JP2012526920A5 - - Google Patents

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JP2012526920A5
JP2012526920A5 JP2012510865A JP2012510865A JP2012526920A5 JP 2012526920 A5 JP2012526920 A5 JP 2012526920A5 JP 2012510865 A JP2012510865 A JP 2012510865A JP 2012510865 A JP2012510865 A JP 2012510865A JP 2012526920 A5 JP2012526920 A5 JP 2012526920A5
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Japan
Prior art keywords
alloy particles
grinding
mill
mill base
nanostructure
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JP2012510865A
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JP2012526920A (ja
JP6230232B2 (ja
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Priority claimed from US12/465,852 external-priority patent/US8287772B2/en
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Claims (7)

  1. 粉砕媒体を含有するペブルミルでミルベースを粉砕し、ナノ構造体の合金粒子を用意することを含む、ナノ構造体の合金粒子を製造する方法であって、
    前記ミルベースが(i)シリコンと、(ii)少なくとも1つの炭素又は遷移金属とを含み、前記ナノ構造体の合金粒子、サイズが50ナノメートルより大きい結晶ドメインが実質的に無い、方法。
  2. リチウムイオン電池用の負極組成物を製造する方法であって、
    (a)粉砕媒体を含有するペブルミルでミルベースを粉砕することを含む方法によってナノ構造体の合金粒子を製造する工程と、
    (b)前記負極組成物を提供するために、重合体結合剤中に前記ナノ構造体の合金粒子を分散させる工程と、を含み、
    前記ミルベースは、
    (i)シリコンと、
    (ii)少なくとも1つの炭素又は遷移金属と、を含み、前記ナノ構造体の合金粒子は、サイズが50ナノメートルより大きい結晶ドメインが実質的に無い、方法。
  3. 前記粉砕媒体の前記ミルベースに対する容積比が、5:1を超える、請求項1又は2に記載の方法。
  4. 前記ナノ構造体の合金粒子が非晶質である、請求項1又は2に記載の方法。
  5. 前記ペブルミルの前記粉砕媒体と前記ミルベースとを合わせた容積に対する容積比が、2:1以下である、請求項1又は2に記載の方法。
  6. 前記ペブルミルが理論的な臨界回転数を有し、前記ペブルミルが、前記理論的な臨界回転数の50〜120パーセントの範囲の回転速度を有する、請求項1又は2に記載の方法。
  7. 前記粉砕媒体が、0.01〜0.3ジュールの範囲の最大衝撃エネルギーを有する、請求項1又は2に記載の方法。
JP2012510865A 2009-05-14 2010-05-07 低エネルギー粉砕方法、低結晶性合金、及び負極組成物 Active JP6230232B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/465,852 2009-05-14
US12/465,852 US8287772B2 (en) 2009-05-14 2009-05-14 Low energy milling method, low crystallinity alloy, and negative electrode composition
PCT/US2010/033955 WO2010132279A1 (en) 2009-05-14 2010-05-07 Low energy milling method, low crystallinity alloy, and negative electrode composition

Publications (3)

Publication Number Publication Date
JP2012526920A JP2012526920A (ja) 2012-11-01
JP2012526920A5 true JP2012526920A5 (ja) 2013-06-20
JP6230232B2 JP6230232B2 (ja) 2017-11-15

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JP2012510865A Active JP6230232B2 (ja) 2009-05-14 2010-05-07 低エネルギー粉砕方法、低結晶性合金、及び負極組成物

Country Status (7)

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US (1) US8287772B2 (ja)
EP (1) EP2429744B1 (ja)
JP (1) JP6230232B2 (ja)
KR (2) KR20120026536A (ja)
CN (1) CN102458720B (ja)
PL (1) PL2429744T3 (ja)
WO (1) WO2010132279A1 (ja)

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