JP2012522125A5 - - Google Patents
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- JP2012522125A5 JP2012522125A5 JP2012501264A JP2012501264A JP2012522125A5 JP 2012522125 A5 JP2012522125 A5 JP 2012522125A5 JP 2012501264 A JP2012501264 A JP 2012501264A JP 2012501264 A JP2012501264 A JP 2012501264A JP 2012522125 A5 JP2012522125 A5 JP 2012522125A5
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- 238000000034 method Methods 0.000 claims description 11
- JTIAYWZZZOZUTK-UHFFFAOYSA-N 1-tert-butyl-3-methylbenzene Chemical compound CC1=CC=CC(C(C)(C)C)=C1 JTIAYWZZZOZUTK-UHFFFAOYSA-N 0.000 claims description 8
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 238000006198 methoxylation reaction Methods 0.000 claims description 6
- XUXDTBHGWCZVEQ-UHFFFAOYSA-N 1-tert-butyl-3-(dimethoxymethyl)benzene Chemical compound COC(OC)C1=CC=CC(C(C)(C)C)=C1 XUXDTBHGWCZVEQ-UHFFFAOYSA-N 0.000 claims description 5
- 239000006184 cosolvent Substances 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 4
- IGVZPDMKUBZLKT-UHFFFAOYSA-N 1-tert-butyl-3-[(3-tert-butylphenyl)methoxymethyl]benzene Chemical compound CC(C)(C)C1=CC=CC(COCC=2C=C(C=CC=2)C(C)(C)C)=C1 IGVZPDMKUBZLKT-UHFFFAOYSA-N 0.000 claims description 3
- 239000003792 electrolyte Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- -1 3-tert-butylbenzyl compounds Chemical class 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 239000007858 starting material Substances 0.000 claims description 2
- FIMHASWLGDDANN-UHFFFAOYSA-M methyl sulfate;tributyl(methyl)azanium Chemical compound COS([O-])(=O)=O.CCCC[N+](C)(CCCC)CCCC FIMHASWLGDDANN-UHFFFAOYSA-M 0.000 claims 2
- HKEQMVXZDQLSDY-UHFFFAOYSA-N 3-tert-butylbenzaldehyde Chemical compound CC(C)(C)C1=CC=CC(C=O)=C1 HKEQMVXZDQLSDY-UHFFFAOYSA-N 0.000 claims 1
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 claims 1
- 239000008151 electrolyte solution Substances 0.000 claims 1
- 230000007062 hydrolysis Effects 0.000 claims 1
- 238000006460 hydrolysis reaction Methods 0.000 claims 1
- LNYJYVGUHXQWLO-UHFFFAOYSA-M methyl sulfate;triethyl(methyl)azanium Chemical compound COS([O-])(=O)=O.CC[N+](C)(CC)CC LNYJYVGUHXQWLO-UHFFFAOYSA-M 0.000 claims 1
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 claims 1
- HBIBDYAXJQFKSJ-UHFFFAOYSA-N 1-tert-butyl-3-[1-[1-(3-tert-butylphenyl)ethoxy]ethyl]benzene Chemical compound C=1C=CC(C(C)(C)C)=CC=1C(C)OC(C)C1=CC=CC(C(C)(C)C)=C1 HBIBDYAXJQFKSJ-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09156398 | 2009-03-27 | ||
| EP09156398.1 | 2009-03-27 | ||
| PCT/EP2010/053656 WO2010108874A1 (de) | 2009-03-27 | 2010-03-22 | Elektrochemisches verfahern zur herstellung von 3-tert.-butylbenzaldehyd-dimethylacetal |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012522125A JP2012522125A (ja) | 2012-09-20 |
| JP2012522125A5 true JP2012522125A5 (https=) | 2013-05-09 |
| JP5553884B2 JP5553884B2 (ja) | 2014-07-16 |
Family
ID=42124639
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012501264A Expired - Fee Related JP5553884B2 (ja) | 2009-03-27 | 2010-03-22 | ３−第三ブチルベンズアルデヒドジメチルアセタールを製造するための電気化学的方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8629304B2 (https=) |
| EP (1) | EP2411564B1 (https=) |
| JP (1) | JP5553884B2 (https=) |
| CN (1) | CN102365393B (https=) |
| ES (1) | ES2637018T3 (https=) |
| MX (1) | MX2011010107A (https=) |
| WO (1) | WO2010108874A1 (https=) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5553884B2 (ja) | 2009-03-27 | 2014-07-16 | ビーエーエスエフ ソシエタス・ヨーロピア | ３−第三ブチルベンズアルデヒドジメチルアセタールを製造するための電気化学的方法 |
| EP2616424B1 (de) | 2010-09-16 | 2015-08-26 | Basf Se | Verfahren zur herstellung von 2-methyl-3-(4-tert-butylphenyl)-propanal mit hoher para-isomerenreinheit |
| KR20150023709A (ko) * | 2012-06-15 | 2015-03-05 | 바스프 에스이 | 친핵체 존재 하의 유기 기판의 애노드 산화 |
| US20130334058A1 (en) * | 2012-06-15 | 2013-12-19 | Basf Se | Anodic oxidation of organic substrates in the presence of nucleophiles |
| WO2022023330A1 (en) * | 2020-07-28 | 2022-02-03 | Basf Se | Cyclic compounds as aroma chemicals |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2848397C2 (de) * | 1978-11-08 | 1982-09-23 | Basf Ag, 6700 Ludwigshafen | Elektrochemische Herstellung von in 4-Stellung substituierten Benzaldehyddialkylacetalen |
| US4318783A (en) * | 1978-11-30 | 1982-03-09 | Bayer Aktiengesellschaft | Process for the preparation of optionally substituted benzaldehyde dialkyl acetals |
| JPS5620174A (en) * | 1979-07-27 | 1981-02-25 | Fuso Kagaku Kogyo Kk | Preparation of p-t-butylbenzaldehyde and its acetal |
| DE3322399A1 (de) | 1983-06-22 | 1985-01-10 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von benz aldehyddialkylacetalen |
| DE3713732A1 (de) * | 1987-04-24 | 1988-11-17 | Basf Ag | Neue benzaldehyddialkylacetale, ihre herstellung und verwendung |
| JP2738093B2 (ja) | 1989-12-19 | 1998-04-08 | 三菱化学株式会社 | 第３級ブチルベンズアルデヒド異性体混合物の製造方法 |
| JP3159471B2 (ja) * | 1991-07-11 | 2001-04-23 | 三井化学株式会社 | サリチル酸誘導体の製造方法 |
| DE4201544A1 (de) * | 1992-01-22 | 1993-07-29 | Basf Ag | Verfahren zur herstellung von benzaldehydacetalen |
| DE4327361A1 (de) | 1993-08-14 | 1995-02-16 | Basf Ag | Verfahren zur Herstellung von Benzaldehyddialkylacetalen |
| DE19904900A1 (de) | 1998-06-26 | 1999-12-30 | Basf Ag | Verfahren zur Herstellung von Alkoxymethylaromaten |
| DE102004011427A1 (de) | 2004-03-09 | 2005-09-29 | Basf Ag | Absorptionsmittel mit verbesserter Oxidationsbeständigkeit und Verfahren zum Entsäuern von Fluidströmen |
| WO2009059944A1 (de) | 2007-11-06 | 2009-05-14 | Basf Se | Elektrochemisches verfahren zur herstellung von benzaldehyddimethylacetalen |
| US20100256421A1 (en) * | 2009-03-23 | 2010-10-07 | O'laughlin Industries, Co. Ltd. | Propanal Production Methods |
| JP5553884B2 (ja) | 2009-03-27 | 2014-07-16 | ビーエーエスエフ ソシエタス・ヨーロピア | ３−第三ブチルベンズアルデヒドジメチルアセタールを製造するための電気化学的方法 |
-
2010
- 2010-03-22 JP JP2012501264A patent/JP5553884B2/ja not_active Expired - Fee Related
- 2010-03-22 MX MX2011010107A patent/MX2011010107A/es active IP Right Grant
- 2010-03-22 EP EP10709552.3A patent/EP2411564B1/de not_active Not-in-force
- 2010-03-22 US US13/260,650 patent/US8629304B2/en not_active Expired - Fee Related
- 2010-03-22 ES ES10709552.3T patent/ES2637018T3/es active Active
- 2010-03-22 CN CN201080014651.6A patent/CN102365393B/zh not_active Expired - Fee Related
- 2010-03-22 WO PCT/EP2010/053656 patent/WO2010108874A1/de not_active Ceased
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