JP2012513534A5 - - Google Patents
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- Publication number
- JP2012513534A5 JP2012513534A5 JP2011543670A JP2011543670A JP2012513534A5 JP 2012513534 A5 JP2012513534 A5 JP 2012513534A5 JP 2011543670 A JP2011543670 A JP 2011543670A JP 2011543670 A JP2011543670 A JP 2011543670A JP 2012513534 A5 JP2012513534 A5 JP 2012513534A5
- Authority
- JP
- Japan
- Prior art keywords
- fluorinated
- polymerization
- aqueous
- fluorinated ionomer
- group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000006116 polymerization reaction Methods 0.000 claims description 25
- 229920000554 ionomer Polymers 0.000 claims description 18
- 239000000178 monomer Substances 0.000 claims description 12
- 239000006185 dispersion Substances 0.000 claims description 10
- 229920002313 fluoropolymer Polymers 0.000 claims description 8
- 239000004811 fluoropolymer Substances 0.000 claims description 8
- 239000003999 initiator Substances 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- 125000003010 ionic group Chemical group 0.000 claims description 6
- 230000000379 polymerizing effect Effects 0.000 claims description 6
- 239000010419 fine particle Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 description 29
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical compound FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 14
- 239000002609 medium Substances 0.000 description 7
- -1 sulfonamide anion Chemical class 0.000 description 7
- GWTYBAOENKSFAY-UHFFFAOYSA-N 1,1,1,2,2-pentafluoro-2-(1,2,2-trifluoroethenoxy)ethane Chemical compound FC(F)=C(F)OC(F)(F)C(F)(F)F GWTYBAOENKSFAY-UHFFFAOYSA-N 0.000 description 4
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 229910052739 hydrogen Inorganic materials 0.000 description 4
- 239000000155 melt Substances 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- 150000007942 carboxylates Chemical class 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 229920001971 elastomer Polymers 0.000 description 3
- 239000000806 elastomer Substances 0.000 description 3
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 3
- 239000011859 microparticle Substances 0.000 description 3
- YSYRISKCBOPJRG-UHFFFAOYSA-N 4,5-difluoro-2,2-bis(trifluoromethyl)-1,3-dioxole Chemical compound FC1=C(F)OC(C(F)(F)F)(C(F)(F)F)O1 YSYRISKCBOPJRG-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 description 2
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 125000001273 sulfonato group Chemical class [O-]S(*)(=O)=O 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- MIZLGWKEZAPEFJ-UHFFFAOYSA-N 1,1,2-trifluoroethene Chemical group FC=C(F)F MIZLGWKEZAPEFJ-UHFFFAOYSA-N 0.000 description 1
- JMGNVALALWCTLC-UHFFFAOYSA-N 1-fluoro-2-(2-fluoroethenoxy)ethene Chemical compound FC=COC=CF JMGNVALALWCTLC-UHFFFAOYSA-N 0.000 description 1
- RFJVDJWCXSPUBY-UHFFFAOYSA-N 2-(difluoromethylidene)-4,4,5-trifluoro-5-(trifluoromethyl)-1,3-dioxolane Chemical compound FC(F)=C1OC(F)(F)C(F)(C(F)(F)F)O1 RFJVDJWCXSPUBY-UHFFFAOYSA-N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- QMIWYOZFFSLIAK-UHFFFAOYSA-N 3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene Chemical group FC(F)(F)C(=C)C(F)(F)F QMIWYOZFFSLIAK-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229920001774 Perfluoroether Polymers 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000011258 core-shell material Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- UEZVMMHDMIWARA-UHFFFAOYSA-M phosphonate Chemical compound [O-]P(=O)=O UEZVMMHDMIWARA-UHFFFAOYSA-M 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 229940124530 sulfonamide Drugs 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14011808P | 2008-12-23 | 2008-12-23 | |
| US61/140,118 | 2008-12-23 | ||
| PCT/US2009/069370 WO2010075496A1 (en) | 2008-12-23 | 2009-12-23 | Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer produced in situ |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012513534A JP2012513534A (ja) | 2012-06-14 |
| JP2012513534A5 true JP2012513534A5 (https=) | 2013-02-07 |
| JP5703233B2 JP5703233B2 (ja) | 2015-04-15 |
Family
ID=42026728
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011543670A Expired - Fee Related JP5703233B2 (ja) | 2008-12-23 | 2009-12-23 | その場生成されるフッ素化イオノマーの分散した微粒子を使用する水性重合によって製造されるフルオロポリマー |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US8058376B2 (https=) |
| EP (1) | EP2367861B1 (https=) |
| JP (1) | JP5703233B2 (https=) |
| CN (1) | CN102264775B (https=) |
| WO (1) | WO2010075496A1 (https=) |
Families Citing this family (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100036053A1 (en) * | 2008-08-08 | 2010-02-11 | E.I. Du Pont De Nemours And Company | Aqueous Polymerization Process for the Manufacture of Fluoropolymer Comprising Repeating Units Arising from a Perfluoromonomer and a Monomer Having a Functional Group and a Polymerizable Carbon-Carbon Double Bond |
| US8153738B2 (en) * | 2008-12-23 | 2012-04-10 | E I Du Pont De Nemours And Company | Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer |
| US9012025B2 (en) * | 2012-04-05 | 2015-04-21 | Xerox Corporation | Fuser member |
| JP5665800B2 (ja) | 2012-06-22 | 2015-02-04 | 三井・デュポンフロロケミカル株式会社 | テトラフルオロエチレン／パーフルオロ（アルキルビニルエーテル）共重合体 |
| WO2014023611A1 (en) | 2012-08-10 | 2014-02-13 | Solvay Specialty Polymers Italy S.P.A. | Allyl-bearing fluorinated ionomers |
| EP2927248B1 (en) * | 2012-11-30 | 2018-06-13 | Daikin Industries, Ltd. | Production method for polytetrafluoroethylene aqueous dispersion |
| EP2935370A1 (en) * | 2012-12-18 | 2015-10-28 | E. I. du Pont de Nemours and Company | Process for producing fluoroelastomers |
| CN105431485A (zh) * | 2013-07-30 | 2016-03-23 | 索尔维特殊聚合物意大利有限公司 | 含氟热塑性弹性体组合物 |
| KR102112645B1 (ko) * | 2013-11-29 | 2020-05-19 | 아사히 가세이 가부시키가이샤 | 고분자 전해질막 |
| EP3053937B1 (en) | 2013-11-29 | 2019-02-27 | Daikin Industries, Ltd. | Modified polytetrafluoroethylene fine powder and uniaxially oriented porous body |
| CN105794031B (zh) | 2013-11-29 | 2019-01-29 | 旭化成株式会社 | 高分子电解质膜 |
| EP4596613A1 (en) | 2013-11-29 | 2025-08-06 | Daikin Industries, Ltd. | Porous body, polymer electrolyte membrane, filter material for filter, and filter unit |
| JP6395411B2 (ja) * | 2014-03-25 | 2018-09-26 | 三井・ケマーズ フロロプロダクツ株式会社 | テトラフルオロエチレンとパーフルオロ（エチルビニルエーテル）との共重合体を含む複合成形体 |
| US20200199259A1 (en) | 2017-09-14 | 2020-06-25 | 3M Innovative Properties Company | Fluoropolymer dispersion, method for making the fluoropolymer dispersion, catalyst ink and polymer electrolyte membrane |
| EP3760649B1 (en) | 2018-03-01 | 2024-01-24 | Daikin Industries, Ltd. | Method for manufacturing fluoropolymer |
| WO2020105651A1 (ja) | 2018-11-19 | 2020-05-28 | ダイキン工業株式会社 | 変性ポリテトラフルオロエチレンの製造方法及び組成物 |
| TWI821458B (zh) * | 2018-11-19 | 2023-11-11 | 日商大金工業股份有限公司 | 組成物及拉伸體 |
| JP7389366B2 (ja) | 2019-04-26 | 2023-11-30 | ダイキン工業株式会社 | フルオロポリマー水性分散液の製造方法、排水の処理方法、及び、フルオロポリマー水性分散液 |
| JP7417129B2 (ja) | 2019-04-26 | 2024-01-18 | ダイキン工業株式会社 | 水の処理方法および組成物 |
| WO2021045165A1 (ja) * | 2019-09-05 | 2021-03-11 | ダイキン工業株式会社 | パーフルオロエラストマーの製造方法および組成物 |
| JP7231868B2 (ja) | 2019-09-05 | 2023-03-02 | ダイキン工業株式会社 | 組成物およびその製造方法 |
| WO2021100836A1 (ja) | 2019-11-19 | 2021-05-27 | ダイキン工業株式会社 | フルオロポリマーの製造方法、ポリテトラフルオロエチレンの製造方法、パーフルオロエラストマーの製造方法および組成物 |
| CN111114836B (zh) * | 2019-12-31 | 2021-07-06 | 上海空间推进研究所 | 大尺寸高基频轻量化表面张力贮箱 |
| CN111690092B (zh) * | 2020-06-03 | 2022-04-19 | 乳源东阳光氟树脂有限公司 | 一种聚偏氟乙烯表面改性的核壳结构锂电池粘结剂及其制备方法和应用 |
| CN112409528B (zh) * | 2020-10-21 | 2021-11-16 | 浙江巨化技术中心有限公司 | 一种核壳结构ptfe分散树脂的制备方法 |
| WO2022107894A1 (ja) | 2020-11-19 | 2022-05-27 | ダイキン工業株式会社 | ポリテトラフルオロエチレンの製造方法およびポリテトラフルオロエチレンを含有する組成物 |
| JP7549257B2 (ja) | 2020-11-19 | 2024-09-11 | ダイキン工業株式会社 | パーフルオロエラストマー水性分散液の製造方法、組成物、架橋性組成物および架橋物 |
| EP4249517A4 (en) | 2020-11-19 | 2024-10-16 | Daikin Industries, Ltd. | PROCESS FOR PRODUCING AN AQUEOUS DISPERSION OF FLUORINE-CONTAINING ELASTOMER, AND COMPOSITION |
| KR20230150868A (ko) | 2021-03-10 | 2023-10-31 | 다이킨 고교 가부시키가이샤 | 도료 조성물, 도포막, 적층체 및 도장 물품 |
| JPWO2022244784A1 (https=) | 2021-05-19 | 2022-11-24 | ||
| JP7741413B2 (ja) | 2021-06-11 | 2025-09-18 | ダイキン工業株式会社 | 含フッ素エラストマー水性分散液の製造方法、組成物および水性分散液 |
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| WO2023277140A1 (ja) | 2021-06-30 | 2023-01-05 | ダイキン工業株式会社 | 高純度フルオロポリマー含有組成物の製造方法および高純度フルオロポリマー含有組成物 |
| CN113549168B (zh) * | 2021-08-19 | 2023-01-20 | 常熟三爱富中昊化工新材料有限公司 | 聚三氟苯乙烯的制备方法 |
| EP4497762A4 (en) | 2022-03-23 | 2026-03-18 | Daikin Ind Ltd | PROCESS FOR PRODUCING FLUORIDED POLYMER, AND COMPOSITION |
| CN119095910A (zh) | 2022-04-28 | 2024-12-06 | 大金工业株式会社 | 含有氟橡胶的组合物 |
| JP7787462B2 (ja) | 2022-04-28 | 2025-12-17 | ダイキン工業株式会社 | フルオロポリマーの製造方法 |
| CN119072500A (zh) * | 2022-04-28 | 2024-12-03 | 大金工业株式会社 | 含有氟树脂的组合物的制造方法和含有氟树脂的组合物 |
| WO2024154773A1 (ja) | 2023-01-18 | 2024-07-25 | ダイキン工業株式会社 | テトラフルオロエチレン系ポリマー組成物、電気化学デバイス用バインダー、電極合剤、電極、及び、二次電池 |
| EP4456182A4 (en) | 2023-01-18 | 2025-09-03 | Daikin Ind Ltd | MIXTURE FOR ELECTROCHEMICAL DEVICE, MIXTURE SHEET FOR ELECTROCHEMICAL DEVICE, ELECTRODE AND ELECTROCHEMICAL DEVICE |
| JP7820661B2 (ja) | 2023-08-14 | 2026-02-26 | ダイキン工業株式会社 | フルオロポリマー水性分散液の製造方法およびフルオロポリマー水性分散液 |
| JP7689278B2 (ja) | 2023-08-28 | 2025-06-06 | ダイキン工業株式会社 | 水溶性含フッ素ポリマーの回収方法 |
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| US7557164B2 (en) * | 2003-08-19 | 2009-07-07 | E. I. Du Pont De Nemours And Company | Membranes of fluorinated ionomer blended with nonionomeric fluoropolymers for electrochemical cells |
| US20050090613A1 (en) * | 2003-10-22 | 2005-04-28 | Daikin Industries, Ltd. | Process for preparing fluorine-containing polymer latex |
| US7071271B2 (en) * | 2003-10-30 | 2006-07-04 | 3M Innovative Properties Company | Aqueous emulsion polymerization of functionalized fluoromonomers |
| DE10352692A1 (de) | 2003-11-12 | 2005-06-23 | Sanguibiotech Gmbh | Verwendung hypo-onkotischer Lösungen in das Blut addierbarer, hyperpolymerer Hämoglobine zur Behandlung eines Lungenödems |
| ATE529451T1 (de) * | 2003-11-17 | 2011-11-15 | 3M Innovative Properties Co | Wässrige ptfe-dispersionen mit einem niedrigen gehalt an fluorierten emulgatoren |
| JP2005320501A (ja) * | 2004-04-07 | 2005-11-17 | Daikin Ind Ltd | 含フッ素エラストマー重合体の製造方法 |
| US20060014887A1 (en) * | 2004-07-19 | 2006-01-19 | 3M Innovative Properties Company | Method of hydrolyzing a dispersion of ionic fluoropolymer |
| GB0511779D0 (en) * | 2005-06-10 | 2005-07-20 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers in the presence of a partially fluorinated oligomer as an emulsifier |
| GB0514398D0 (en) * | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant |
| GB0514387D0 (en) * | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant |
| US7671112B2 (en) * | 2005-07-15 | 2010-03-02 | 3M Innovative Properties Company | Method of making fluoropolymer dispersion |
| CN100558753C (zh) | 2005-10-17 | 2009-11-11 | 旭硝子株式会社 | 聚四氟乙烯水性乳化液、由其制得的聚四氟乙烯细粉和多孔体 |
| JP5141256B2 (ja) | 2005-10-20 | 2013-02-13 | 旭硝子株式会社 | ポリテトラフルオロエチレン水性分散液およびその製品 |
| WO2007046377A1 (ja) | 2005-10-20 | 2007-04-26 | Asahi Glass Company, Limited | 溶融成形可能なフッ素樹脂の製造方法 |
| EP1942118B1 (en) | 2005-10-26 | 2013-09-11 | Asahi Glass Company, Limited | Fluororesin with low fluorine-containing emulsifier residual and method for producing same |
| JP5439186B2 (ja) | 2006-11-09 | 2014-03-12 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | フルオロポリエーテル酸または塩および炭化水素系界面活性剤を含む重合剤を用いるフッ素化モノマーの水性重合 |
| US7989566B2 (en) | 2008-01-22 | 2011-08-02 | Dupont Performance Elastomers Llc | Process for producing fluoropolymers |
-
2009
- 2009-12-18 US US12/641,374 patent/US8058376B2/en not_active Expired - Fee Related
- 2009-12-23 CN CN200980152388.4A patent/CN102264775B/zh not_active Expired - Fee Related
- 2009-12-23 WO PCT/US2009/069370 patent/WO2010075496A1/en not_active Ceased
- 2009-12-23 JP JP2011543670A patent/JP5703233B2/ja not_active Expired - Fee Related
- 2009-12-23 EP EP09796576.8A patent/EP2367861B1/en not_active Not-in-force
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