 一种氟乙烯聚合方法 |
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| WO2007049517A1 (ja) | 2005-10-26 | 2007-05-03 | Asahi Glass Company, Limited | 含フッ素乳化剤の残留量が少ないフッ素樹脂およびその製造方法 |
| WO2007061914A1 (en) | 2005-11-18 | 2007-05-31 | E.I. Du Pont De Nemours And Company | Core/shell polymer |
| US20070282044A1 (en) | 2006-05-31 | 2007-12-06 | Robert John Cavanaugh | Concentrated fluoropolymer dispersions stabilized with anionic polyelectrolyte dispersing agents |
| WO2008019155A1 (en) * | 2006-08-11 | 2008-02-14 | The University Of North Carolina At Chapel Hill | Process of fluoromonomer polymerization |
| EP2084195B1 (en) | 2006-11-09 | 2011-06-08 | E.I. Du Pont De Nemours And Company | Aqueous polymerization of fluorinated monomers using polymerization agent comprising fluoropolyether acid or salt and hydrocarbon surfactant |
| EP2087018B1 (en) | 2006-11-09 | 2011-05-25 | E.I. Du Pont De Nemours And Company | Aqueous polymerization of fluorinated monomers using polymerization agent comprising fluoropolyether acid or salt and siloxane surfactant |
| ATE510857T1 (de) | 2006-11-09 | 2011-06-15 | Du Pont | Wässrige polymerisation eines fluorinierten monomers mithilfe eines polymerisationsmittels mit einer fluorpolyethersäure oder einem salz daraus und einem kurzkettigen fluortensid |
| US7521513B2 (en) * | 2006-11-29 | 2009-04-21 | Dupont Performance Elastomers Llc | Semi-batch process for producing fluoroelastomers |
| US20080262177A1 (en) | 2006-12-19 | 2008-10-23 | Lyons Donald F | Process for producing fluoroelastomers |
| US20080146757A1 (en) | 2006-12-19 | 2008-06-19 | Lyons Donald F | Process for producing fluoroelastomers |
| WO2009013214A1 (en) | 2007-07-20 | 2009-01-29 | Solvay Solexis S.P.A. | Process for polymer dispersions |
| WO2009126504A2 (en) | 2008-04-07 | 2009-10-15 | Arkema Inc. | Polymerization of fluoropolymers using polycaprolactone |
| US8153738B2 (en) | 2008-12-23 | 2012-04-10 | E I Du Pont De Nemours And Company | Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer |
| EP2284200A1 (en) * | 2009-07-31 | 2011-02-16 | 3M Innovative Properties Company | Aqueous fluoropolymer dispersions containing a polyol comprising at least one long chain residue and method for producing them |
| CN102482363B (zh) | 2009-08-28 | 2014-01-01 | 大金工业株式会社 | 含氟聚合物的制造方法 |
| US8735492B2 (en) | 2009-08-28 | 2014-05-27 | Daikin Industries, Ltd. | Method for producing fluorine-containing polymer |
| CN103210003B (zh) * | 2010-11-09 | 2016-09-07 | 纳幕尔杜邦公司 | 减弱含烃表面活性剂在含氟单体含水分散体聚合反应中的调聚性能 |
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2011
- 2011-11-09 JP JP2013538854A patent/JP6201236B2/ja active Active
- 2011-11-09 EP EP11787984.1A patent/EP2638082B1/en active Active
- 2011-11-09 CN CN201710049835.XA patent/CN106674392B/zh active Active
- 2011-11-09 WO PCT/US2011/059978 patent/WO2012064846A1/en not_active Ceased
- 2011-11-09 EP EP19168595.7A patent/EP3533811B1/en active Active
- 2011-11-09 CN CN201180053785.3A patent/CN103201301B/zh active Active
- 2011-11-09 US US13/292,344 patent/US8563670B2/en active Active
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2013
- 2013-09-19 US US14/031,335 patent/US9371405B2/en active Active
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