JP2012533413A5 - - Google Patents
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- Publication number
- JP2012533413A5 JP2012533413A5 JP2012520819A JP2012520819A JP2012533413A5 JP 2012533413 A5 JP2012533413 A5 JP 2012533413A5 JP 2012520819 A JP2012520819 A JP 2012520819A JP 2012520819 A JP2012520819 A JP 2012520819A JP 2012533413 A5 JP2012533413 A5 JP 2012533413A5
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- catalyst precursor
- precursor composition
- composition
- magnesium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 claims description 72
- 239000012018 catalyst precursor Substances 0.000 claims description 41
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 36
- 229910052742 iron Inorganic materials 0.000 claims description 14
- 229910052751 metal Inorganic materials 0.000 claims description 14
- 239000002184 metal Substances 0.000 claims description 14
- 229910052750 molybdenum Inorganic materials 0.000 claims description 9
- 150000002736 metal compounds Chemical class 0.000 claims description 5
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 3
- 239000000347 magnesium hydroxide Substances 0.000 claims description 3
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 3
- 239000003054 catalyst Substances 0.000 claims 26
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 18
- 239000002245 particle Substances 0.000 claims 16
- 239000010941 cobalt Substances 0.000 claims 12
- 229910017052 cobalt Inorganic materials 0.000 claims 12
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims 12
- 229910003455 mixed metal oxide Inorganic materials 0.000 claims 11
- 229910052749 magnesium Inorganic materials 0.000 claims 9
- 239000011777 magnesium Substances 0.000 claims 9
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims 9
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims 8
- 239000000395 magnesium oxide Substances 0.000 claims 8
- 239000011733 molybdenum Substances 0.000 claims 8
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims 7
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 5
- -1 magnesium aluminate Chemical class 0.000 claims 4
- QIJNJJZPYXGIQM-UHFFFAOYSA-N 1lambda4,2lambda4-dimolybdacyclopropa-1,2,3-triene Chemical compound [Mo]=C=[Mo] QIJNJJZPYXGIQM-UHFFFAOYSA-N 0.000 claims 3
- 229910039444 MoC Inorganic materials 0.000 claims 3
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims 3
- 229910001567 cementite Inorganic materials 0.000 claims 3
- 150000002681 magnesium compounds Chemical class 0.000 claims 3
- 238000001354 calcination Methods 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 229910020068 MgAl Inorganic materials 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- 239000002041 carbon nanotube Substances 0.000 description 5
- 229910021393 carbon nanotube Inorganic materials 0.000 description 5
- 239000002048 multi walled nanotube Substances 0.000 description 5
- 238000005325 percolation Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- 229940011182 cobalt acetate Drugs 0.000 description 2
- QAHREYKOYSIQPH-UHFFFAOYSA-L cobalt(II) acetate Chemical compound [Co+2].CC([O-])=O.CC([O-])=O QAHREYKOYSIQPH-UHFFFAOYSA-L 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 description 2
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002071 nanotube Substances 0.000 description 2
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- XUFUCDNVOXXQQC-UHFFFAOYSA-L azane;hydroxy-(hydroxy(dioxo)molybdenio)oxy-dioxomolybdenum Chemical compound N.N.O[Mo](=O)(=O)O[Mo](O)(=O)=O XUFUCDNVOXXQQC-UHFFFAOYSA-L 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 150000001869 cobalt compounds Chemical class 0.000 description 1
- UFMZWBIQTDUYBN-UHFFFAOYSA-N cobalt dinitrate Chemical compound [Co+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O UFMZWBIQTDUYBN-UHFFFAOYSA-N 0.000 description 1
- 229910001981 cobalt nitrate Inorganic materials 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000002506 iron compounds Chemical class 0.000 description 1
- PVFSDGKDKFSOTB-UHFFFAOYSA-K iron(3+);triacetate Chemical compound [Fe+3].CC([O-])=O.CC([O-])=O.CC([O-])=O PVFSDGKDKFSOTB-UHFFFAOYSA-K 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000005078 molybdenum compound Substances 0.000 description 1
- 150000002752 molybdenum compounds Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US22643809P | 2009-07-17 | 2009-07-17 | |
| US61/226,438 | 2009-07-17 | ||
| PCT/US2010/042321 WO2011009071A1 (en) | 2009-07-17 | 2010-07-16 | Catalyst and methods for producing multi-wall carbon nanotubes |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014255341A Division JP5932010B2 (ja) | 2009-07-17 | 2014-12-17 | 多層カーボンナノチューブ製造のための触媒および方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012533413A JP2012533413A (ja) | 2012-12-27 |
| JP2012533413A5 true JP2012533413A5 (enExample) | 2013-08-29 |
| JP5670451B2 JP5670451B2 (ja) | 2015-02-18 |
Family
ID=43449832
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012520819A Active JP5670451B2 (ja) | 2009-07-17 | 2010-07-16 | 多層カーボンナノチューブ製造のための触媒および方法 |
| JP2014255341A Active JP5932010B2 (ja) | 2009-07-17 | 2014-12-17 | 多層カーボンナノチューブ製造のための触媒および方法 |
| JP2016088743A Active JP6310956B2 (ja) | 2009-07-17 | 2016-04-27 | 多層カーボンナノチューブ製造のための触媒および方法 |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014255341A Active JP5932010B2 (ja) | 2009-07-17 | 2014-12-17 | 多層カーボンナノチューブ製造のための触媒および方法 |
| JP2016088743A Active JP6310956B2 (ja) | 2009-07-17 | 2016-04-27 | 多層カーボンナノチューブ製造のための触媒および方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US9084990B2 (enExample) |
| EP (1) | EP2454015B1 (enExample) |
| JP (3) | JP5670451B2 (enExample) |
| CN (1) | CN106829925A (enExample) |
| CA (1) | CA2768474A1 (enExample) |
| WO (1) | WO2011009071A1 (enExample) |
Families Citing this family (35)
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| JP2851505B2 (ja) | 1993-02-26 | 1999-01-27 | 信越化学工業株式会社 | シリコーン系防水処理剤およびこれによる防水処理方法 |
| AU2010236807B2 (en) | 2009-04-17 | 2014-09-25 | Seerstone Llc | Method for producing solid carbon by reducing carbon oxides |
| CN106829925A (zh) * | 2009-07-17 | 2017-06-13 | 西南纳米科技公司 | 用于制备多壁碳纳米管的催化剂和方法 |
| KR101424910B1 (ko) * | 2012-01-11 | 2014-07-31 | 주식회사 엘지화학 | 카본나노튜브 및 그 제조방법 |
| NO2749379T3 (enExample) | 2012-04-16 | 2018-07-28 | ||
| MX354529B (es) | 2012-04-16 | 2018-03-07 | Seerstone Llc | Métodos para producir carbono sólido mediante la reducción de dióxido de carbono. |
| CN104284861A (zh) | 2012-04-16 | 2015-01-14 | 赛尔斯通股份有限公司 | 处理含有碳氧化物的废气的方法 |
| MX354526B (es) | 2012-04-16 | 2018-03-07 | Seerstone Llc | Metodos y sistemas para capturar y secuestrar carbono y para reducir la masa de oxidos de carbono en una corriente de gas de desechos. |
| WO2013158156A1 (en) | 2012-04-16 | 2013-10-24 | Seerstone Llc | Methods and structures for reducing carbon oxides with non-ferrous catalysts |
| US9896341B2 (en) | 2012-04-23 | 2018-02-20 | Seerstone Llc | Methods of forming carbon nanotubes having a bimodal size distribution |
| WO2014011631A1 (en) | 2012-07-12 | 2014-01-16 | Seerstone Llc | Solid carbon products comprising carbon nanotubes and methods of forming same |
| US10815124B2 (en) | 2012-07-12 | 2020-10-27 | Seerstone Llc | Solid carbon products comprising carbon nanotubes and methods of forming same |
| WO2014011206A1 (en) | 2012-07-13 | 2014-01-16 | Seerstone Llc | Methods and systems for forming ammonia and solid carbon products |
| US9779845B2 (en) | 2012-07-18 | 2017-10-03 | Seerstone Llc | Primary voltaic sources including nanofiber Schottky barrier arrays and methods of forming same |
| JP6389824B2 (ja) | 2012-11-29 | 2018-09-12 | シーアストーン リミテッド ライアビリティ カンパニー | 固体炭素材料を製造するための反応器および方法 |
| EP3129321B1 (en) | 2013-03-15 | 2021-09-29 | Seerstone LLC | Electrodes comprising nanostructured carbon |
| WO2014151898A1 (en) | 2013-03-15 | 2014-09-25 | Seerstone Llc | Systems for producing solid carbon by reducing carbon oxides |
| WO2014151144A1 (en) | 2013-03-15 | 2014-09-25 | Seerstone Llc | Carbon oxide reduction with intermetallic and carbide catalysts |
| US9783416B2 (en) | 2013-03-15 | 2017-10-10 | Seerstone Llc | Methods of producing hydrogen and solid carbon |
| WO2014151138A1 (en) | 2013-03-15 | 2014-09-25 | Seerstone Llc | Reactors, systems, and methods for forming solid products |
| WO2015005709A1 (ko) | 2013-07-10 | 2015-01-15 | 주식회사 엘지화학 | 담지촉매, 탄소나노튜브 집합체 및 그 제조방법 |
| KR101535388B1 (ko) | 2013-07-19 | 2015-07-08 | 주식회사 엘지화학 | 담지촉매, 이의 제조방법 및 이를 이용하여 제조된 탄소나노구조체의 2차구조물 |
| CN105899752B (zh) * | 2013-12-18 | 2018-08-17 | 哈利伯顿能源服务公司 | 具有纳米管毯的钻地钻头 |
| KR20170012745A (ko) * | 2015-07-23 | 2017-02-03 | 에스케이이노베이션 주식회사 | 다중벽 탄소나노튜브 제조용 촉매 및 이를 이용한 다중벽 탄소나노튜브의 제조 방법 |
| US11752459B2 (en) | 2016-07-28 | 2023-09-12 | Seerstone Llc | Solid carbon products comprising compressed carbon nanotubes in a container and methods of forming same |
| JP6380588B1 (ja) * | 2017-03-15 | 2018-08-29 | 東洋インキＳｃホールディングス株式会社 | 多層カーボンナノチューブおよび多層カーボンナノチューブの製造方法 |
| JP7052336B2 (ja) * | 2017-12-20 | 2022-04-12 | 東洋インキＳｃホールディングス株式会社 | 多層カーボンナノチューブおよび多層カーボンナノチューブの製造方法 |
| CN110418766B (zh) * | 2017-03-15 | 2022-11-11 | 东洋油墨Sc控股株式会社 | 多层碳纳米管、多层碳纳米管的制造方法、分散液、树脂组合物及涂膜 |
| US10759663B2 (en) | 2017-05-23 | 2020-09-01 | Indian Oil Corporation Limited | Multi-metal catalyst composition for production of morphology controlled CNT's and process thereof |
| JP6590034B1 (ja) * | 2018-06-28 | 2019-10-16 | 東洋インキＳｃホールディングス株式会社 | カーボンナノチューブ分散液およびその利用 |
| CN111135788A (zh) * | 2019-09-18 | 2020-05-12 | 青岛农业大学 | 一种磁性掺氮碳纳米管水处理吸附剂及其制备方法 |
| EP4408796A4 (en) * | 2021-10-01 | 2025-09-03 | Chasm Advanced Mat Inc | SYSTEM AND METHOD FOR THE SYNTHESIS OF CARBON NANOTUBES AND HYBRID MATERIALS BY CATALYTIC CHEMICAL DEPOSITION |
| JP2024538123A (ja) * | 2021-10-13 | 2024-10-18 | キャズム アドバンスト マテリアルズ，インク． | コンクリート用途のためのカーボンナノチューブハイブリッド材料 |
| KR20240056211A (ko) * | 2022-10-21 | 2024-04-30 | 금호석유화학 주식회사 | 저직경 탄소나노튜브의 제조방법 및 그에 따라 제조된 탄소나노튜브 |
| WO2025072478A1 (en) * | 2023-09-29 | 2025-04-03 | Chasm Advanced Materials, Inc. | Carbon nanotube catalyst preconditioning |
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| KR101007183B1 (ko) * | 2008-10-23 | 2011-01-12 | 제일모직주식회사 | 탄소나노튜브 합성용 담지촉매, 그 제조방법 및 이를 이용한 탄소나노튜브 |
| US20100266478A1 (en) * | 2008-12-10 | 2010-10-21 | Cheil Industries Inc. | Metal Nano Catalyst, Method for Preparing the Same and Method for Controlling the Growth Types of Carbon Nanotubes Using the Same |
| KR100976174B1 (ko) * | 2009-02-13 | 2010-08-16 | 금호석유화학 주식회사 | 얇은 다중벽 탄소나노튜브 제조용 촉매조성물 및 이의 제조방법 |
| CN106829925A (zh) * | 2009-07-17 | 2017-06-13 | 西南纳米科技公司 | 用于制备多壁碳纳米管的催化剂和方法 |
-
2010
- 2010-07-16 CN CN201610528088.3A patent/CN106829925A/zh active Pending
- 2010-07-16 US US13/383,963 patent/US9084990B2/en active Active
- 2010-07-16 JP JP2012520819A patent/JP5670451B2/ja active Active
- 2010-07-16 EP EP10800624.8A patent/EP2454015B1/en active Active
- 2010-07-16 CA CA2768474A patent/CA2768474A1/en not_active Abandoned
- 2010-07-16 WO PCT/US2010/042321 patent/WO2011009071A1/en not_active Ceased
-
2014
- 2014-12-17 JP JP2014255341A patent/JP5932010B2/ja active Active
-
2015
- 2015-06-16 US US14/740,870 patent/US9855551B2/en active Active
-
2016
- 2016-04-27 JP JP2016088743A patent/JP6310956B2/ja active Active
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