JP2012513945A5 - - Google Patents
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- JP2012513945A5 JP2012513945A5 JP2011542814A JP2011542814A JP2012513945A5 JP 2012513945 A5 JP2012513945 A5 JP 2012513945A5 JP 2011542814 A JP2011542814 A JP 2011542814A JP 2011542814 A JP2011542814 A JP 2011542814A JP 2012513945 A5 JP2012513945 A5 JP 2012513945A5
- Authority
- JP
- Japan
- Prior art keywords
- compound
- mixture
- oxidation state
- general formula
- hpo
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 150000001875 compounds Chemical class 0.000 claims description 29
- 230000003647 oxidation Effects 0.000 claims description 13
- 238000007254 oxidation reaction Methods 0.000 claims description 13
- 239000003638 chemical reducing agent Substances 0.000 claims description 9
- 229910052698 phosphorus Inorganic materials 0.000 claims description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 7
- 125000004437 phosphorous atom Chemical group 0.000 claims description 7
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 2
- 239000011574 phosphorus Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 19
- 239000000203 mixture Substances 0.000 claims 17
- 239000004020 conductor Substances 0.000 claims 6
- 239000002245 particle Substances 0.000 claims 6
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims 4
- 229910001416 lithium ion Inorganic materials 0.000 claims 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- 229910052744 lithium Inorganic materials 0.000 claims 2
- 229910052748 manganese Inorganic materials 0.000 claims 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims 2
- 229910052759 nickel Inorganic materials 0.000 claims 2
- 229920000049 Carbon (fiber) Polymers 0.000 claims 1
- 229910018119 Li 3 PO 4 Inorganic materials 0.000 claims 1
- 125000004429 atom Chemical group 0.000 claims 1
- 239000006229 carbon black Substances 0.000 claims 1
- 239000004917 carbon fiber Substances 0.000 claims 1
- 239000002134 carbon nanofiber Substances 0.000 claims 1
- 239000002041 carbon nanotube Substances 0.000 claims 1
- 229910021393 carbon nanotube Inorganic materials 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- 229920001940 conductive polymer Polymers 0.000 claims 1
- 229910002804 graphite Inorganic materials 0.000 claims 1
- 239000010439 graphite Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- 230000007935 neutral effect Effects 0.000 claims 1
- 239000002243 precursor Substances 0.000 claims 1
- 229910052720 vanadium Inorganic materials 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 description 5
- 239000002707 nanocrystalline material Substances 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14111708P | 2008-12-29 | 2008-12-29 | |
| US61/141,117 | 2008-12-29 | ||
| PCT/EP2009/067742 WO2010076265A2 (en) | 2008-12-29 | 2009-12-22 | Synthesis of lithium-metal-phosphates under hydrothermal conditions |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012513945A JP2012513945A (ja) | 2012-06-21 |
| JP2012513945A5 true JP2012513945A5 (https=) | 2016-06-30 |
| JP5957225B2 JP5957225B2 (ja) | 2016-07-27 |
Family
ID=42199893
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011542814A Expired - Fee Related JP5957225B2 (ja) | 2008-12-29 | 2009-12-22 | 熱水条件下でのリチウム−金属−フォスフェイトの合成 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9156693B2 (https=) |
| EP (1) | EP2382156B1 (https=) |
| JP (1) | JP5957225B2 (https=) |
| KR (1) | KR20110112387A (https=) |
| CN (1) | CN102272044A (https=) |
| CA (1) | CA2746965A1 (https=) |
| TW (1) | TWI474970B (https=) |
| WO (1) | WO2010076265A2 (https=) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW201010944A (en) * | 2008-04-17 | 2010-03-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| KR20110139281A (ko) | 2009-03-17 | 2011-12-28 | 바스프 에스이 | 열수 조건 하의 리튬-철-포스페이트의 합성 방법 |
| KR101356970B1 (ko) | 2009-05-22 | 2014-02-03 | 샤프 가부시키가이샤 | 정극 활물질, 정극 및 비수 이차 전지 |
| CN102714315A (zh) * | 2009-08-09 | 2012-10-03 | 美洲锂能公司 | 电活性颗粒及由其组成的电极和电池 |
| JP5551019B2 (ja) * | 2009-09-02 | 2014-07-16 | シャープ株式会社 | 正極活物質、正極及び非水二次電池 |
| US9373844B2 (en) | 2010-07-01 | 2016-06-21 | Sharp Kabushiki Kaisha | Positive electrode active substance containing lithium-containing metal oxide |
| JP5132727B2 (ja) | 2010-07-12 | 2013-01-30 | シャープ株式会社 | 正極活物質、正極及び非水電解質二次電池 |
| WO2013091573A1 (zh) * | 2011-12-21 | 2013-06-27 | 台湾立凯电能科技股份有限公司 | 具氧空缺的正极材料及其制法 |
| CN102496714A (zh) * | 2011-12-27 | 2012-06-13 | 天津力神电池股份有限公司 | 一种正极活性物质及其生产方法和所应用的锂离子电池 |
| WO2014021395A1 (ja) * | 2012-07-31 | 2014-02-06 | シャープ株式会社 | 非水電解質二次電池用正極活物質 |
| US20140147586A1 (en) * | 2012-11-27 | 2014-05-29 | Universite De Montreal | Process for making an alkali metal oxyanion comprising iron |
| KR20140076107A (ko) * | 2012-12-12 | 2014-06-20 | 한국전자통신연구원 | 리튬 알루미늄 티타늄 포스페이트 제조방법 |
| GB201223473D0 (en) * | 2012-12-28 | 2013-02-13 | Faradion Ltd | Metal-containing compounds |
| US10086351B2 (en) | 2013-05-06 | 2018-10-02 | Llang-Yuh Chen | Multi-stage process for producing a material of a battery cell |
| CN103500829B (zh) * | 2013-08-15 | 2016-12-28 | 江苏华东锂电技术研究院有限公司 | 磷酸亚铁锂的制备方法 |
| CN103441265B (zh) * | 2013-09-24 | 2015-10-28 | 上海空间电源研究所 | 一种共掺杂富锂复合正极材料及其制备方法 |
| CN103779566A (zh) * | 2014-02-21 | 2014-05-07 | 张萍 | 一种多元素掺杂磷酸锰锂-碳复合正极材料的制备方法 |
| WO2016164617A1 (en) | 2015-04-07 | 2016-10-13 | Brown University | Cation energy storage device and methods |
| CN104966832A (zh) * | 2015-06-02 | 2015-10-07 | 中国科学院青海盐湖研究所 | 一种电化学-化学反应制备金属氧化物或多金属氧化物电极材料的方法 |
| CN106169570A (zh) * | 2016-08-25 | 2016-11-30 | 合肥国轩高科动力能源有限公司 | 一种金属元素掺杂锂离子电池用磷酸钒锂正极材料的制备方法 |
| DE102017106913A1 (de) | 2017-03-30 | 2018-10-04 | Chemische Fabrik Budenheim Kg | Verfahren zur Herstellung von elektrisch leitenden Strukturen auf einem Trägermaterial |
| DE102017106911A1 (de) | 2017-03-30 | 2018-10-04 | Chemische Fabrik Budenheim Kg | Verwendung von kristallwasserfreien Fe(II)-Verbindungen als Strahlungsabsorber |
| DE102017106912A1 (de) * | 2017-03-30 | 2018-10-04 | Chemische Fabrik Budenheim Kg | Verfahren zur Herstellung von Fe(II)P / Fe(II)MetP-Verbindungen |
| CN108530053B (zh) * | 2018-03-30 | 2021-03-30 | 华南理工大学 | 一种pH值敏感变色无机材料及其制备方法 |
| WO2020264464A1 (en) | 2019-06-28 | 2020-12-30 | eJoule, Inc. | Assisted gas flow inside a reaction chamber of a processing system |
| US11673112B2 (en) | 2020-06-28 | 2023-06-13 | eJoule, Inc. | System and process with assisted gas flow inside a reaction chamber |
| US11376559B2 (en) | 2019-06-28 | 2022-07-05 | eJoule, Inc. | Processing system and method for producing a particulate material |
| US11121354B2 (en) | 2019-06-28 | 2021-09-14 | eJoule, Inc. | System with power jet modules and method thereof |
| US12577119B2 (en) * | 2021-11-19 | 2026-03-17 | Crystaphase Products, Inc. | Method for forming insoluble solute adducts using an acidic medium |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6514640B1 (en) | 1996-04-23 | 2003-02-04 | Board Of Regents, The University Of Texas System | Cathode materials for secondary (rechargeable) lithium batteries |
| US6203946B1 (en) * | 1998-12-03 | 2001-03-20 | Valence Technology, Inc. | Lithium-containing phosphates, method of preparation, and uses thereof |
| US6528033B1 (en) | 2000-01-18 | 2003-03-04 | Valence Technology, Inc. | Method of making lithium-containing materials |
| US6777132B2 (en) | 2000-04-27 | 2004-08-17 | Valence Technology, Inc. | Alkali/transition metal halo—and hydroxy-phosphates and related electrode active materials |
| US8057769B2 (en) * | 2000-04-27 | 2011-11-15 | Valence Technology, Inc. | Method for making phosphate-based electrode active materials |
| CA2483918C (en) * | 2002-05-17 | 2007-01-09 | Valence Technology, Inc. | Synthesis of metal compounds useful as cathode active materials |
| ATE433202T1 (de) * | 2002-12-19 | 2009-06-15 | Valence Technology Inc | Aktives elektrodenmaterial und verfahren zur herstellung desselben |
| FR2852148B1 (fr) | 2003-03-07 | 2014-04-11 | Batscap Sa | Materiau pour electrode composite, procede pour sa preparation |
| CN1233054C (zh) | 2003-12-17 | 2005-12-21 | 北京科技大学 | 一种采用微波法制备LiFePO4材料的方法 |
| JP2006155941A (ja) | 2004-11-25 | 2006-06-15 | Kyushu Univ | 電極活物質の製造方法 |
| DE102005012640B4 (de) * | 2005-03-18 | 2015-02-05 | Süd-Chemie Ip Gmbh & Co. Kg | Kreisprozess zur nasschemischen Herstellung von Lithiummetallphosphaten |
| DE102005015613A1 (de) | 2005-04-05 | 2006-10-12 | Süd-Chemie AG | Kristallines Ionenleitendes Nanomaterial und Verfahren zu seiner Herstellung |
| JP4869629B2 (ja) * | 2005-05-30 | 2012-02-08 | 住友大阪セメント株式会社 | リチウム電池用正極活物質の製造方法及びリチウム電池用正極活物質並びにリチウム電池 |
| JP5084131B2 (ja) | 2005-10-28 | 2012-11-28 | トヨタ自動車株式会社 | ＬｉＭｎＰＯ４の製造方法 |
| EP1989747B1 (en) | 2006-02-14 | 2017-04-12 | Dow Global Technologies LLC | Lithium manganese phosphate positive material for lithium secondary battery |
| WO2007113624A1 (en) | 2006-04-06 | 2007-10-11 | High Power Lithium S.A. | Synthesis of nanoparticles of lithium metal phosphate positive material for lithium secondary battery |
| JP5213213B2 (ja) * | 2006-11-27 | 2013-06-19 | 日立マクセル株式会社 | 電気化学素子用活物質、その製造方法、および電気化学素子 |
| JP5115697B2 (ja) * | 2007-05-22 | 2013-01-09 | Ｎｅｃエナジーデバイス株式会社 | リチウム二次電池用正極及びそれを用いたリチウム二次電池 |
| TW201010944A (en) | 2008-04-17 | 2010-03-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| KR20110139281A (ko) | 2009-03-17 | 2011-12-28 | 바스프 에스이 | 열수 조건 하의 리튬-철-포스페이트의 합성 방법 |
| US20140147586A1 (en) * | 2012-11-27 | 2014-05-29 | Universite De Montreal | Process for making an alkali metal oxyanion comprising iron |
-
2009
- 2009-11-30 TW TW098140836A patent/TWI474970B/zh not_active IP Right Cessation
- 2009-12-22 WO PCT/EP2009/067742 patent/WO2010076265A2/en not_active Ceased
- 2009-12-22 CA CA2746965A patent/CA2746965A1/en not_active Abandoned
- 2009-12-22 EP EP09796730.1A patent/EP2382156B1/en not_active Not-in-force
- 2009-12-22 JP JP2011542814A patent/JP5957225B2/ja not_active Expired - Fee Related
- 2009-12-22 US US13/142,606 patent/US9156693B2/en not_active Expired - Fee Related
- 2009-12-22 KR KR1020117017967A patent/KR20110112387A/ko not_active Abandoned
- 2009-12-22 CN CN2009801530676A patent/CN102272044A/zh active Pending
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