JP2010509444A5 - - Google Patents
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- JP2010509444A5 JP2010509444A5 JP2009536316A JP2009536316A JP2010509444A5 JP 2010509444 A5 JP2010509444 A5 JP 2010509444A5 JP 2009536316 A JP2009536316 A JP 2009536316A JP 2009536316 A JP2009536316 A JP 2009536316A JP 2010509444 A5 JP2010509444 A5 JP 2010509444A5
- Authority
- JP
- Japan
- Prior art keywords
- salt
- acid
- polymerization medium
- weight
- fluoropolymer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000034 method Methods 0.000 claims description 32
- 239000002253 acid Substances 0.000 claims description 16
- 238000006116 polymerization reaction Methods 0.000 claims description 16
- 150000003839 salts Chemical class 0.000 claims description 15
- 229920002313 fluoropolymer Polymers 0.000 claims description 12
- 239000004811 fluoropolymer Substances 0.000 claims description 12
- 230000000379 polymerizing effect Effects 0.000 claims description 8
- 239000004215 Carbon black (E152) Substances 0.000 claims description 7
- 229930195733 hydrocarbon Natural products 0.000 claims description 7
- 150000002430 hydrocarbons Chemical class 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- 239000004094 surface-active agent Substances 0.000 claims description 7
- 239000000178 monomer Substances 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 3
- 125000001153 fluoro group Chemical group F* 0.000 claims description 2
- 239000003999 initiator Substances 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- 239000002609 medium Substances 0.000 description 11
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 2
- YSYRISKCBOPJRG-UHFFFAOYSA-N 4,5-difluoro-2,2-bis(trifluoromethyl)-1,3-dioxole Chemical compound FC1=C(F)OC(C(F)(F)F)(C(F)(F)F)O1 YSYRISKCBOPJRG-UHFFFAOYSA-N 0.000 description 2
- UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 239000010702 perfluoropolyether Substances 0.000 description 2
- MIZLGWKEZAPEFJ-UHFFFAOYSA-N 1,1,2-trifluoroethene Chemical group FC=C(F)F MIZLGWKEZAPEFJ-UHFFFAOYSA-N 0.000 description 1
- JMGNVALALWCTLC-UHFFFAOYSA-N 1-fluoro-2-(2-fluoroethenoxy)ethene Chemical compound FC=COC=CF JMGNVALALWCTLC-UHFFFAOYSA-N 0.000 description 1
- RFJVDJWCXSPUBY-UHFFFAOYSA-N 2-(difluoromethylidene)-4,4,5-trifluoro-5-(trifluoromethyl)-1,3-dioxolane Chemical compound FC(F)=C1OC(F)(F)C(F)(C(F)(F)F)O1 RFJVDJWCXSPUBY-UHFFFAOYSA-N 0.000 description 1
- QMIWYOZFFSLIAK-UHFFFAOYSA-N 3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene Chemical group FC(F)(F)C(=C)C(F)(F)F QMIWYOZFFSLIAK-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000012985 polymerization agent Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US85800806P | 2006-11-09 | 2006-11-09 | |
| US60/858,008 | 2006-11-09 | ||
| PCT/US2007/023642 WO2008060463A1 (en) | 2006-11-09 | 2007-11-09 | Aqueous polymerization of fluorinated monomers using polymerization agent comprising fluoropolyether acid or salt and hydrocarbon surfactant |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010509444A JP2010509444A (ja) | 2010-03-25 |
| JP2010509444A5 true JP2010509444A5 (https=) | 2010-12-24 |
| JP5439186B2 JP5439186B2 (ja) | 2014-03-12 |
Family
ID=39110524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009536316A Active JP5439186B2 (ja) | 2006-11-09 | 2007-11-09 | フルオロポリエーテル酸または塩および炭化水素系界面活性剤を含む重合剤を用いるフッ素化モノマーの水性重合 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US7897682B2 (https=) |
| EP (1) | EP2084195B1 (https=) |
| JP (1) | JP5439186B2 (https=) |
| CN (1) | CN101605826B (https=) |
| AT (1) | ATE512165T1 (https=) |
| WO (1) | WO2008060463A1 (https=) |
Families Citing this family (53)
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|---|---|---|---|---|
| US8080621B2 (en) * | 2005-06-10 | 2011-12-20 | Arkema Inc. | Aqueous process for making fluoropolymers |
| ATE510857T1 (de) * | 2006-11-09 | 2011-06-15 | Du Pont | Wässrige polymerisation eines fluorinierten monomers mithilfe eines polymerisationsmittels mit einer fluorpolyethersäure oder einem salz daraus und einem kurzkettigen fluortensid |
| US20090281241A1 (en) | 2008-05-09 | 2009-11-12 | E. I. Du Pont De Nemours And Company | Aqueous Polymerization of Fluorinated Monomer Using a Mixture of Fluoropolyether Acids or Salts |
| US20100113691A1 (en) * | 2008-11-06 | 2010-05-06 | E. I. Du Pont De Nemours And Company | Fluoro olefin polymerization |
| US8436053B2 (en) * | 2008-12-23 | 2013-05-07 | E.I. Du Pont De Nemours And Company | Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer |
| US8436054B2 (en) * | 2008-12-23 | 2013-05-07 | E I Du Pont De Nemours And Company | Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer produced in situ |
| US8153738B2 (en) | 2008-12-23 | 2012-04-10 | E I Du Pont De Nemours And Company | Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer |
| US8058376B2 (en) | 2008-12-23 | 2011-11-15 | E. I. Du Pont De Nemours And Company | Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated lonomer produced in situ |
| US8835547B2 (en) | 2008-12-23 | 2014-09-16 | E I Du Pont De Nemours And Company | Fluoropolymer particles having a nucleus of fluorinated ionomer |
| RU2522749C2 (ru) * | 2009-07-31 | 2014-07-20 | Зм Инновейтив Пропертиз Компани | Соединения фторполимера, содержащие многоатомные соединения, и способы из производства |
| CN102822213B (zh) * | 2009-12-18 | 2016-06-15 | 索尔维特殊聚合物意大利有限公司 | 制造偏二氟乙烯聚合物分散体的方法 |
| JP5684283B2 (ja) * | 2009-12-18 | 2015-03-11 | ソルヴェイ・スペシャルティ・ポリマーズ・イタリー・エッセ・ピ・ア | フルオロポリマーの製造方法 |
| CN103201300B (zh) | 2010-11-09 | 2016-11-09 | 纳幕尔杜邦公司 | 使用烃表面活性剂的含氟单体的含水聚合 |
| JP6201236B2 (ja) | 2010-11-09 | 2017-09-27 | ザ ケマーズ カンパニー エフシー リミテッド ライアビリティ カンパニー | フルオロモノマーの水性重合における核形成 |
| CN103210003B (zh) * | 2010-11-09 | 2016-09-07 | 纳幕尔杜邦公司 | 减弱含烃表面活性剂在含氟单体含水分散体聚合反应中的调聚性能 |
| JP5730093B2 (ja) * | 2011-03-28 | 2015-06-03 | 株式会社クレハ | フッ化ビニリデン系重合体の製造方法 |
| CN102585070B (zh) * | 2012-01-06 | 2015-12-09 | 石家庄市海森化工有限公司 | 三氟氯乙烯-乙烯共聚物的制备方法 |
| CN102627719B (zh) * | 2012-03-23 | 2014-05-07 | 上海三爱富新材料股份有限公司 | 一种高强度耐蠕变性的聚四氟乙烯制备方法 |
| US9676929B2 (en) | 2013-11-26 | 2017-06-13 | The Chemours Company Fc, Llc | Employing polyalkylene oxides for nucleation in aqueous polymerization of fluoromonomer |
| US10407588B2 (en) | 2015-03-13 | 2019-09-10 | Daikin Industries, Ltd. | Coating composition and coated article |
| CN108017746B (zh) * | 2016-10-28 | 2020-03-20 | 中昊晨光化工研究院有限公司 | 一种低压缩永久变形的过氧化物硫化氟橡胶及其制备方法 |
| CN110461883B (zh) | 2017-03-31 | 2021-11-30 | 大金工业株式会社 | 含氟聚合物的制造方法、聚合用表面活性剂和表面活性剂的使用 |
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| SG11202000862YA (en) | 2017-08-10 | 2020-02-27 | Daikin Ind Ltd | Method for producing purified polytetrafluoroethylene aqueous dispersion liquid, method for producing modified polytetrafluoroethylene powder, method for producing polytetrafluoroethylene molded body, and composition |
| WO2019031617A1 (ja) | 2017-08-10 | 2019-02-14 | ダイキン工業株式会社 | 精製ポリテトラフルオロエチレン水性分散液の製造方法、改質ポリテトラフルオロエチレン粉末の製造方法、ポリテトラフルオロエチレン成形体の製造方法、及び、組成物 |
| JP7345454B2 (ja) * | 2017-09-08 | 2023-09-15 | ソルベイ スペシャルティ ポリマーズ イタリー エス．ピー．エー． | フルオロポリマーを製造する方法 |
| EP3689916B1 (en) * | 2017-09-28 | 2023-12-27 | AGC Inc. | Method for producing modified polytetrafluoroethylene, method for producing modified polytetrafluoroethylene powder, and method for producing stretched porous body |
| US11634514B2 (en) | 2018-02-08 | 2023-04-25 | Daikin Industries. Ltd. | Method for manufacturing fluoropolymer, surfactant for polymerization, use for surfactant, and composition |
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| US12583947B2 (en) | 2018-03-07 | 2026-03-24 | Daikin Industries, Ltd. | Method for producing fluoropolymer |
| CN112154162B (zh) * | 2018-05-18 | 2022-07-26 | Ａｇｃ株式会社 | 含氟聚合物的制造方法及含氟离子交换聚合物的制造方法 |
| CN112739728B (zh) * | 2018-10-03 | 2023-03-10 | 大金工业株式会社 | 聚四氟乙烯的制造方法 |
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| CA3151436A1 (en) * | 2019-10-11 | 2021-04-15 | Rajeev Chauhan | Process for preparing fluoropolymers and fluoroelastomers in presence of a non fluorinated sulfonate type hydrocarbon containing surfactant thereof |
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| CN114651018A (zh) | 2019-11-19 | 2022-06-21 | 大金工业株式会社 | 含氟聚合物的制造方法、聚四氟乙烯的制造方法、全氟弹性体的制造方法和组合物 |
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| KR20230009876A (ko) * | 2020-05-14 | 2023-01-17 | 구자라트 플루오로케미칼스 리미티드 | 플루오르화 및 비-플루오르화 계면활성제의 조합을 사용한 플루오로단량체 중합 방법 |
| WO2022072693A1 (en) | 2020-10-01 | 2022-04-07 | The Chemours Company Fc, Llc | Low reactivity hydrocarbon dispersing agents in the aqueous polymerization of fluoropolymers |
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| EP4342921A4 (en) | 2021-05-19 | 2025-04-23 | Daikin Industries, Ltd. | Process for producing a fluoropolymer, process for producing polytetrafluoroethylene and composition |
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| CN121219330A (zh) | 2023-05-31 | 2025-12-26 | 大金工业株式会社 | 含氟聚合物水性分散液的制造方法和含氟聚合物水性分散液 |
| CN116854841B (zh) * | 2023-07-31 | 2026-02-17 | 河南省氟基新材料科技有限公司 | 一种锂电级聚偏二氟乙烯粘结剂的制备方法 |
| TW202528491A (zh) | 2023-12-06 | 2025-07-16 | 美商科慕Ｆｃ有限責任公司 | 部分氟化芳基醚界面活性劑組成物及使用方法 |
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| WO2005003075A1 (ja) | 2003-07-02 | 2005-01-13 | Daikin Industries, Ltd. | フルオロアルキルカルボン酸誘導体、含フッ素重合体の製造方法及び含フッ素重合体水性分散液 |
| US20050090613A1 (en) | 2003-10-22 | 2005-04-28 | Daikin Industries, Ltd. | Process for preparing fluorine-containing polymer latex |
| US7141537B2 (en) | 2003-10-30 | 2006-11-28 | 3M Innovative Properties Company | Mixture of fluorinated polyethers and use thereof as surfactant |
| EP1533325B1 (en) * | 2003-11-17 | 2011-10-19 | 3M Innovative Properties Company | Aqueous dispersions of polytetrafluoroethylene having a low amount of fluorinated surfactant |
| ITMI20050007A1 (it) * | 2005-01-05 | 2006-07-06 | Solvay Solexis Spa | Uso di dispersioni acquose di polimeri a base di vdf nella preparazione di vernici per rivestimenti di substrati architettonici |
| US7671112B2 (en) | 2005-07-15 | 2010-03-02 | 3M Innovative Properties Company | Method of making fluoropolymer dispersion |
| GB0514387D0 (en) | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant |
| GB0514398D0 (en) | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant |
| GB0525978D0 (en) | 2005-12-21 | 2006-02-01 | 3M Innovative Properties Co | Fluorinated Surfactants For Making Fluoropolymers |
| EP1939222B2 (en) | 2005-10-17 | 2019-09-04 | AGC Inc. | Process for producing an AQUEOUS POLYTETRAFLUOROETHYLENE EMULSION, AND POLYTETRAFLUOROETHYLENE FINE POWDER AND POROUS MATERIAL PRODUCED FROM THE SAME |
| JP5141256B2 (ja) | 2005-10-20 | 2013-02-13 | 旭硝子株式会社 | ポリテトラフルオロエチレン水性分散液およびその製品 |
| WO2007046377A1 (ja) | 2005-10-20 | 2007-04-26 | Asahi Glass Company, Limited | 溶融成形可能なフッ素樹脂の製造方法 |
| WO2007049517A1 (ja) | 2005-10-26 | 2007-05-03 | Asahi Glass Company, Limited | 含フッ素乳化剤の残留量が少ないフッ素樹脂およびその製造方法 |
| ATE510857T1 (de) | 2006-11-09 | 2011-06-15 | Du Pont | Wässrige polymerisation eines fluorinierten monomers mithilfe eines polymerisationsmittels mit einer fluorpolyethersäure oder einem salz daraus und einem kurzkettigen fluortensid |
-
2007
- 2007-11-09 EP EP07840004A patent/EP2084195B1/en not_active Not-in-force
- 2007-11-09 US US11/937,536 patent/US7897682B2/en active Active
- 2007-11-09 JP JP2009536316A patent/JP5439186B2/ja active Active
- 2007-11-09 AT AT07840004T patent/ATE512165T1/de not_active IP Right Cessation
- 2007-11-09 WO PCT/US2007/023642 patent/WO2008060463A1/en not_active Ceased
- 2007-11-09 CN CN200780041364.2A patent/CN101605826B/zh not_active Expired - Fee Related
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