JP2011517653A5 - - Google Patents
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- Publication number
- JP2011517653A5 JP2011517653A5 JP2011504453A JP2011504453A JP2011517653A5 JP 2011517653 A5 JP2011517653 A5 JP 2011517653A5 JP 2011504453 A JP2011504453 A JP 2011504453A JP 2011504453 A JP2011504453 A JP 2011504453A JP 2011517653 A5 JP2011517653 A5 JP 2011517653A5
- Authority
- JP
- Japan
- Prior art keywords
- compound
- oxidation state
- hpo
- containing compound
- electrically conductive
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 claims 25
- 238000000034 method Methods 0.000 claims 14
- 239000000203 mixture Substances 0.000 claims 13
- 230000003647 oxidation Effects 0.000 claims 10
- 238000007254 oxidation reaction Methods 0.000 claims 10
- 229910052698 phosphorus Inorganic materials 0.000 claims 7
- 239000004020 conductor Substances 0.000 claims 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 6
- 125000004437 phosphorous atom Chemical group 0.000 claims 6
- 239000003638 chemical reducing agent Substances 0.000 claims 4
- 239000007787 solid Substances 0.000 claims 4
- 239000012798 spherical particle Substances 0.000 claims 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 2
- PMVSDNDAUGGCCE-TYYBGVCCSA-L Ferrous fumarate Chemical compound [Fe+2].[O-]C(=O)\C=C\C([O-])=O PMVSDNDAUGGCCE-TYYBGVCCSA-L 0.000 claims 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 2
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- 229910052744 lithium Inorganic materials 0.000 claims 2
- 229910001416 lithium ion Inorganic materials 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims 2
- 229920000049 Carbon (fiber) Polymers 0.000 claims 1
- 229910018119 Li 3 PO 4 Inorganic materials 0.000 claims 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 1
- 125000004429 atom Chemical group 0.000 claims 1
- 239000006229 carbon black Substances 0.000 claims 1
- 239000004917 carbon fiber Substances 0.000 claims 1
- 239000002134 carbon nanofiber Substances 0.000 claims 1
- 239000002041 carbon nanotube Substances 0.000 claims 1
- 229910021393 carbon nanotube Inorganic materials 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- 229920001940 conductive polymer Polymers 0.000 claims 1
- 238000010304 firing Methods 0.000 claims 1
- 229910002804 graphite Inorganic materials 0.000 claims 1
- 239000010439 graphite Substances 0.000 claims 1
- 229910052748 manganese Inorganic materials 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 239000011574 phosphorus Substances 0.000 claims 1
- 239000002243 precursor Substances 0.000 claims 1
- 238000001694 spray drying Methods 0.000 claims 1
- 229910052720 vanadium Inorganic materials 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US4579808P | 2008-04-17 | 2008-04-17 | |
| US61/045,798 | 2008-04-17 | ||
| PCT/EP2009/054486 WO2009127672A1 (en) | 2008-04-17 | 2009-04-16 | Process for the preparation of crystalline lithium-, iron- and phosphate-comprising materials |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011517653A JP2011517653A (ja) | 2011-06-16 |
| JP2011517653A5 true JP2011517653A5 (enExample) | 2012-06-14 |
| JP5653905B2 JP5653905B2 (ja) | 2015-01-14 |
Family
ID=40935481
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011504453A Active JP5653905B2 (ja) | 2008-04-17 | 2009-04-16 | リチウム、鉄及びリン酸を含有する結晶性材料の製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8673497B2 (enExample) |
| EP (1) | EP2282971B1 (enExample) |
| JP (1) | JP5653905B2 (enExample) |
| KR (1) | KR101592051B1 (enExample) |
| CN (1) | CN102066242B (enExample) |
| CA (1) | CA2721204A1 (enExample) |
| TW (1) | TW200951066A (enExample) |
| WO (1) | WO2009127672A1 (enExample) |
Families Citing this family (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8057769B2 (en) * | 2000-04-27 | 2011-11-15 | Valence Technology, Inc. | Method for making phosphate-based electrode active materials |
| DE102006041762A1 (de) * | 2006-09-04 | 2008-03-06 | Daimler Ag | Vorrichtung und Verfahren zum Befeuchten eines zu einer Brennstoffzelle strömenden Gasstroms |
| CN102123943B (zh) | 2007-10-01 | 2013-07-10 | 巴斯夫欧洲公司 | 制备包含锂、钒和磷酸根的多孔材料的方法 |
| JP5705541B2 (ja) * | 2007-10-01 | 2015-04-22 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | 結晶性リチウム−、バナジウム−、及びフォスフェイト−含有材料を製造するための方法 |
| TW201010944A (en) * | 2008-04-17 | 2010-03-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| TWI440597B (zh) * | 2008-08-26 | 2014-06-11 | Basf Se | 於水熱條件下合成ＬｉＦｅＰＯ4 |
| KR20110139281A (ko) | 2009-03-17 | 2011-12-28 | 바스프 에스이 | 열수 조건 하의 리튬-철-포스페이트의 합성 방법 |
| JP5886193B2 (ja) * | 2009-06-24 | 2016-03-16 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | ＬｉＦｅＰＯ４−炭素合成物を製造するための方法 |
| JP5729802B2 (ja) * | 2009-12-25 | 2015-06-03 | 三菱マテリアル株式会社 | Ｌｉイオン電池用正極活物質、およびその製造方法 |
| CN101885582B (zh) * | 2010-06-11 | 2012-02-08 | 济南大学 | 四元磷酸铁锂玻璃及其制备方法 |
| WO2012006725A1 (en) * | 2010-07-15 | 2012-01-19 | Phostech Lithium Inc. | Battery grade cathode coating formulation |
| KR101253319B1 (ko) * | 2010-09-10 | 2013-04-10 | 국립대학법인 울산과학기술대학교 산학협력단 | 리튬 이차 전지용 양극 활물질, 이의 제조방법 및 이를 포함하는 리튬 이차 전지 |
| JP5557715B2 (ja) * | 2010-12-06 | 2014-07-23 | 株式会社日立製作所 | リチウムイオン二次電池用正極材料およびその製造方法，リチウムイオン二次電池用正極活物質，リチウムイオン二次電池用正極，リチウムイオン二次電池 |
| JP5942852B2 (ja) * | 2010-12-09 | 2016-06-29 | 日本電気株式会社 | 二次電池用正極活物質及びそれを使用した二次電池 |
| US8945498B2 (en) * | 2011-03-18 | 2015-02-03 | Semiconductor Energy Laboratory Co., Ltd. | Method for manufacturing lithium-containing composite oxide |
| WO2012132307A1 (en) | 2011-03-25 | 2012-10-04 | Semiconductor Energy Laboratory Co., Ltd. | Lithium-ion secondary battery |
| JP2012229147A (ja) * | 2011-04-27 | 2012-11-22 | Nichia Corp | オリビン型リチウム遷移金属酸化物及びその製造方法 |
| US9118077B2 (en) | 2011-08-31 | 2015-08-25 | Semiconductor Energy Laboratory Co., Ltd. | Manufacturing method of composite oxide and manufacturing method of power storage device |
| US9249524B2 (en) | 2011-08-31 | 2016-02-02 | Semiconductor Energy Laboratory Co., Ltd. | Manufacturing method of composite oxide and manufacturing method of power storage device |
| EP2665114A1 (de) * | 2012-05-14 | 2013-11-20 | Basf Se | Verfahren zur Herstellung von Elektrodenmaterialien |
| CN102760880A (zh) * | 2012-08-07 | 2012-10-31 | 杨志宽 | 一种高功率磷酸铁锂电池材料及其制备方法 |
| GB201223473D0 (en) * | 2012-12-28 | 2013-02-13 | Faradion Ltd | Metal-containing compounds |
| EP2778126A1 (en) * | 2013-03-15 | 2014-09-17 | Clariant International Ltd. | Lithium transition metal phosphate secondary agglomerates and process for its manufacture |
| JP6089896B2 (ja) * | 2013-04-03 | 2017-03-08 | 株式会社村田製作所 | リン酸鉄リチウムの製造方法 |
| EP2884568A1 (en) * | 2013-12-13 | 2015-06-17 | Basf Se | Process for producing electrode materials |
| JP2015143189A (ja) * | 2015-04-23 | 2015-08-06 | 日亜化学工業株式会社 | オリビン型リチウム遷移金属酸化物及びその製造方法 |
| US20180013151A1 (en) * | 2016-07-08 | 2018-01-11 | Semiconductor Energy Laboratory Co., Ltd. | Positive electrode active material, power storage device, electronic device, and method for manufacturing positive electrode active material |
| CN108706595A (zh) * | 2018-04-23 | 2018-10-26 | 东莞中子科学中心 | 铁基聚阴离子AxFe3P5SiO19化合物及制备方法 |
| KR102713210B1 (ko) | 2019-02-13 | 2024-10-02 | 주식회사 엘지에너지솔루션 | 괴타이트를 포함하는 리튬 이차전지용 양극 및 이를 구비한 리튬 이차전지 |
| CN110350189A (zh) * | 2019-05-23 | 2019-10-18 | 青海泰丰先行锂能科技有限公司 | 一种高容量高压密橄榄石阴极材料的制备方法 |
| AU2020203801B1 (en) * | 2020-06-09 | 2021-03-11 | VSPC Ltd | Method for making lithium metal phosphates |
| CN112723332B (zh) * | 2021-04-02 | 2021-07-13 | 金驰能源材料有限公司 | 一种超细多孔结构的电池级磷酸铁及其制备方法 |
| WO2025051918A1 (en) | 2023-09-07 | 2025-03-13 | Sun Chemical Corporation | Iron phosphate-comprising materials |
Family Cites Families (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5910382A (en) * | 1996-04-23 | 1999-06-08 | Board Of Regents, University Of Texas Systems | Cathode materials for secondary (rechargeable) lithium batteries |
| US6514640B1 (en) | 1996-04-23 | 2003-02-04 | Board Of Regents, The University Of Texas System | Cathode materials for secondary (rechargeable) lithium batteries |
| US6203946B1 (en) * | 1998-12-03 | 2001-03-20 | Valence Technology, Inc. | Lithium-containing phosphates, method of preparation, and uses thereof |
| CA2270771A1 (fr) * | 1999-04-30 | 2000-10-30 | Hydro-Quebec | Nouveaux materiaux d'electrode presentant une conductivite de surface elevee |
| US6528033B1 (en) * | 2000-01-18 | 2003-03-04 | Valence Technology, Inc. | Method of making lithium-containing materials |
| CA2320661A1 (fr) * | 2000-09-26 | 2002-03-26 | Hydro-Quebec | Nouveau procede de synthese de materiaux limpo4 a structure olivine |
| EP1261050A1 (en) | 2001-05-23 | 2002-11-27 | n.v. Umicore s.a. | Lithium transition-metal phosphate powder for rechargeable batteries |
| GB2386276B (en) * | 2002-03-09 | 2004-09-08 | Rx Technology Europ Ltd | Image capture and retrieval apparatus |
| FR2848205B1 (fr) * | 2002-12-05 | 2006-03-24 | Commissariat Energie Atomique | Composes d'insertion du lithium substitues au bore, materiaux actifs d'electrodes, accumulateurs et dispositifs electrochromes |
| FR2852148B1 (fr) | 2003-03-07 | 2014-04-11 | Batscap Sa | Materiau pour electrode composite, procede pour sa preparation |
| JP4522682B2 (ja) * | 2003-10-09 | 2010-08-11 | 住友大阪セメント株式会社 | 電極材料粉体の製造方法と電極材料粉体及び電極並びにリチウム電池 |
| CN1233054C (zh) | 2003-12-17 | 2005-12-21 | 北京科技大学 | 一种采用微波法制备LiFePO4材料的方法 |
| CA2906604A1 (en) * | 2003-12-23 | 2005-07-07 | Laurent Gauthier | Process for preparing electroactive insertion compounds and electrode materials obtained therefrom |
| CN100336247C (zh) * | 2004-03-30 | 2007-09-05 | 中国科学院物理研究所 | 一种锂离子电池的磷酸盐正极材料的制备方法 |
| JP2007230784A (ja) * | 2004-03-30 | 2007-09-13 | Agc Seimi Chemical Co Ltd | リチウム鉄複合酸化物の製造方法 |
| JP2006155941A (ja) | 2004-11-25 | 2006-06-15 | Kyushu Univ | 電極活物質の製造方法 |
| DE102005012640B4 (de) | 2005-03-18 | 2015-02-05 | Süd-Chemie Ip Gmbh & Co. Kg | Kreisprozess zur nasschemischen Herstellung von Lithiummetallphosphaten |
| DE102005015613A1 (de) * | 2005-04-05 | 2006-10-12 | Süd-Chemie AG | Kristallines Ionenleitendes Nanomaterial und Verfahren zu seiner Herstellung |
| WO2006116251A2 (en) * | 2005-04-26 | 2006-11-02 | The University Of Chicago | Processes for making dense, spherical, active materials for lithium-ion cells |
| JP4869629B2 (ja) * | 2005-05-30 | 2012-02-08 | 住友大阪セメント株式会社 | リチウム電池用正極活物質の製造方法及びリチウム電池用正極活物質並びにリチウム電池 |
| JP4804045B2 (ja) * | 2005-06-15 | 2011-10-26 | Ａｇｃセイミケミカル株式会社 | リチウム鉄複合酸化物の製造方法 |
| US7524529B2 (en) * | 2005-09-09 | 2009-04-28 | Aquire Energy Co., Ltd. | Method for making a lithium mixed metal compound having an olivine structure |
| CN100376475C (zh) * | 2005-10-14 | 2008-03-26 | 江苏大学 | 一种球形多孔高密度LiFePO4粉体及其制备方法 |
| CN100420076C (zh) * | 2005-12-19 | 2008-09-17 | 南开大学 | 溶胶凝胶法合成锂离子电池正极材料磷酸钒锂的方法 |
| KR100821832B1 (ko) | 2007-04-20 | 2008-04-14 | 정성윤 | 리튬전이금속 인산화물의 나노입자 분말의 제조방법 |
| JP5293936B2 (ja) * | 2007-05-21 | 2013-09-18 | 戸田工業株式会社 | 非水電解質二次電池用オリビン型複合酸化物及びその製造方法、並びに二次電池 |
| CN102123943B (zh) * | 2007-10-01 | 2013-07-10 | 巴斯夫欧洲公司 | 制备包含锂、钒和磷酸根的多孔材料的方法 |
| JP5705541B2 (ja) * | 2007-10-01 | 2015-04-22 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | 結晶性リチウム−、バナジウム−、及びフォスフェイト−含有材料を製造するための方法 |
| CN101980956A (zh) * | 2008-03-31 | 2011-02-23 | 户田工业株式会社 | 磷酸铁锂颗粒粉末的制造方法、橄榄石型结构的磷酸铁锂颗粒粉末、使用该磷酸铁锂颗粒粉末的正极材料片和非水溶剂类二次电池 |
| JP5517032B2 (ja) * | 2008-03-31 | 2014-06-11 | 戸田工業株式会社 | 非水電解質二次電池用オリビン型複合酸化物粒子粉末及びその製造方法、並びに二次電池 |
| KR20110139281A (ko) * | 2009-03-17 | 2011-12-28 | 바스프 에스이 | 열수 조건 하의 리튬-철-포스페이트의 합성 방법 |
-
2009
- 2009-04-06 TW TW098111398A patent/TW200951066A/zh unknown
- 2009-04-16 WO PCT/EP2009/054486 patent/WO2009127672A1/en not_active Ceased
- 2009-04-16 CN CN200980122747.1A patent/CN102066242B/zh active Active
- 2009-04-16 CA CA2721204A patent/CA2721204A1/en not_active Abandoned
- 2009-04-16 EP EP09731835.6A patent/EP2282971B1/en active Active
- 2009-04-16 KR KR1020107025817A patent/KR101592051B1/ko active Active
- 2009-04-16 JP JP2011504453A patent/JP5653905B2/ja active Active
- 2009-04-16 US US12/988,222 patent/US8673497B2/en active Active
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